• Title/Summary/Keyword: Stirring rate

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Factors Affecting the Characteristics of Melamine Resin Microcapsules Containing Fragrant Oils

  • Hwang, Jun-Seok;Kim, Jin-Nam;Wee, Young-Jung;Jang, Hong-Gi;Kim, Sun-Ho;Ryu, Hwa-Won
    • Biotechnology and Bioprocess Engineering:BBE
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    • v.11 no.5
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    • pp.391-395
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    • 2006
  • Microcapsules containing fragrant oils as a core material were prepared by in situ polymerization, using melamine-formaldehyde prepolymer as the wall material. The several parameters, such as stirring times, stirring rates, emulsifier types, emulsifier concentrations, and the viscosity of the core materials, affect the characteristics of the microcapsules. These parameters were investigated by the analyses of microcapsule size, particle size distribution, and morphology. The average microcapsule size decreased with an increase in stirring time, stirring rate, emulsifier concentration, and viscosity of the core material. It was also found that poly(vinyl alcohol) as a protective colloid could enhance the stability of the melamine-formaldehyde microcapsules.

Mechanical Properties of SiC Particulate Reinforced Mg Matrix Composites Fabricated by Melt Stirring Method (용탕교반법에 의한 SiC 입자강화 Mg기 복합재료의 기계적 특성)

  • Lim, Suk-Won;Choh, Takao;Park, Young-Jin
    • Journal of Korea Foundry Society
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    • v.13 no.5
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    • pp.441-449
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    • 1993
  • SiC particulate reinforced magnesium matrix composites were fabricated by melt stirring method. The effet of several factors on mechanical properties and the efficiency of melt stirring method from the viewpoint of these properties were investigated. The tensile strength increased and the elongation decreased with decrease of the particle size or the increase of the paticulate volume fraction for pure magnesium matrix and Mg-5%Zn alloy matrix composites. A longer stirring time improved the tensile strength of these composites. The tensile strength of Mg-5%Ca alloy matrix composites which shows no uniform paticulate distribution was a little lower than that of matrix alloy. Rapid solidification rate is preferred for the improved tensile strength of these composites. The pure magnesium matrix and Mg-5%Zn alloy matrix composites have tensile strength of about 400MPa. This value agrees with the tensile strength of some magnesium matrix composites fabricated by liquid infiltration method or powder metallurgy method at the same volume fraction of reinforcements of whisker or particle. Therefore, the melt stirring method which has the advantages of simple process is considered to be efficient in fabricating magnesium matrix composites.

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Investigation of Reinforced Distribution in Fabrication Process of Metal Matrix Composites by Combined Stirring Process (복합교반법에 의한 금속복합재료의 제조공정에 따른 강화재의 분산성 검토)

  • 이동건;강충길
    • Composites Research
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    • v.14 no.5
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    • pp.1-11
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    • 2001
  • The particulates reinforced metal matrix composites(PMMC) have a number of interesting mechanical properties. including high strength and good resistance to wear at high temperature and low thermal expansion. The equipment structure to obtain the homogeneous distribution in composites are proposed for the continuous pouring of reinforcement at the desired temperature. The particulates reinforced metal matrix composites(A357/SiCp) were fabricated by the process of the combined stirring method with the various fabrication process. The combined stirring method to niform distribution of particle is consisted of two stirring force both electro-magnetic stirring generated from induction heating and mechanical stirring with graphite stirrer. PMMC billets were fabricated with the volume fractions ranged from 0% to 20% and particle sizes ranged from 14${\mu}{\textrm}{m}$ to 25${\mu}{\textrm}{m}$. It is important to cont the size of primary $\alpha$-Al solid particles because it could become the cause of the particle pushing or capture phenomena from the fact that secondary dendrite arm spacing size depends on the cooling rate during the solidification in hypoeutectic Al-Si alloy. Therefore, the effect of primary $\alpha$-Al on the reinforcement distribution in matrix alloys has been investigated. The microstructure of PMMC fabracated with various volume fractions(0%, 10%, and 20%) and particle size were observed.

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Effects of Stirring and Addition of Chemical Compounds on Glycerolysis of Triglyceride in Reversed Micelles

  • Chang, Pahn-Shick
    • Journal of Microbiology and Biotechnology
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    • v.1 no.3
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    • pp.197-201
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    • 1991
  • Glycerolysis of triolein by lipase from Chromobacterium viscosum lipase was studied batchwise in AOT-isooctane reversed micelles. The reaction mixture was extracted with chloroform and the content of triolein, 1, 2-diolein, 1, 3-diolein, 1-monoolein, and free fatty acid in the condensed chloroform solution was determined using high performance liquid chromatography (HPLC). The effect of agitation speed on the initial rate of conversion was examined. As the speed of agitation increased up to 700 rpm, the reaction rate increased. However, above 700 rpm, the rate approached maximum and did not increase that much. The glycerolysis activity and the stability of the enzyme were affected by stirring and addition of histidine or copper. Addition of histidine and copper increased the rates of glycerolysis but they are detrimental to the operational stability in reversed micelles.

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The effect of the primary particle of the A356 Alloy according to different wall thickness of the sleeve of die-casting by electromagnetic stirrer (전자교반시스템에서 Sleeve 의 크기가 유동특성과 미세조직에 미치는 영향)

  • 고재홍;서판기;강충길
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2004.10a
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    • pp.660-663
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    • 2004
  • Recently in the automotive industries, light and high quality material is strongly required because of emissions regulation issues. In the electromagnetic stirring process, it has many merits that are the exact control ability about material processing and a good point of the protection of environment. In this paper, the morphology of the change of primary Al phase in A356 alloy by electro magnetic stirrer was investigated to obtain the globular structure. The parameters are the current, stirring time, pouring temperature and cooling rate of different wall thickness; 5mm, 15mm, 25mm respectively. By proper selection of the processing parameters, globular primary particles can be obtained by electromagnetic stirrer.

