• 제목/요약/키워드: Stripping Method

검색결과 163건 처리시간 0.022초

Novel Method for Stripping of Molybdenum(VI) after Its Extraction with Cyanex 301

  • Saberyan, Kamal;Maragheh, Mohammad Ghannadi;Ganjali, Mohammad Reza
    • Bulletin of the Korean Chemical Society
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    • 제25권4호
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    • pp.460-465
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    • 2004
  • Hydrofluoric acid has been used as a novel stripping agent for molybdenum(VI) after its extraction with Cyanex 301. In the extraction step, the effects of parameters such as type and initial concentration of acid, type of diluent, extractant concentration, metal concentration and temperature have been studied. In the stripping step, the effects of various stripping agents on stripping efficiency have been investigated. Hydrofluoric acid has been chosen as an effective stripping agent, and the effects of concentration of hydrofluoric acid, stripping time, volume of hydrofluoric acid and the number of stages of stripping have been studied. Molybdenum(VI) has been effectively separated from a large number of elements in binary mixtures, with a very high tolerance limit. Finally, the optimized method has been extended for the analysis of Mo(VI) in spent molybdenum catalysts.

Dip 추출에서 유체 표면의 영향을 고려한 친환경 포토레지스트 박리공정 (Green Photoresist Stripping Process with the Influence of Free Surface from Dip Withdrawal)

  • 김준현;김승현;정병현;주기태;김용성
    • 한국생산제조학회지
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    • 제25권1호
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    • pp.14-20
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    • 2016
  • This paper describes a green stripping process to effectively strip the remaining DFR layer on a non-alkali-based ITO glass surface after an etching process. A stripper, water-soluble amine compound, is used to investigate the characteristics of stripping ability and to suggest a valid method for the green process. Increasing the composition (5-30% concentration) of the ethanol amine-based stripper was found to greatly reduce the stripping time applied in the dipping method. The composition (30%) achieved an excellent stripping effect and free-residue impurities. Additionally, it was possible to obtain the effect of stripping in a way to sustain the release before generating DFR sludge from the ITO glass surface by using dipping condition (stripping time) in the composition. An Additional stripping process (buffering) out of dipping can realize productivity improvement and cost reduction because of the higher proportion of re-use of the stripping solution used in the DFR removal step.

디더 운동 측정치 모델 기반 링레이저 자이로 스트리핑 방법 (Stripping Method of Ring Laser Gyroscope Based on Measurement Model of Dither Motion)

  • 김천중;심규민
    • 한국군사과학기술학회지
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    • 제17권4호
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    • pp.531-536
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    • 2014
  • There are trapping and stripping methods as the technique to remove the dither motion from RLG(Ring Laser Gyro) output. V/F converter output of angular sensor to measure the dither motion is used in stripping method. But bias and scale factor error is always included in V/F converter output and is a critical limiting factor for the wide application of stripping method to RLG. Therefore there have been many researches to solve this problem. The method to accurately estimate the bias and scale factor error of V/F converter using measurements of the angular sensor acquired at data sampling rate of INS is presented in this paper. To this end, stripping technique based on model of dither motion is newly applied.

피부장벽회복에 영향을 미치는 인자에 관한 연구 (The study on the factors which improve skin barrier recovery)

  • 차재훈;김윤범
    • 한방안이비인후피부과학회지
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    • 제21권2호
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    • pp.39-45
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    • 2008
  • Objective : Skin barrier protects skin against harmful environment. Its function includes antimicrobial barrier as well as physical barrier. But there are few studies about the factors which improve skin barrier recovery after injury. The aim of this study is to investigate the factors which improve skin barrier recovery. Method : Nine hairless mice was anesthetized by inhalation and we tape stripped them. We used thermometer to know temperature one day ago, before anesthesia, before tape stripping, and after tape stripping. Vapometer was used to know transepidermal water loss before tape stripping, after tape stripping. And we used doppler flowmeter to measure blood flow before tape stripping, after tape stripping. Result : After analyzed data, we concluded that temperature was lower after anesthesia than before anesthesia and after tape stripping than before tape stripping. We could know that transepidermal water loss was lower after tape stripping than before tape stripping and more blood flowed after tape stripping. Conclusion : In our study, it was observed that temperature, transepidermal water loss, blood flow changed after tape stripping. But we thought lowered temperature was pathologic situation, more blood flow was to recover after injury. In traditional korean medicine, cold(寒) and imbalance of blood flow(血行) don't only make many skin diseases, but cold(寒) also obstructs blood flow. So we need to study how to warm cold(寒) and improve blood flow.

