• Title/Summary/Keyword: Structure determination

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Chromatographical Determination of Radiochemical Purity of Hippuran $^131 I$

  • Kim, Jaerok;Kim, Tae-Ho
    • Nuclear Engineering and Technology
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    • v.5 no.3
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    • pp.234-239
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    • 1973
  • A recently known method of paper chromatographical separation of o-iodobenzoic acid-$^{131}$ I and o-iodohippuric acid-$^{131}$ I was found to be in error. The solvent mixture proposed in the method for the efficient separation of the two compounds of similar structure not only be made nonhomogeneous but also brings about no separation. It was also confirmed that no o-iodohippuric acid is converted to o-iodobenzoic acid during the process for Hippuran -$^{131}$ I preparation by isotopic exchange. Upon it, an alternate method of chromato-graphical determination of radiochemical purity of Hippuran-$^{131}$ I is proposed in present paper.

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A Study on the Determination of Cutting Work Envelope of Articular Robot for H-beam Cutting (H-beam 절단용 다관절 로봇의 절단작업영역 설정에 관한 연구)

  • Park, Ju-Yong;Lee, Yong-Gu
    • Journal of Welding and Joining
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    • v.27 no.6
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    • pp.55-61
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    • 2009
  • This study aims for determination of cutting work envelope of an articular robot for H-beam cutting. The robot has its own work envelope. The cutting of piece with groove requires the specific position of the torch which contracts the work envelope. This study suggested the new method to determine the cutting work envelope for this case. The method simplified the problem by use of the combination of inverse kinematics and forward kinematics. The method was used for cutting the H-beam with groove. The cutting work envelope was determined easily. The result was verified by 3D simulation system which implements the articular robot with 6 axes and the H-beam in the virtual shop.

Buzz Margin Determination of Supersonic Intake (초음속 흡입구의 버즈여유 결정기법)

  • Park, Ik-Soo;Choi, Jong-Ho;Yoon, Hyun-Gull;Lim, Jin-Shik
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2011.04a
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    • pp.132-135
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    • 2011
  • A technology for buzz margin determination is suggested to obtain stable shock structure and high compression efficiency of supersonic intake. By using the shock equilibrium equation of supersonic intake, sensitivity equation of terminal shock position for free stream and back pressure is induced and disturbances are quantified through statistical approach. Numerical results show that the sensitivity of shock position for disturbances is proportional to Mach number and the back pressure is dominant for variance of terminal shock position.

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Four New Furanosesquiterpenes Isolated from the Marine Sponge Dysidea species

  • Yeong Du Yoo;Jung-Rae Rho
    • Journal of the Korean Magnetic Resonance Society
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    • v.27 no.4
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    • pp.35-41
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    • 2023
  • From a marine sponge Dysidea species, four new furanosesquiterterpenoids were isolated and characterized. Their structural elucidation was achieved through an extensive analysis employing NMR, MS data, and DFT method. Notably, all compounds shared as identical molecular formula. Compound 2 was identified as a derivative of compound 1, while compounds 3 and 4 exhibited an identical planar structure. Determination of the configurations of chiral centers in compounds 1 and 2 involved a comparative analysis between measured and calculated ECD spectra, along with the application of DP4+ probability analysis. Distinctly, the configurations of isomers 3 and 4 were established by scrutinizing proton chemical shifts based on the NOE correlation.

Experimental study on the cable rigidness and static behaviors of AERORail structure

  • Li, Fangyuan;Wu, Peifeng;Liu, Dongjie
    • Steel and Composite Structures
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    • v.12 no.5
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    • pp.427-444
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    • 2012
  • This paper presented a new aerial platform-AERORail for rail transport and its structure evolution based on the elastic stiffness of cable; through the analysis on the cable properties when the cable supported a small service load with high-tensile force, summarized the theoretical basis of the AERORail structure and the corresponding simplified analysis model. There were 60 groups of experiments for a single naked cable model under different tensile forces and different services loads, and 48 groups of experiments for the cable with rail combined structure model. The experimental results of deflection characteristics were compared with the theoretical values for these two types of structures under the same conditions. It proved that the results almost met the classical cable theory. The reason is that a small deflection was required when this structure was applied. After the tension increments tests with moving load, it is verified that the relationships between the structure stiffness and tension force and service load are simple. Before further research and applications are made, these results are necessary for the determination of the reasonable and economic tensile force, allowable service load for the special span length for this new platform.

Consideration of CCD Gate Structure in the Determination of the Point Spread Function of Yohkoh Soft X-Ray Telescope (SXT)

  • Shin, Jun-Ho;Sakurai, Takashi
    • The Bulletin of The Korean Astronomical Society
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    • v.37 no.1
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    • pp.93.2-93.2
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    • 2012
  • Point Spread Function (PSF) is one of the most important optical characteristics for describing the performance of a telescope. And a concept of subpixelization is inevitable in evaluating the undersampled PSF (Shin and Sakurai 2009). Then, the internal structure of Yohkoh SXT CCD pixel is not uniform: For the top half of pixel area, the X-ray should pass a so-called gate structure where the charges are transferred to an output amplifier. This gate structure shows energy-dependent sensitivity (Tsuneta et al. 1991). For example, for Al-K (8.34 A) X-ray emission, the transmission of the polysilicon gate is about 0.9. Also, for the peak coronal response of the SXT thin filters, around 17 angstrom (0.729 keV), the transmission of the gate is about 0.6, falling off sharply towards longer wavelengths. It should be noted that this spectrally dependent non-uniform response of each CCD pixel will certainly have a noticeable effect on the properties of the PSF at longer wavelengths. Therefore, especially for analyzing the undersampled PSF of low energy source, a careful consideration of non-uniform internal pixel structure is required in determining the shape of the PSF core. The details on the effect of gate structure will be introduced in our presentation.

