• 제목/요약/키워드: Stirring speed

검색결과 148건 처리시간 0.158초

Recovery of Golden yellow and Cibacron LSG dyes from aqueous solution by bulk liquid membrane technique

  • Muthuraman, G;Ali, P. Jahfar
    • Membrane and Water Treatment
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    • 제3권4호
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    • pp.243-252
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    • 2012
  • Tri-n-butyl phosphate (TBP) was used as carrier for the transport of Golden yellow and Cibacron LSG dyes through a hexane bulk liquid membrane. The transport efficiency of dyes by TBP was investigated under various experimental conditions such as pH of the feed phase (dyes solution), concentration of the receiving phase (NaOH solution), concentration of TBP in membrane, rate of stirring, effect of transport time, type of solvent, dye concentration in feed phase, effect of temperature.. The maximum transport dyes occurs at ratio of 1:1 TBP-hexane At pH 3.0 0.1 (feed phase) the transport dyes decreased. At high stirring speed (300 rpm) the dyes transport from the feed phase to the strip phase was completed within 60 minutes at $27^{\circ}C$. Under optimum conditions: Feed phase 100 mg/L dyes solution at pH 1.0 0.1, receiving phase 0.1 mol/L NaOH solution, membrane phase 1:1 TBP-hexane , Stirring speed 300 rpm and temperature $27^{\circ}C$, the proposed liquid membrane was applied to recover the textile effluent.

Rheo-Compocasting에 의한 $SiC_p$/6063 Al합금의 복합조직 (Composite Structures of $SiC_p$/6063 Aluminum Alloy by Rheo-Compocasting.)

  • 최정철
    • 한국주조공학회지
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    • 제10권4호
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    • pp.309-315
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    • 1990
  • Aluminum alloy matrix composites reinforced by SiC particles were prepared by rheocompocasting, a process which consists of the incoporation and distribution of reinforcement by stirring within a semi-solid alloy. When the volume fraction of SiCp and stirring speed were fixed, the dispersion of SiCp in Al-matrix alloy depended on stirring time and solid volume fraction in slurry. The results were as follows : 1) As a dispersed SiCp during stirring at $647^{\circ}C$ in 6063-Al alloy, SiC was better dispersed than that other temperature, where solid volume fraction was 43% in slurry. 2) When increased solid fraction in slurry, rate of dispersing SiC increased during stirring and porosities decreased in matrix alloy after casting. 3) Inspite of stirring with 800rpm, since solid particles of matrix alloy in slurry joined each other and occured joining growth, so that SiC was not dispersed into solid particle.

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Effect of Methylcellulose on the Nylon Microcapsules Containing Acetaminophen

  • Park, Soon-Chull;Lee, Min-Hwa
    • Journal of Pharmaceutical Investigation
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    • 제13권3호
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    • pp.89-99
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    • 1983
  • Nylon microcapsules containing acetaminophen could be obtained by interfacial polymerization between sebacoyl chloride and 1, 6-hexamethylenediamine. Methylcellulose affected the micromeritic properties and dissolution characteristics of microcapsules. The particle size distribution was affected by the stirring speed and viscosity grade of methylcellulose. The surface observed by the scanning electron microscopy was affected by the methylcellulose. Nylon microcapsules produced in above method containing acetaminophen exhibited the retarded dissolution in comparison with uncoated acetaminophen. Release of acetaminophen from microcapsules decreased with decreasing pH of medium and with increasing the viscosity grade of methylcellulose and stirring speed.

