• Title/Summary/Keyword: Structural Adhesive

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Cure Monitoring of Epoxy Resin by Using Fiber Bragg Grating Sensor (광섬유 브래그 격자 센서를 이용한 에폭시 수지의 경화도 모니터링)

  • Lee, Jin-Hyuk;Kim, Dae-Hyun
    • Journal of the Korean Society for Nondestructive Testing
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    • v.36 no.3
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    • pp.211-216
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    • 2016
  • In several industrial fields, epoxy resin is widely used as an adhesive for co-curing and manufacturing various structures. Controlling the manufacturing process is required for ensuring robust bonding performance and the stability of the structures. A fiber optic sensor is suitable for the cure monitoring of epoxy resin owing to the thready shape of the sensor. In this paper, a fiber Bragg grating (FBG) sensor was applied for the cure monitoring of epoxy resin. Based on the experimental results, it was demonstrated that the FBG sensor can monitor the status of epoxy resin curing by measuring the strain caused by volume shrinkage and considering the compensation of temperature. In addition, two types of epoxy resin were used for the cure-monitoring; moreover, when compared to each other, it was found that the two types of epoxy had different cure-processes in terms of the change of strain during the curing. Therefore, the study proved that the FBG sensor is very profitable for the cure-monitoring of epoxy resin.

Antibacterial activity of enrofloxacin loaded gelatin-sodium alginate composite nanogels against intracellular Staphylococcus aureus small colony variants

  • Luo, Wanhe;Liu, Jinhuan;Algharib, Samah Attia;Chen, Wei
    • Journal of Veterinary Science
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    • v.23 no.3
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    • pp.48.1-48.12
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    • 2022
  • Background: The poor intracellular concentration of enrofloxacin might lead to treatment failure of cow mastitis caused by Staphylococcus aureus small colony variants (SASCVs). Objectives: In this study, enrofloxacin composite nanogels were developed to increase the intracellular therapeutic drug concentrations and enhance the efficacy of enrofloxacin against cow mastitis caused by intracellular SASCVs. Methods: Enrofloxacin composite nanogels were formulated by an electrostatic interaction between gelatin (positive charge) and sodium alginate (SA; negative charge) with the help of CaCl2 (ionic crosslinkers) and optimized by a single factor test using the particle diameter, zeta potential (ZP), polydispersity index (PDI), loading capacity (LC), and encapsulation efficiency (EE) as indexes. The formation mechanism, structural characteristics, bioadhesion ability, cellular uptake, and the antibacterial activity of the enrofloxacin composite nanogels against intracellular SASCVs strain were studied systematically. Results: The optimized formulation was comprised of 10 mg/mL (gelatin), 5 mg/mL (SA), and 0.25 mg/mL (CaCl2). The size, LC, EE, PDI, and ZP of the optimized enrofloxacin composite nanogels were 323.2 ± 4.3 nm, 15.4% ± 0.2%, 69.6% ± 1.3%, 0.11 ± 0.02, and -34.4 ± 0.8 mV, respectively. Transmission electron microscopy showed that the enrofloxacin composite nanogels were spherical with a smooth surface and good particle size distributions. In addition, the enrofloxacin composite nanogels could enhance the bioadhesion capacity of enrofloxacin for the SASCVs strain by adhesive studies. The minimum inhibitory concentration, minimum bactericidal concentration, minimum biofilm inhibitory concentration, and minimum biofilm eradication concentration were 2, 4, 4, and 8 ㎍/mL, respectively. The killing rate curve had a concentration-dependent bactericidal effect as increasing drug concentrations induced swifter and more radical killing effects. Conclusions: This study provides a good tendency for developing enrofloxacin composite nanogels for treating cow mastitis caused by intracellular SASCVs and other intracellular bacterial infections.