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Optimum Design of the Power Yacht Based on Micro-Genetic Algorithm

  • Park, Joo-Shin;Kim, Yun-Young
    • Journal of Navigation and Port Research
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    • v.33 no.9
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    • pp.635-644
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    • 2009
  • The optimum design of power yacht belongs to the nonlinear constrained optimization problems. The determination of scantlings for the bow structure is a very important issue with in the whole structural design process. The derived design results are obtained by the use of real-coded micro-genetic algorithm including evaluation from Lloyd's Register small craft guideline, so that the nominal limiting stress requirement can be satisfied. In this study, the minimum volume design of bow structure on the power yacht was carried out based on the finite element analysis. The target model for optimum design and local structural analysis is the bow structure of a power yacht. The volume of bow structure and the main dimensions of structural members are chosen as an objective function and design variable, respectively. During optimization procedure, finite element analysis was performed to determine the constraint parameters at each iteration step of the optimization loop. optimization results were compared with a pre-existing design and it was possible to reduce approximately 19 percents of the total steel volume of bow structure from the previous design for the power yacht.

Vibration-based method for story-level damage detection of the reinforced concrete structure

  • Mehboob, Saqib;Zaman, Qaiser U.
    • Computers and Concrete
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    • v.27 no.1
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    • pp.29-39
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    • 2021
  • This study aimed to develop a method for the determination of the damaged story in reinforced concrete (RC) structure with ambient vibrations, based on modified jerk energy methodology. The damage was taken as a localized reduction in the stiffness of the structural member. For loading, random white noise excitation was used, and dynamic responses from the finite element model (FEM) of 4 story RC shear frame were extracted at nodal points. The data thus obtained from the structure was used in the damage detection and localization algorithm. In the structure, two damage configurations have been introduced. In the first configuration, damage to the structure was artificially caused by a local reduction in the modulus of elasticity. In the second configuration, the damage was caused, using the Elcentro1940 and Kashmir2005 earthquakes in real-time history. The damage was successfully detected if the frequency drop was greater than 5% and the mode shape correlation remained less than 0.8. The results of the damage were also compared to the performance criteria developed in the Seismostruct software. It is demonstrated that the proposed algorithm has effectively detected the existence of the damage and can locate the damaged story for multiple damage scenarios in the RC structure.

Age Determination and Estimation of Growth Parameters Using Otoliths of Small Yellow Croaker, Pseudosciaena polyactis Bleeker in Korean Waters (이석을 이용한 참조기(Pseudosciaena polyactis Bleeker)의 연령사정과 성장식 추정)

  • 이만우;장창익;이장욱
    • Journal of the Korean Society of Fisheries and Ocean Technology
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    • v.36 no.3
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    • pp.222-233
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    • 2000
  • A methodology for determining age by otolith of small yellow croaker, Pseudosoiaena polyactis Bleeker, was developed. A thin section method was chosen to be suitable for age determination because the otolith had a three-dimensional shape and thus it was not possible to read the otolith rings on the surface. The clear rings were identified on the vertical-axis cross-sectioned otoliths. The total length-total weight relationship and the growth parameters were estimated with error structure to endow with accuracy. In the relationship between total length and total weight, a multiplicative error structure was assumed because variability in growth increased as a function of the length, and the estimated equation was $W=0.0049L^{3.2153}$. The variability in growth was constant as a function of the age, revealing an additive error structure. The von Bertalanffy growth parameters were obtained from a nonlinear regression as $L_{\infty}= 37.11cm, K=0.20/yr and t_0=-1.88.$

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A Study on the Practical Load with T-shape Joint Structure by the FEA (유한요소해석에 의한 T형 결합구조물에서의 실하중 산출에 관한 연구)

  • 송준혁;김경재;박형일;강희용;김동우;양성모
    • Transactions of the Korean Society of Automotive Engineers
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    • v.9 no.2
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    • pp.107-115
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    • 2001
  • It is required more precise analysis for practical load because of complexities and varieties of vehicle structure. To establish the numerical model, many researchers have been developed designing tools for linking F.E. Analysis results and experimental results. There studies have generally focused on each experimental method or analytical method separately. There are few studies based on both methods. This paper conceives new procedure for the determination of the load direction and magnitude applied on mechanical structures. New procedure is the combination of the analytical and empirical method with analyzed strain by F.E. Analysis under unit load and with measured principal stress by strain gages under driving load, respectively. In this paper, we theorize the procedure of practical load determination and make the validity and the practicality of the procedure with the application to T-shape jointed structure. F.E. Analysis is conducted to get the principal stress on arbitrary points in the F.E. model of T-shape joint under unit load. Then experiment is carried out to get the principal stress on the same points of F.E. model. To demonstrate the actual driving condition, the load conditions are bending and torsion. From these two data sets, the magnitude, the direction and the position of load can be obtained. Theory and practice do not always coincide; since there are some errors such as ill-poseness, measuring error and modeling error in experimental data, we examine the proper method of error minimization.

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