• Title/Summary/Keyword: Stirring intensity

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Microchip-based cell aggregometer using stirring-disaggregation mechanism

  • Shin, Se-Hyun;Yang, Yi-Jie;Suh, Jang-Soo
    • Korea-Australia Rheology Journal
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    • v.19 no.3
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    • pp.109-115
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    • 2007
  • A new microchip-based aggregometer that uses a stirring-aided disaggregation mechanism in a microchip was developed to measure red blood cell (RBC) aggregation in blood and RBC suspensions. Conventional methods of RBC disaggregation, such as the rotational Couette system, were replaced with a newly designed stirring-induced disaggregation mechanism. Using a stirrer in a microchip, the aggregated RBCs stored in a microchip can be easily disaggregated. With an abrupt halt of the stirring, the backscattered light intensity can be measured in a microchip with respect to time. The time recording of the backscattered light intensity (syllectogram) shows an exponential decreasing curve representing the RBC aggregation. By analyzing the syllectogram, aggregation indices such as AI and M were determined. The results showed excellent agreement with LORCA. The essential feature of this design is the incorporation of a disposable microchip and the stirring-induced disaggregation mechanism.

Characteristics of Friction Stir Lap Welded A5052 with Probe Length (프루브 길이에 따른 A5052 겹치기 마찰교반접합 특성)

  • Ko, Young-Bong;Kang, Chae-Won;Choi, Jun-Woong;Park, Kyeung-Chae
    • Journal of the Korean institute of surface engineering
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    • v.42 no.6
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    • pp.294-300
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    • 2009
  • The Friction Stir Welding (FSW) has mainly been used for making butt joints in Al alloys. The development of Friction Stir Lap Welding (FSLW) would expand the number of applications. In this study, for effective application on thin aluminum alloy lap joint, non-heat treatment A5052 alloys were joined by FSLW with the length of probe 2.3 mm and 3.0 mm. Investigating the characteristics of joint area showed the results were as below ; When the length of probe was 2.3 mm, good joint area was formed at all welding condition except for 600 rpm-700 mm/min. In the case of 3.0 mm probe length, there was formed good joint area without defects at 1500 rpm-100 mm/min. The width of joint area, position and size of defects were very important factors for FSLW, due to heat input and stirring intensity.

A Study on Photo-Luminescence Spectrum Properties of ZnS:Mn QD Prepared by Wet-Process (습식공정을 이용한 ZnS:Mn2+계 QD의 합성 조건에 따른 광 특성 변화 연구)

  • Cha, Ji Min;Lee, Yoon Ji;Moon, Seong Cheol;Lee, Seong Eui
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.30 no.1
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    • pp.42-47
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    • 2017
  • In this study, the physical and optical properties of $ZnS:Mn^{2+}$ Quantum Dot prepared by wet-process condition with Mn/Zn ratio was valuated. The powder characteristics and optical behavior were investigated through XRD, TEM and Photo spectrometer exicted by various UV light source. We found the main peak of ZnS (111) was shifted by 0.8 degree to low angle position with increasing stirring energy from 200 RPM to 600 RPM, which is thought to be the increase of lattice defects during wet process. The photo luminescence at 600 RPM shows also higher blue intensity which is well correlated with XRD results. With increasing Mn/Zn ratio, the PL intensity become higher and shifed by 8.5nm to right side, by the increment of substitutional $Mn^{2+}$ ions.

3-D Dynamic Visualization by Stereoscopic PIV

  • LEE Young-Ho
    • 한국가시화정보학회:학술대회논문집
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    • 2004.12a
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    • pp.15-23
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    • 2004
  • The present study is aimed to achieve dynamic visualization from the in-house 3-D stereoscopic PIV to represent quantitative flow information such as time-resolved 3-D velocity distribution, vorticity, turbulent intensity or Reynolds stresses and so on. One of the application of the present study is Leading edge extension(LEX) flow appearing on modern delta wing aircraft. The other is mixing flow in stirring tank used in industry field. LEX in a highly swept shape applied to a delta wing features the modern air-fighters. The LEX vortices generated upon the upper surface of the wing at high angle of attack enhance the lift force of the delta wing by way of increased negative suction pressure over the surfaces. The present method resolves also the complicated flow patterns of two type impellers rotating in stirring vessel. Flow quantities such as three velocity vector components, vorticity and other flow information can be easily visualized via the 3D time-resolved post-processing visualization. And it makes the easy understanding of the unsteady flow characteristics of the typical industrial mixers.