Efficient influence of cross section shape on the mechanical and economic properties of concrete canvas and CFRP reinforced columns management using metaheuristic optimization algorithms

  • Ge, Genwang;Liu, Yingzi;Al-Tamimi, Haneen M.;Pourrostam, Towhid;Zhang, Xian;Ali, H. Elhosiny;Jan, Amin;Salameh, Anas A.
    • Computers and Concrete
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    • v.29 no.6
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    • pp.375-391
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    • 2022
  • This paper examined the impact of the cross-sectional structure on the structural results under different loading conditions of reinforced concrete (RC) members' management limited in Carbon Fiber Reinforced Polymers (CFRP). The mechanical properties of CFRC was investigated, then, totally 32 samples were examined. Test parameters included the cross-sectional shape as square, rectangular and circular with two various aspect rates and loading statues. The loading involved concentrated loading, eccentric loading with a ratio of 0.46 to 0.6 and pure bending. The results of the test revealed that the CFRP increased ductility and load during concentrated processing. A cross sectional shape from 23 to 44 percent was increased in load capacity and from 250 to 350 percent increase in axial deformation in rectangular and circular sections respectively, affecting greatly the accomplishment of load capacity and ductility of the concentrated members. Two Artificial Intelligence Models as Extreme Learning Machine (ELM) and Particle Swarm Optimization (PSO) were used to estimating the tensile and flexural strength of specimen. On the basis of the performance from RMSE and RSQR, C-Shape CFRC was greater tensile and flexural strength than any other FRP composite design. Because of the mechanical anchorage into the matrix, C-shaped CFRCC was noted to have greater fiber-matrix interfacial adhesive strength. However, with the increase of the aspect ratio and fiber volume fraction, the compressive strength of CFRCC was reduced. This possibly was due to the fact that during the blending of each fiber, the volume of air input was increased. In addition, by adding silica fumed to composites, the tensile and flexural strength of CFRCC is greatly improved.

Enhanced antibacterial activity of tilmicosin against Staphylococcus aureus small colony variants by chitosan oligosaccharide-sodium carboxymethyl cellulose composite nanogels

  • Luo, Wanhe;Liu, Jinhuan;Zhang, Shanling;Song, Wei;Algharib, Samah Attia;Chen, Wei
    • Journal of Veterinary Science
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    • v.23 no.1
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    • pp.1.1-1.11
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    • 2022
  • Background: The poor bioadhesion capacity of tilmicosin resulting in treatment failure for Staphylococcus aureus small colony variants (SASCVs) mastitis. Objectives: This study aimed to increase the bioadhesion capacity of tilmicosin for the SASCVs strain and improve the antibacterial effect of tilmicosin against cow mastitis caused by the SASCVs strain. Methods: Tilmicosin-loaded chitosan oligosaccharide (COS)-sodium carboxymethyl cellulose (CMC) composite nanogels were formulated by an electrostatic interaction between COS (positive charge) and CMC (negative charge) using sodium tripolyphosphate (TPP) (ionic crosslinkers). The formation mechanism, structural characteristics, bioadhesion, and antibacterial activity of tilmicosin composite nanogels were studied systematically. Results: The optimized formulation was comprised of 50 mg/mL (COS), 32 mg/mL (CMC), and 0.25 mg/mL (TPP). The size, encapsulation efficiency, loading capacity, polydispersity index, and zeta potential of the optimized tilmicosin composite nanogels were 357.4 ± 2.6 nm, 65.4 ± 0.4%, 21.9 ± 0.4%, 0.11 ± 0.01, and -37.1 ± 0.4 mV, respectively; the sedimentation rate was one. Scanning electron microscopy showed that tilmicosin might be incorporated in nano-sized crosslinked polymeric networks. Moreover, adhesive studies suggested that tilmicosin composite nanogels could enhance the bioadhesion capacity of tilmicosin for the SASCVs strain. The inhibition zone of native tilmicosin, tilmicosin standard, and tilmicosin composite nanogels were 2.13 ± 0.07, 3.35 ± 0.11, and 1.46 ± 0.04 cm, respectively. The minimum inhibitory concentration of native tilmicosin, tilmicosin standard, and tilmicosin composite nanogels against the SASCVs strain were 2, 1, and 1 ㎍/mL, respectively. The in vitro time-killing curves showed that the tilmicosin composite nanogels increased the antibacterial activity against the SASCVs strain. Conclusions: This study provides a potential strategy for developing tilmicosin composite nanogels to treat cow mastitis caused by the SASCVs strain.

