• Composites Research
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• v.28 no.6
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• pp.361-365
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• 2015

The influence of MWCNTs on fracture toughness properties of MWCNTs/Nickel-Pitch Fibers/epoxy composites (MWCNTs/Ni-PFs/epoxy) was investigated according to MWCNTs content. Nickel-Pitch-based carbon fibers (Ni-PFs) were prepared by electroless nickel-plating. The surface properties of Ni-PFs were determined by scanning electron microscopy (SEM) and X-ray photoelectron spectrometry (XPS). The fracture toughness of MWCNTs/Ni-PFs/epoxy was assessed by critical stress intensity factor ($K_{IC}$) and critical strain energy release rate ($G_{IC}$). From the results, it was found that the fracture toughness properties of MWCNTs/Ni-PFs/epoxy were enhanced with increasing MWCNTs content, whereas the value decreased above 5 wt.%. MWCNTs content. This was probably considered that the MWCNTs entangled with each other in epoxy due to an excess of MWCNTs.

• Macromolecular Research
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• v.17 no.8
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• pp.585-590
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• 2009

The cure behaviors, dielectric characteristics and fracture toughness of diglycidylether of bisphenol-A (DGEBA)/poly(ethylene terephthalate) (PET) blend system were investigated. The degree of conversion for the DGEBA/PET blend system was measured using Fourier transform infrared (FTIR) spectroscopy. The cure kinetics were investigated by measuring the cure activation energies ($E_a$) with dynamic differential scanning calorimetry (DSC). The dielectric characteristic was examined by dielectric analysis (DEA). The mechanical properties were investigated by measuring the critical stress intensity factor ($K_{IC}$), critical strain energy release rate ($G_{IC}$), and impact strength test. As a result, DGEBAIPET was successfully blended. The Ea of the blend system was increased with increasing PET content to a maximum at 10 phr PET. The dielectric constant was decreased with increasing PET content. The mechanical properties of the blend system were also superior to those of the neat DGEBA. These results were attributed to the increased cross-linking density of the blend system, resulting from the interaction between the epoxy group of DGEBA and the carboxyl group of PET.

• Structural Engineering and Mechanics
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• v.10 no.2
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• pp.139-156
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• 2000

This paper concerns the development of a computational model for the damage evolution of engineering materials under dynamic loading. Two models describing the anisotropic damage evolution of a material are presented; the first is based on a power function of the effective equivalent stress and the second on the damage strain energy release rate. The methods for computing the damage accumulated in structural components and their implementation in a finite element programme are presented together with some numerical results. The dynamic response of a damaged structural component and the dynamic behaviour of a damaged material have been studied numerically. This study shows that the frequency spectrum of a damaged structure is down-shifted, while the damping ratio of damaged materials becomes higher, the amplitude of the response significantly increases and the resonance ensuing from the damage growth still occurs in a damaged structure.

• Composites Research
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• v.13 no.3
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• pp.48-57
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• 2000

Fracture analysis of coating cracking on a substrate system described in a companion paper was applied and verified by four-point bending tests. The multiple cracking of coating was predicted using a fracture mechanics approach. The strain energy release rate (G) due to the formation of a new crack in a coating was obtained. A crack density vs. strain data of metallic and polymeric substrate was used to get the in-situ fracture toughness of coating with respect to various baking time and temperature. The $G_c$ was decreased as the baking temperature and time was increased. This paper gave insight about usefulness of four-point bending test for fracture toughness evaluation of coating and it gave a new method for in-situ coating toughness.

• Structural Engineering and Mechanics
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• v.64 no.4
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• pp.487-494
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• 2017

The present paper deals with a theoretical study of delamination fracture in the Crack Lap Shear (CLS) functionally graded beam configuration. The basic purpose is to analyze the fracture with taking into account the material non-linearity. The mechanical behavior of CLS was described by using a non-linear stress-strain relation. It was assumed that the material is functionally graded along the beam height. The fracture was analyzed by applying the J-integral approach. The curvature and neutral axis coordinate of CLS beam were derived in order to solve analytically the J-integral. The non-linear solution of J-integral obtained was verified by analyzing the strain energy release rate with considering material non-linearity. The effects of material gradient, crack location along the beam height and material non-linearity on fracture behavior were evaluated. The J-integral non-linear solution derived is very suitable for parametric studies of longitudinal fracture in the CLS beam. The results obtained can be used to optimize the functionally graded beam structure with respect to the fracture performance. The analytical approach developed in the present paper contributes for the understanding of delamination fracture in functionally graded beams exhibiting material non-linearity.