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Characteristics of Friction Stir Lap Weldment according to Joining Parameter in 5052 Aluminium Alloy (5052 알루미늄 합금에서 접합변수에 따른 겹치기 마찰교반접합부의 특성)

  • Ko, Young-Bong;Park, Kyeung-Chae
    • Journal of the Korean institute of surface engineering
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    • v.45 no.5
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    • pp.181-187
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    • 2012
  • The Friction Stir Welding (FSW) has mainly been used for making butt joints in Al alloys. The development of Friction Stir Lap Welding (FSLW) would expand the number of applications. In this study, microstructures and mechanical properties of FSLW in A5052 alloy were investigated under varying rotating speed and probe length. Investigating the characteristics as FSLWed conditions were as below ; Failure Maximum load by shear fracture was increased proportional to the width of joint area, which was increased by input heat, stirring intensity in the case of 2.3 mm probe length. Tensile fracture occurred, and maximum load was determined due to side worm hole of joint area and softening of microstructure in the case of 3.0 mm probe length. In the case of 3.7 mm probe length, material hook and bottom worm hole were appeared at the end interface of joint area. The most sound FSLW condition with no defects was 3.0 mm probe length and 1500 rpm-100 mm/min. No defects were showed in 1500 rpm-100 mm/min and 1800 rpm-100 mm/min, but Vickers microhardness distribution in TMAZ/HAZ which was fracture zone was lower in 1800 rpm-100 mm/min than in 1500 rpm-100 mm/min. In this condition highest tensile strength, 215 MPa (allowable rate 78% of joint efficient) was obtained.

Manufacturing Al-scrap into Hypereutectic Al-Si Alloy by Using Electromagnetic Force (전자기력을 이용한 Al scrap으로 부터 과공정 Al-Si합금의 제조)

  • Yoon, Ji-Hyun;Moon, Kwang-Ho;Kim, Yong-Hyun;Lee, Kwang-Hak
    • Journal of Korea Foundry Society
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    • v.21 no.6
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    • pp.328-335
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    • 2001
  • The objective of this study is to investigate on manufacturing Al-scrap into hypereutectic Al-Si alloy by using electromagnetic force. The Fe element in the aluminium scrap was controlled by intermetallic compound method and using EMF(electromagnetic force). The most lumped compound was found after 10min holding at $690^{\circ}C$. A number of segregated compound was revealed when imposed to EMF at 30A. The refinement of primary Si particles was achieved by EMF stirring. Primary Si particles were refined and spheroidized most of all with the magnetic intensity of 180G for 10 min.

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Disinfection Characteristic of Sewage Wastewater Treatment Using Solar Light/TiO2 Film System (태양광/광촉매를 이용한 오폐수 살균특성)

  • Cho Il-Hyoung;Lee Nae-Hyun;An Sang-Woo;Kim Young-Kyu;Lee Seung-Mok
    • Journal of Environmental Science International
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    • v.15 no.7
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    • pp.677-688
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    • 2006
  • Currently, the application of $TiO_2$ photocatalyst has been focused on purification and treatment of wastewater. However, the use of conventional $TiO_2$ slurry photocatalyst results in disadvantage of stirring during the reaction and of separation after the reaction. And the usage of artificial UV lamp has made the cost of photocatalyst treatment system high. Consequently, we studied that solar light/$TiO_2$ film system was designed and developed in order to examine disinfection characteristics of sewage wastewater treatment. The optimum conditions for disinfection such as solar light intensity, characteristic of sewage wastewater, amounts of $TiO_2$ and comparison of solar ligth/$TiO_2$ systems with UV light/$TiO_2$ system was examined. The results are as follows: (1) photocatalytic disinfection process with solar light in the presence of $TiO_2$ film more effectively killed total coliform (TC) than solar light or $TiO_2$ film absorption only. (2) The survival ratio of TC and residual ratio of organic material (BOD, CODcr) decreased with remain resistant material. (3) The survival ratio of TC and residual ratio of organic material (BOD, CODcr) decreased with the increase of amounts of $TiO_2$. (4) TC survival ratio decreased linearly with increasing UV light intensity. (5) The disinfection effect of solar light/$TiO_2$ slurry system decreased more than UV light/$TiO_2$ film systems. (6) The disinfection reaction followed first-order kinetics. We suggest that solar light instead of using artificial UV light was conducted to investigate the applicability of alternative energy source in the disinfection of TC and the degradation of organic material.