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폐수의 감압 암모니아 탈기에 관한 연구 (A Study on the Decompressed Ammonia Stripping from Ammonia Contained Wastewater)

  • 신대윤;오유경
    • 한국환경보건학회지
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    • 제27권1호
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    • pp.93-99
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    • 2001
  • This study aims at finding out pertinent reaction conditions for treating high concentration ammonia contained in N-chemical factory wastewater with decompressed ammonia stripping method that was designed. And it also tries to investigate adsorption capability of removed ammonia to soil. The results from experiments are as follows ; 1. The removal rate of N $H_3$-N of synthetic wastewater was under 85% at pH 10 with decompressed ammonia stripping method. The reaction time in pressure 360 mmHg at pH 11 and 12 was shorter than in 460 mmHg, and the removal rate of N $H_3$-N with decompressed ammonia stripping method at 9$0^{\circ}C$ was 11~15% higher than air stripping 2. The optimum conditions for decompressed ammonia stripping with synthetic sample were shown as pH 12, temperature 9$0^{\circ}C$, internal reaction pressure 460 mmHg and reaction time 50 minutes. These conditions were applied to treat the wastewater containing organic-N 290.5mg/$\ell$, N $H_3$-N 168.9mg/$\ell$, N $O_2$-N 23.2mg/$\ell$, N $O_3$-N 252.4mg/$\ell$, T-N 735mg/$\ell$. Organic-N turned out to be removed 60%, the removal rate of N $H_3$-N IS 94%, T-N is 50%. But N $O_2$-N and N $O_3$-N were increased with 7.8% and 14.9% respectively. 3. The CO $D_{Sr}$ removal rate in decompressed ammonia stripping reaction was 42% and S $O_4$$^{2-}$ was removed 8.2%. It was turned out caused with higher pH and thermolysis. 4. In soil adsorption of ammonia desorbed from the decompressed stripping process of wastewater, the recovery rate was 76% in wet soil.

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Nd:YAG 레이저를 이용한 의료기기용 마이크로 동축케이블의 실드선 탈피에 관한 연구 (A Study on Shield Wire Stripping of Micro Coaxial Cable for Medical Device Using Nd:YAG Laser)

  • 이정완;김정훈
    • 산업기술연구
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    • 제26권B호
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    • pp.35-41
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    • 2006
  • Recently, as ultrasonic medical devices are gradually developed, many of those requires smaller and more precision coaxial cables in probe. So, the use of micro coaxial cable becomes an efficient solution for ultrasonic machine. However, there are many difficulties in stripping micro coaxial cable by traditional mechanical process. In this paper, we use the Nd-YAG laser for the efficient stripping of conduct wire of cable. We propose a new method to strip the shield wire of micro coaxial cable. Through some experiments, we found that there is a new possibility in the proposed method. Also, in order to enhance the performance, we propose a preprocess of the cable before stripping.

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Stripping of Fe(III) from the Loaded Mixture of D2EHPA and TBP with Sulfuric Acid Containing Reducing Agents

  • Liu, Yang;Nam, Sang-Ho;Lee, Manseung
    • Bulletin of the Korean Chemical Society
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    • 제35권7호
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    • pp.2109-2113
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    • 2014
  • Solvent extraction of Fe(III) from chloride solution by using a mixture of D2EHPA (Di-(2-ethylhexyl)-phosphoric acid) and TBP (Tri-butyl phosphate) and the reductive stripping of Fe(III) from the loaded organic were investigated. Quantitative extraction of Fe(III) from the solution (Fe concentration = 90 g/L) was accomplished in two cross-current extraction stages by using the mixture of D2EHPA and TBP. In order to facilitate the stripping efficiency, a reductive stripping method was employed by using $H_2SO_3$ or $Na_2SO_3$ as a reducing agent. The addition of $H_2SO_4$ into reducing agents led to improvement in the stripping efficiency while high concentration acid would suppress it. Both of the mixtures of $H_2SO_4+H_2SO_3$ and $H_2SO_4+Na_2SO_3$ showed good efficiency for the stripping of Fe(III), while the latter was recommended as the stripping solution based on the economics and experimental condition.