Bond and Flexural Behavior of RC Beams Strengthened Using Ductile PET (고연성 PET 섬유로 보강된 철근콘크리트 보의 부착 및 휨 거동)

  • Park, Hye-Sun;Kim, So-Young;Lim, Myung-Kwan;Choi, Donguk
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.20 no.6
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    • pp.30-39
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    • 2016
  • An experimental study was performed to investigate flexural performance and bond characteristics of RC beams strengthened using ductile polyethylene terephthalate(PET) with low elastic modulus. Bond tests were planned and completed following CSA S806. Test variables were fiber type and fiber amount. Also, total of 8 RC beams was tested. Major test variables of the beam tests included section ductility(${\mu}=3.4$, 7.0), fiber type(CF, GF, PET) and amount of fiber strengthening. Moment-curvature analyses of the beam sections were also performed. In bond tests, the bond stress distribution as well as the maximum bond stress increased with increasing amount of PET. In case of 10 layers of PET, the effective bond length was 60 mm with the maximum and the average bond stress of 2.33 and 2.10 MPa, respectively. RC beam test results revealed that the moment capacity of the RC beams strengthened using PET 10 and 20 layers increased over the control beam with little reduction in ductility by fiber strengthening. All beams strengthened using PET resulted in ductile flexural failure without any sign of fiber debonding or fiber rupture. It was important to include the mechanical properties of adhesive in the moment-curvature analysis of PET-strengthened beam sections.

Moment Resistance Performance Evaluation of Larch Glulam Joints using GFRP-reinforced Laminated Plate and GFRP Rod (GFRP 보강적층판 및 GFRP rod를 이용한 낙엽송 집성재 접합부의 모멘트저항 성능평가)

  • Jung, Hong-Ju;Song, Yo-Jin;Lee, In-Hwan;Hong, Soon-Il
    • Journal of the Korean Wood Science and Technology
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    • v.44 no.1
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    • pp.40-47
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    • 2016
  • Instead of metal connector generally used on the structural glued laminated timber rahmen joints, the GFRP reinforced laminated plates combining veneer and GFRP (Glass Fiber Reinforced Plastic) and bonded type GFRP rod were used as the connectors. As a result of moment resistance performance evaluation on the joint part applied with these connectors, the yield moment of specimen using the GFRP reinforced laminated plates and GFRP rod pin was measured 4 % lower in comparison to the specimen (Type-1) using the metal connectors, but the initial rotational stiffness was measured 29% higher. Also, the yield moment and rotational stiffness of the specimen using the GFRP-reinforced laminated plates and wood (Eucalyptus marginata) pin showed were measured 11% and 56% higher in comparison to the Type-1 specimen, showing the best performance. It was also confirmed through the failure shape and perfect elasto-plasticity analysis that it showed ductility behavior, not brittle fracture, from the shear resisting force by the pin and the bonding strength increased and the unification of member was carried out. On the other hand, in case of the specimen bonded with GFRP rod, it was impossible to measure the bonding performance or it was measured very low due to poor bonding.

Fine Structure of the Silk Spinning Apparatus in the Spider Nurscia albofasciata (살깃자갈거미(Nurscia albofasciata) 방적장치의 미세구조)

  • Park, Eun-Ah;Moon, Myung-Jin
    • Applied Microscopy
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    • v.39 no.2
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    • pp.157-165
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    • 2009
  • Here we demonstrate the fine structural characteristics of the spigots on the cribellum and its peculiar sieve-like structure at the aspects of the functional significance. The surface of the cribellum is covered by hundred of tiny spigots which producing numerous cribellate silk fibrils. It has been known that the cribellar silk is considered as a quite different sort of catching silk with dry-adhesive properties. By our fine structural observation using the field emission scanning electron microscopy (FESEM), the titanoecid spiders have a specialized sieve-like plate just in front of the anterior spinnerets. The other types of the silk spigots were identified as follows: ampullate, pyriform and aciniform glands. Two pairs of major ampullate glands send secretory ductules to the anterior spinnerets, and another 1~2 pairs of minor ampullate glands supply the median spinnerets. In addition, the pyriform glands send ductules to the anterior spinnerets, and the aciniform glands feed silk into the median and the posterior spinnerets, respectively. Characteristically, 2 distinct types (A & B types) of the aciniform spigots were identified in this spider, and the spigots of the aciniform B type are always detected at the posterior spinneret, however sexual dimorphism for spigot is unlikely to be exhibited in this species of spider.