Preparation and Characterization of Palladium Nanoparticles Supported on Nickel Hexacyanoferrate for Fuel Cell Application

  • Choi, Kwang-Hyun;Shokouhimehr, Mohammadreza;Kang, Yun Sik;Chung, Dong Young;Chung, Young-Hoon;Ahn, Minjeh;Sung, Yung-Eun
    • Bulletin of the Korean Chemical Society
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    • v.34 no.4
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    • pp.1195-1198
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    • 2013
  • Nickel hexacyanoferrate supported palladium nanoparticles (Pd-NiHCF NPs) were synthesized and studied for oxygen reduction reactions in direct methanol fuel cell. The NiHCF support was readily synthesized by a comixing of $Ni(OCOCH_3)_2$ and equimolar $K_3[Fe(CN)_6]$ solution into DI water under rigorous stirring. After the preparation of NiHCF support, Pd NPs were loaded on NiHCF via L-ascorbic acid reduction method at $80^{\circ}C$. Pd-NiHCF NPs were electrochemically active for oxygen reduction reaction in 0.1 M $HClO_4$ solution. X-ray absorption near edge structure analysis was conducted to measure the white line intensity of Pd-NiHCF to verify the OH adsorption. As a comparison, carbon supported Pd NPs exhibited same white line intensity. This study provides a general synthetic approach to easily load Pd NPs on porous coordination polymers such as NiHCF and can provide further light to load Pd based alloy NPs on NiHCF framework.

KOH Hydrothermal Synthesis of Zeolites from Hadong Kaolin (KOH수열 처리에 의한 하동카오린으로부터 Zeolite의 합성)

  • 이무강;신현무;임경천
    • Journal of Environmental Science International
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    • v.12 no.12
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    • pp.1321-1327
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    • 2003
  • Two different kinds of cases, with and without addition of noncrystalline silica to the Hadong kaolin were studied to obtain useful information on the synthesis of zeolite. The research was carried out to investigate the formation area and the crystalized degree of zeolite according to a synthetic time, the water content of raw material mixture, KOH concentration, and stirring intensity. In the case of without addition of noncrystalline silica to the Hadong kaolin and the low concentration range of KOH, the structure of the kaolin was not changed. However, when the mole ratio of K2O/SiO$_2$ in natural kaolin was increased, Linde-L zeolite and unknown structure of kaolins, U-1 and U-2 were produced. While in the high concentration range of KOH, the unknown structure of kaolins, U-6 and U-2, were produced and the production rate of U-6 was increased with the increased of K2O/SiO$_2$ mole ratio. In the case of with addition of noncrystalline silica to the Hadong kaolin and treatment with KOH hydrothermal processing, ZSM-5, ZSM-35, and Linde-L zeolites and the mixture of unknown structure of zeolites, U-1, U-2, U-3, and U-4, were obtained. Both cases demonstrated that the synthesis of zeolite from the Hadong kaolin was highly influenced by KOH concentration of raw material mixture.

Effect of Solvent on Swelling, Porosity and Morphology of Transparent Poly (HEMA)

  • Pathak Tara Sankar;Kim Lae-Hyun;Chung Kun-Yong
    • Korean Membrane Journal
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    • v.8 no.1
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    • pp.67-73
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    • 2006
  • Transparent materials are well known but preparation of transparent poly 2-hydroxyethyl methacrylate {poly (HEMA)} material by varying solvent is a new one and economically reliable. This material is prepared from hydroxyl based monomer HEMA by radical polymerization using benzoyl peroxide (BPO) as initiator and isobutanol, 2-butanol, 1-butanol, hexane and toluene as a solvent. The reaction temperature, time and stirring speed were set at $70^{\circ}C$, 4 hrs and 150 rpm, respectively. The polymer was characterized for functional group by IR spectroscopy. It was observed that the intensity of band at $1637 cm^{-1}$ a characteristic band of C=C stretching disappeared indicating that it was completely consumed after polymerization. It was observed that swelling percentage increases with increase as time passes but after a certain time a constant swelling percentage is achieved. SEM pictures reveals that poly (HEMA) prepared by different solvent shows pore with a distinguishable void up to several micrometers. The BET surface area, cumulative pore volume and average pore diameter is greater in poly (HEMA) prepared by hexane as a solvent compared to other solvents. Poly (HEMA) prepared by 1-butanol as a solvent shows higher glass transition temperature compared to other solvents. Poly (HEMA) prepared by different solvents shows $90{\sim}94%$ light transmission property from light transmission measurement and looks transparent.