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전자교반에 의한 Cu-0.5wt%Zr 합금의 반응고 조직제어에 관한 연구 (The Effect of Electromagnetic Stirring on the Semi-Solid Microstructure of Cu-0.15wt%Zr Alloy)

  • 임성철;이흥복;김경훈;권혁천;윤의박
    • 한국주조공학회지
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    • 제26권1호
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    • pp.40-45
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    • 2006
  • Most of the work reported concerned the semi-solid processing of low melting point alloys, and in particular light alloys of aluminum and magnesium. The purpose of this paper is to develop a semi-solid microstructure of Cu alloys using electromagnetic stirring applicable for squirrel cage rotor of induction motor. The size of primary solid particle and the degree of sphericity as a function of the variation in cooling rate, stirring speed, and holding time were observed. By applying electromagnetic stirring, primary solid particles became finer and rounder relative to as-cast sample. As the input frequency increased from 30 to 40 Hz, particle size decreased. The size of primary solid particle was found to be decreased with increasing cooling rate. Also, it decreased with stirring up to 3 minutes but increased above that point. The degree of sphericity became closer to be 1 with hold time. Semi-solid microstructure of Cu alloys, one of the high melting point alloys, could be controlled by electromagnetic stirring.

Progressive Freezing에 의한 동결 농축법에 있어서의 농축효과에 미치는 동결조건의 영향 (Effects of Freezing Conditions on the Concentration-Efficiency in the Progressive Freeze-Concentration)

  • 배승권
    • 한국식품영양과학회지
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    • 제24권6호
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    • pp.984-989
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    • 1995
  • The concentration-efficiencyh of blue dextran solution in the progressive freeze-concentration was related to the freezing conditions such as the freezing speed and the stirring speed in the solution phase. From the theoreticla balance equation of heat and mass transfer at freezing front, the relationship between the freezing conditions and the ice structure at freezing front was drived. A high freeze-concentration efficiency was obtained under the operating conditions represented by a low speed of freezing and a high speed of stirring. The operating conditions were related to a smooth solid-liquid interface and these results were well explained by the theoretical equation. Effect of the solute component size on the concentration efficiency in the progressive freezeconcentration was also tested. The concentration efficiency of latex particles showed a lower value than that of blue dextran, however, its difference was insignificant.

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Al6061-T6의 마찰교반용접 시 회전 Tool Pin 형상에 따른 기계적 특성 평가 (Mechanical Characteristic Evaluation by Spin Tool of Different Pin Shapes in Friction Stir Welding Al6061-T6)

  • 임병철;김대환;박상흡
    • 한국생산제조학회지
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    • 제23권4호
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    • pp.345-349
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    • 2014
  • In this study, an age-hardened 6061-T6 alloy sheet was used, which is commonly utilized for auto parts. The junction strength characteristics in relation to the stirring speed and welding speed were studied in accordance with the friction stir welding rotation of the tool pin. Micro hardness measurements of A type and B type pins, for a welding speed of 400 mm/min and a tool rotational speed 3000 rpm, were obtained as Hv104 and Hv111, respectively. For a welding speed of 200 mm/min and a tool rotational speed of 2000 rpm, we obtained Hv48 and Hv50 for A and B type pins, respectively. Microstructure observation showed that the stirring portion was fine and uniform, which occurred because of its plastic deformation. In the thermomechanically affected zone, partial recrystallization was present because of the plastic deformation. The crystal grains in the heat affected zone were coarsened due to the heat generated by friction stir welding.

폴리에스테르 섬유의 호발과 정련에서 초음파진동 효과 (The Effect of Ultrasonic Vibration in Desizing and Scouring of Polyester Fabrics)

  • 박영태;최호상;이광수
    • 한국염색가공학회지
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    • 제11권5호
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    • pp.1-6
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    • 1999
  • This study was carried out to investigate the effect of a scouring machine including an ultrasonic system on desizing and scouring polyester fabrics. The ultrasonic frequency of the improved machine showed up at 28.882 kHz. Frequency amplitude increased with the current and the bath temperature, and then showed a constant level. Scouring effect of the ultrasonic machine was better than that of the conventional scouring machine using the mechanical stirring. The ultrasonic machine showed the optimum scouring effect at $50^\circ{C}$ of bath temperature and 10 min. of operation time, as compared to the conventional machine that required operating conditions of high temperature at $90^\circ{C}$, stirring speed at 40 rpm, and stirring time for 15 min..