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Continuous Combined Process for Homogeneous Dispersion of Ceramic Particle and Aluminum Materials (세라믹 입자/알루미늄 소재의 연속복합 균일분산)

  • 이동건;이승후;강충길
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2001.04a
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    • pp.381-384
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    • 2001
  • The combined stirring method to uniform distribution of particle is consisted of two strring force both electro-magnetic stirring generated from induction heating and mechanical stirring with graphite stirrer. PMMC billets were fabricated with the volume fractions ranged from 0% to 20% and particle sizes ranged from 14$\mu\textrm{m}$ to 25$\mu\textrm{m}$. It is important to control the size of primary ${\alpha}$-AI solid particles because it could become the cause of the particle pushing or capture phenomena from the fact that secondary dendrite arm spacing size depends on the cooling rate during the solidification in hypoeutectic AI-Si alloy.

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A Study of Rheology Properties of AM50A Magnesium Alloy (AM50A 마그네슘합금의 레오로지 특성에 관한 연구)

  • Han S.H.;Lee J.H.;Kang C.G.
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2006.05a
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    • pp.431-432
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    • 2006
  • In this study, the effect of the temperature of magnesium slurry was investigated by mechanical stirring method. The evaluations of rheological behavior of AM50A magnesium alloy were measuring of viscosity and microstructures in the semisolid state. The apparent viscosity was investigated at continuous cooling rate using a concentric cylinder viscometer. Measurement of viscosity measures torque that act to stirrer rotating in slurry doing continuous cooling using torque-meter and expressed by POWER-LAW. Microstructures were observed after mechanical stirring that enforce time at steady state temperature of solid fraction.

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The Effect of Electromagnetic Stirring on the Microstructure of A356 Al Alloy by the Continuous Casting Process (A356 합금의 연속주조시 전자기 교반에 따른 미세조직 변화)

  • Kim, Won-Bae;Kwon, Tae-Woo;Kim, Jong-Chul;Park, Tae-Ho;Ye, Byung-Joon
    • Journal of Korea Foundry Society
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    • v.25 no.4
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    • pp.156-160
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    • 2005
  • There are many factors that influence solidification behavior during continuous casting, e.g. include superheat, casting speed, cooling rate and holding time. However, when melt is stirred by electromagnetic force, there would be some changes in its solidification behavior compared to that of the ordinary casting process. In this study, the billets of A356 alloy with a diameter of 3 inch were fabricated with electromagnetic stirring under various conditions of superheat, casting speed and input voltage of electro magnetic stirring (EMS) device. The microstructure was also investigated under the various casting conditions and electromagnetic input voltages. When increase in input voltage, the microstructure was changed from dendritic to rosette type and finally to spheroidal. With pouring temperature, casting speed and electromagnetic input voltage were $650^{\circ}C$, 100 mm/min and 140 V, respectively, the billet with a diameter of 3 inch, which has a uniform dispersed spheroidal particles in the whole area of billet except for the surface area, was manufactured.

The effect of forging process conditions of semi-solid aluminum material on mechanical properties (반용융 알루미늄재료의 단조공정조건이 기계적 성질에 미치는 영향)

  • Gang, Chung-Gil;Gang, Dong-U
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.21 no.9
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    • pp.1400-1413
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    • 1997
  • Semi-solid forging(SSF) process of A356 aluminium alloy has been studied to assess the effect of process variables on the component integrity. Semi-solid material(SSM) was fabricated by mechanical and electro-magnetic stirring process. The fabricated SSM by using mechanical stirring process has been carried out on cooling rate of 0.022.deg. C/sec 0.0094.deg. C/sec and stirring speed n=600, 1000 rpm, respectively. The fabricated SSM by using electro-magnetic stirring process is supplied by Pechiney. The holding time and temperature in the semi-solid state before forging also affects the globular microstructure of alloy. Therefore, the influence of these two parameters is discussed in terms of the microstructure of alloy. The SSF process has been conducted with three different die temperatures($T_{die}$=250.deg. C, 300.deg. C, 350.deg. C) and two kinds of gate types(straight gate and orifice gate). This paper is to investigate the influence of gate shapes of die on filling phenomena in SSF process more deeply. The mechanical properties of forged components were also investigated for variation of process conditions such as die temperature, gate shape and SSM.

Recovery of Golden yellow and Cibacron LSG dyes from aqueous solution by bulk liquid membrane technique

  • Muthuraman, G;Ali, P. Jahfar
    • Membrane and Water Treatment
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    • v.3 no.4
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    • pp.243-252
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    • 2012
  • Tri-n-butyl phosphate (TBP) was used as carrier for the transport of Golden yellow and Cibacron LSG dyes through a hexane bulk liquid membrane. The transport efficiency of dyes by TBP was investigated under various experimental conditions such as pH of the feed phase (dyes solution), concentration of the receiving phase (NaOH solution), concentration of TBP in membrane, rate of stirring, effect of transport time, type of solvent, dye concentration in feed phase, effect of temperature.. The maximum transport dyes occurs at ratio of 1:1 TBP-hexane At pH 3.0 0.1 (feed phase) the transport dyes decreased. At high stirring speed (300 rpm) the dyes transport from the feed phase to the strip phase was completed within 60 minutes at $27^{\circ}C$. Under optimum conditions: Feed phase 100 mg/L dyes solution at pH 1.0 0.1, receiving phase 0.1 mol/L NaOH solution, membrane phase 1:1 TBP-hexane , Stirring speed 300 rpm and temperature $27^{\circ}C$, the proposed liquid membrane was applied to recover the textile effluent.