Seismic Performance Evaluation of Masonry Walls Retrofitted with Semi-buried Lattice Reinforcement (조적식 구조물의 부분 매입식 격자철근 보강기법의 내진 성능 평가)

  • Kim, Sang Hyo;Choi, Moon Seock;Park, Se Jun;Ahn, Jin Hee
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.15 no.3
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    • pp.88-98
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    • 2011
  • Masonry structure is a style of building which has been widely applied as residential facilities of low and middle stories, commercial and public facilities etc. But it is possible to destroy by loss of adhesive strength or sliding when lateral forces, such as earthquake, occurs. This study proposes a seismic retrofit method for masonry structure and its seismic performance is demonstrated by shaking table test. Two specimens per each shaking direction were made, having out-of-plane(weak axis) and in-plane(strong axis) direction. External load of 1 ton was also applied for each specimen during the test, to model the behavior of reinforced masonry wall. As a result of shaking table tests, it is shown that the specimen applying the proposed seismic retrofit method showed acceptable behaviors in both of Korea building design criteria(0.14g) and USA seismic criteria suggested by IBC(0.4g). However, it was observed that stiffness of the specimen toward out-of-plane was rapidly decreasing when seismic excitations over 0.14g were loaded. In comparison of relative displacements, maximum relative displacement of specimens which were accelerated toward out-of-plane with 0.4g at once was 29~31% of maximum relative displacement when specimens were gradually accelerated from 0.08g to 0.4g, while the maximum relative displacement of specimens accelerated toward in-plane has similar value in both cases. Therefore, it is concluded that the wall accelerated toward out-of-plane is more affected by hair crack or possible fatigues caused by seismic excitation.

Flexural Behavior of High-Strength Reinforced Concrete Beam with Recycled Aggregate Strengthened by FRP Plate (FRP로 보강된 순환골재 고강도 철근콘크리트 보의 휨거동)

  • Hong, Seong-Uk;Lee, Seung-Ho;Kim, Seung-Hun
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.22 no.4
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    • pp.126-132
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    • 2018
  • As means to increase the use of concrete with recycled coarse aggregate (RCA), this study aims to evaluate the applicability for flexural strengthening of reinforced concrete beam with high-strength concretes and RCA on which FRP plates, used for repair and strengthening of old and low-durability reinforced concrete structures, is applied. In order to increase the adhesive force of epoxy and FRP plate, FRP plate was installed according to Near-Surface-Mounted (NSM) method. 12 specimens were manufactured using substitution rate of RCA (30%), concrete strengths (40MPa, 60MPa), diameters of deformed bar (D10, D13), and types of FRP plate (AFRP, CFRP) as variables to analyse flexural performance according to FRP plate and substitution rate of recycled aggregate. As a result, in all specimens, specimens strengthened by FRP plate showed a maximum of 17% increase in performance compared to specimens without FRP plate and strengthening performance of CFRP was found to be higher than AFRP. When modulus of rupture was used, the value of cracking moment was similar to that of the reference equation. As bending moment of some specimens strengthened by FRP plate failed to satisfy the criteria of KCI 2012 and ACI 440-2R, additional experiment is deemed as necessary.

A Study on the Eco-Friendly Durable Pre-Painting for Concrete Structure (콘크리트 구조물의 친환경 내구성 도장에 관한 기초 연구)

  • Jo, Byung Wan;Choi, Ji Sun;Lee, Seong Won
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.17 no.2
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    • pp.110-116
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    • 2013
  • A concrete structure has become bigger and higher because of development of construction technology and a change in construction environment. Also it tends to focus on repairing, reinforcement and exterior in harmony with environment for structure maintenance and performance improvement. The research is about eco friendly durable painting applicable to concrete structure using civil and architecture. it purpose to improve external beauties and durable problems due to flexibility by variation of temperature, adhesion of exterior wall, crack and delamination in existing organic and mineral painting. For those problems, we made a eco friendly pre-paint that is made with preliminary treatment mixture as a highly enriched waterproof agent and adhesive increasing agent in preprocessing mixture. Then we performed an experiment on durability of prevention neutralization of concrete, durability abrasion, hiding power, adhesion, temperature resistance and resistance to chemical attack. The result of an experiment shows that hiding power is over 0.96 in standard test, durability abrasion test got higher value 1mg than water paint 75mg and tensile strength is 6 times higher than standard waterproof specification.