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Effects of Stirring and Addition of Chemical Compounds on Glycerolysis of Triglyceride in Reversed Micelles

  • Chang, Pahn-Shick
    • Journal of Microbiology and Biotechnology
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    • 제1권3호
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    • pp.197-201
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    • 1991
  • Glycerolysis of triolein by lipase from Chromobacterium viscosum lipase was studied batchwise in AOT-isooctane reversed micelles. The reaction mixture was extracted with chloroform and the content of triolein, 1, 2-diolein, 1, 3-diolein, 1-monoolein, and free fatty acid in the condensed chloroform solution was determined using high performance liquid chromatography (HPLC). The effect of agitation speed on the initial rate of conversion was examined. As the speed of agitation increased up to 700 rpm, the reaction rate increased. However, above 700 rpm, the rate approached maximum and did not increase that much. The glycerolysis activity and the stability of the enzyme were affected by stirring and addition of histidine or copper. Addition of histidine and copper increased the rates of glycerolysis but they are detrimental to the operational stability in reversed micelles.

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산업폐수중 유화액막에 의한 크롬(VI)의 분리 (Separation of Chromium(VI) Ion in Industrial Waste Water throunh Liquid Surfactant Membrane)

  • 초민승;강안수;우인성;이영순
    • 한국안전학회지
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    • 제4권1호
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    • pp.15-24
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    • 1989
  • The transport of Chromium(Vl) ion from waste water throughl the liquid surfactant membrane containing tri-n-octylamine as a carrier, was analyzed by a slab model and was investigated through experiments. For the experiment of membrane stability, concentrations of surfactant and liquid parafnn oil were analyzed. Extraction euperiments were carried out to observe the effect of system variables, such as stirring speed, concentration of carrier, and NaOH in internal aqueous phase, and concentrations of H$_2$SO$_4$and initial chromium(VI) ion in external aqueous phase at $25^{\circ}C$. It is concluded that the most stable formation of liquid membrane emulsion was obtained when surfactant concentration is above 3 wt. % and liquid parafnn oil concentration is 50 vol. %. The transport of chromium(VI) ion in bacth extractor increased with increasing carrier concentration, the volume ratio of emulsion to external aqueous phases, and initial concentration of chromium(VI) ion under the optimum stirring speed of chromium(VI) ion below 2 ppm. The theoretical equation on the transport of chromium(Vl) ion agreed well with the experimental results.

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반용융 알루미늄재료의 단조공정조건이 기계적 성질에 미치는 영향 (The effect of forging process conditions of semi-solid aluminum material on mechanical properties)

  • 강충길;강동우
    • 대한기계학회논문집A
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    • 제21권9호
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    • pp.1400-1413
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    • 1997
  • Semi-solid forging(SSF) process of A356 aluminium alloy has been studied to assess the effect of process variables on the component integrity. Semi-solid material(SSM) was fabricated by mechanical and electro-magnetic stirring process. The fabricated SSM by using mechanical stirring process has been carried out on cooling rate of 0.022.deg. C/sec 0.0094.deg. C/sec and stirring speed n=600, 1000 rpm, respectively. The fabricated SSM by using electro-magnetic stirring process is supplied by Pechiney. The holding time and temperature in the semi-solid state before forging also affects the globular microstructure of alloy. Therefore, the influence of these two parameters is discussed in terms of the microstructure of alloy. The SSF process has been conducted with three different die temperatures($T_{die}$=250.deg. C, 300.deg. C, 350.deg. C) and two kinds of gate types(straight gate and orifice gate). This paper is to investigate the influence of gate shapes of die on filling phenomena in SSF process more deeply. The mechanical properties of forged components were also investigated for variation of process conditions such as die temperature, gate shape and SSM.