Determination of Ultra Trace Levels of Copper in Whole Blood by Adsorptive Stripping Voltammetry

  • Attar, Tarik;Harek, Yahia;Larabi, Lahcen
    • 대한화학회지
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    • 제57권5호
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    • pp.568-573
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    • 2013
  • A selective and sensitive method for simultaneous determination of copper in blood by adsorptive differential pulse cathodic stripping voltammetry is presented. The procedure involves an adsorptive accumulation of Cu(II)-ETSC (4- ethyl-3-thiosemicarbazide) on a hanging mercury drop electrode, followed by a stripping voltammetry measurement of reduction current of adsorbed complex at about -715 mV. The optimum conditions for the analysis of copper (II) ion are : pH 10.3, concentration of 4-ethyl-3-thiosemicarbazide $3.25{\times}10^{-6}$ M and an accumulation potential of -100 mV. The peak current is proportional to the concentration of copper over the range 0.003-125 ng/mL with a detection limit of 0.001 ng/mL and an accumulation time of 60 s. Moreover, with the use of the proposed method, there is a considerable improvement in the detection limit, the linear dynamic range and the deposition time, compared with the methods of adsorptive stripping voltammetry for the determination of copper. The developed method was validated by analysis of whole blood certified reference materials.

치아인접면 삭제 및 연마에 따른 법랑질 표면의 변화에 관한 주사전자현미경적 연구 (A SCANNING ELECTRON MICROSCOPIC STUDY ON CHANGES OF ENAMEL SURFACE BY INTERPROXIMAL STRIPPING AND POLISHING)

  • 김영순;김광원
    • 대한치과교정학회지
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    • 제22권1호
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    • pp.123-131
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    • 1992
  • This study was done to evaluate the changes of enamel surface by interproximal stripping and recovery of it by polishing. The number of 34 1st premolars which had extracted for orthodontic treatment were selected as samples. Interproximal stripping was performed by hand with metal strip and strip placer (Dentaurum Co., Germany) and low speed handpiece with diamond disk (Superdiaflex, Germany). Polishing was performed by hand with plastic strip (3M Col) and low speed handpiece with whip-mix, DCPA (Dicalcium Phosphate, Anhydrous, $CaHPO_4$) powder and Sof-lex (3M Co. U.S.A.) polishing kit. Each groups were examined under the scanning electron microscope (JEOL Co., JSM-840A, Japan) and the following results were obtained: 1. The stripped group performed by metal strip and diamond disk altogether showed deep furrow on the enamel surface as wide as about $10{{\mu}m}$. 2. There could be seen more irregular scratched line in the group stripped by metal strip than that by diamond disk. 3. The polished group performed by plastic strip and DCPA powder showed slight smoothening of the edge of stripped furrow on the enamel surface without relation to the stripping method. 4. The polished group performed by Sof-lex progressive polishing kit could not avoid the formation of the furrows on the enamel surface according to the particle size without relation to the stripping method. 5. The polished group performed by the superfine polishing wheel, the final stage of Sof-lex polishing method showed shallow scratched line as wide as within about $2{{\mu}m}$ on the enamel surface without relation to the stripping method. 6. The interproximal stripped enamel surface could not recover its original surface texture by any kind of polishing methods.

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링레이저 자이로의 몸체진동 검출센서를 이용한 dither-stripping 연구 (A study on the dither-stripping with dither motion sensor of a ring laser gyroscope)

  • 심규민;임후장
    • 한국항공우주학회지
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    • 제31권5호
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    • pp.63-71
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    • 2003
  • 본 논문에서는 몸체진동형 링레이저 자이로에서 몸체진동을 검출하기 위한 각속도 센서 출력을 V-F 변환하여 링레이저 출력에서 몸체진동에 의한 출력을 제거하는 dither-stripping 방법에 대하여 논의하였다. Dither-stripping에서는 V-F 출력펄스와 링레이저 출력펄스간의 환산계수를 산출하는 방법과 V-F 출력펄스의 offset를 보정해주는 방법이 중요하다. 각속도 센서의 출력을 V-F 변환하여 dither-stripping하는 경우에는 offset을 보정하는 과정에서 몸체진동의 진폭잡음에 의한 자이로 출력의 오차가 크게 발생한다. 우리는 V-F 출력펄스를 미분하여 offset을 제거하는 방법을 고안하였다. 이를 위해서는 각속도 센서의 출력을 90deg 위상 이동시켜서 각도신호를 만들고 V-F 변환해야 하며 링레이저 출력의 위상도 샘플링의 반주기만큼 이동시켜야 한다. 그리고 두 펄스간의 환산계수는 분산을 이용하여 산출하였다. 이러한 각도신호 미분방식의 dither-stripping에 의하여 개선된 결과를 얻을 수 있었다.