• Journal of the Korean Society of Safety
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• v.34 no.6
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• pp.1-6
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• 2019

Carbon fiber has excellent specific strength, corrosion resistance and heat resistance. And p-Aramid fiber has high toughness and heat resistance and high elasticity, and is used in various fields such as industrial protective materials, bulletproof helmets and vests, as well as industrial fields. However, carbon fiber is relatively expensive, and is susceptible to brittle fracture behavior due to its low fracture strain. On the other hand, the aramid fiber tends to decrease in elastic modulus and strength when applied to the epoxy matrix, but it is inexpensive and has higher elongation and fracture toughness than carbon fiber. Thus the twill hybrid carbonaramid fiber reinforced composite laminate composite was investigated for a delamination fracture toughness under Mode I loading by 2 kinds of MBT and MCC deduction. The specimen was fabricated with 20 hybrid fabric plies. The initial crack was made by inserting the teflon tape in the center plane with a₀/W=0.5 length. The results show that SERR(Strain Energy Release Rate) as the critical and stable delamination fracture toughness were 0.09 kJ/㎡, 0.386 kJ/㎡ by MBT deduction, and 0.192 kJ/㎡, 0.67 kJ/㎡ by MCC deduction, respectively.

• Coupled systems mechanics
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• v.6 no.1
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• pp.97-111
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• 2017

The present paper reports an analytical study of delamination fracture in the Mixed Mode Flexure (MMF) functionally graded beam with considering the material non-linearity. The mechanical behavior of MMF beam is modeled by using a non-linear stress-strain relation. It is assumed that the material is functionally graded along the beam height. Fracture behavior is analyzed by the J-integral approach. Non-linear analytical solution is derived of the J-integral for a delamination located arbitrary along the beam height. The J-integral solution derived is verified by analyzing the strain energy release rate with considering the non-linear material behavior. The effects of material gradient, crack location along the beam height and material non-linearity on the fracture are evaluated. It is found that the J-integral value decreases with increasing the upper crack arm thickness. Concerning the influence of material gradient on the non-linear fracture, the analysis reveals that the J-integral value decreases with increasing the ratio of modulus of elasticity in the lower and upper edge of the beam. It is found also that non-linear material behavior leads to increase of the J-integral value. The present study contributes for the understanding of fracture in functionally graded beams that exhibit material non-linearity.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2002.10a
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• pp.265-268
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• 2002

In this work, the blend system of epoxy and PMR-15 polyimide is investigated in terms of the cure behaviors and thermal stabilities. The cure behaviors are studied in DSC measurements and thermal stabilities are also carried out by TGA analysis. DDM (4, 4'-diamino diphenyl methane) is used as curing agent for EP and the content of PMR-15 is varied within 0, 5, 10, 35, and 20 phr to neat EP. As a result, the cure activation energy ($E_a$) is increased at 10 phr of PMR-15, compared with that of neat EP. From the TGA results of EP/PMR-15 blend system, the thermal stabilities based in the initial decomposed temperature (IDT) and integral procedural decomposition temperature (IPDT) are increased with increasing the PMR-15 content. The fracture toughness, measured in the context of critical stress intensity factor ($K_{IC}$) and critical strain energy release rate ($G_{IC}$), shows a similar behavior with $E_a$. This result is probably due to the crosslinking developed by the interactions between intermolecules in the polymer chains.

• Polymer(Korea)
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• v.37 no.1
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• pp.61-65
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• 2013

In this work, the anodic oxidation of carbon fibers was carried out to enhance the mechanical interfacial properties of carbon fibers-reinforced epoxy matrix composites. The surface characteristics of the carbon fibers were studied by FTIR, X-ray photoelectron spectroscopy (XPS), and scanning electron microscopy (SEM). Also, the mechanical interfacial properties of the composites were studied with interlaminar shear strength (ILSS), critical stress intensity factor ($K_{IC}$), and critical strain energy release rate ($G_{IC}$). The anodic oxidation led to a significant change in the surface characteristics of the carbon fibers. The anodic oxidation of carbon fiber improved the mechanical interfacial properties, such as ILSS, $K_{IC}$, and $G_{IC}$ of the composites. The mechanical interfacial properties of the composites anodized at 20% sulfuric/nitric (3/1) were the highest values among the anodized carbon fibers. These results were attributed to the increase of the degree of adhesion at interfaces between the carbon fibers and the matrix resins in the composite systems.

• Geomechanics and Engineering
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• v.17 no.4
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• pp.375-383
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• 2019

In underground retreating longwall coal mining, hard roof collapse is one of the most challenging safety problems for mined-out areas. Identifying precursors for hard roof collapse is of great importance for the development of warning systems related to collapse geohazards and ground control. In this case study, the Xinhe mine was chosen because it is a standard mine and the minable coal seam usually lies beneath hard strata. Real-time monitoring of hard roof collapse was performed in longwall face 5301 of the Xinhe mine using support resistance and microseismic (MS) monitoring; five hard roof collapse cases were identified. To reveal the characteristics of MS activity during hard roof collapse development and to identify its precursors, the change in MS parameters, such as MS event rate, energy release, bursting strain energy, b value and the relationships with hard roof collapse, were studied. This research indicates that some MS parameters showed irregularity before hard roof collapse. For the Xinhe coalmine, a substantial decrease in b value and a rapid increase in MS event rate were reliable hard roof collapse precursors. It is suggested that the b value has the highest predictive sensitivity, and the MS event rate has the second highest.