• 한국추진공학회지
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• 제24권6호
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• pp.101-107
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• 2020

본 논문에서는 HTPB/AP 계열의 추진제의 경화 온도를 변화시키는 Step 경화 방법으로 경화일 단축 연구를 진행하였다. 이 연구는 HTPB/AP 계열의 추진기관 제작 시 생산성 향상(제작기간 단축 및 치구회수율 증대)을 목적으로 한다. 정상 경화 대비 추진제의 기계적 물성을 비교하여 정상 경화 시 60℃ 5일 소요되는 경화일을 Step 경화로 4일(60℃ 1일 / 65℃ 3일)로 설정하였다. 경화일 단축을 적용 시 추진제 노화 특성을 알아보기 위해 Step 경화 후 후경화(Post-cure) 시험을 진행하였다. 이를 통해 기계적 물성 및 열팽창 계수를 측정하여 추진제의 후경화 특성을 분석하였다. 또한, Step 경화 후 가속 노화 시험을 진행하여 12주차 경과 후 인장시험을 수행하였다. 그 결과, Sm(bar)은 8 bar 이상, Em(%)은 40%이상으로 요구되는 우수한 기계적 물성을 가지는 것을 알 수 있었다.

• 대한치과보철학회지
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• 제38권3호
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• pp.310-320
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• 2000

Statement of the problem. The record base in fabricating procedures of the complete denture, as a temporary form for reproducing denture base, is used to record upper and lower jaw relation and to align artificial teeth and try-in it in the mouth. The accuracy of jaw relation record is affected by the accuracy, stiffness and stability of the record base. So, the accuracy of record base is the most important requirements of jaw relation records. Purpose of study. The purpose of this study was to evaluate the gap that occurred over the palatal area of a maxillary record base fabricated with autopolymerizing resin and light-curing resin. Methods/material. The maxillary record bases were fabricated out of autopolymerizing resin that is used the most frequently in clinics and light-curing resin that attracts special attention for its several merits. The light-curing resin was made by two kinds of polymerization methods, which are one step curing method and multiple step curing method. All record bases were cut in certain positions of the master cast 1 hour and 1 day later after fabrication and the accuracy of the master cast was measured and analyzed with a microscope. Results. A pattern of gap formation between the record base and the maxillary cast was observed in all specimens. According to kinds of resins, autopolymerizing resin was significantly more accurate than light-curing resin. There was no statistical difference according to time lapse, and in all three groups, the maximum discrepancy occurred at the posterior border in the mid-palatal region. Conclusion. The autopolymerizing resin is better than light-curing resin, and multiple step curing method is more accurate than one step curing method when using light-curing resin.

• Restorative Dentistry and Endodontics
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• 제25권2호
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• pp.299-308
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• 2000

The purpose of this in vitro study was to evaluate the microleakage of 5 curing methods in class V composite restorations which are composed of two-step light curing, pulse-delay cure, low curing-light intensity, moderate curing-light intensity and high curing-light intensity. In this study, class V cavities were prepared on buccal and lingual surfaces of 50 extracted human upper or lower molars on cementum margin. Single Bond adhesive and Z-100 shade A2 were applied for each group following the manufacture's instruction. The experimental teeth were randomly divided into 5 groups of 10 samples (20 surfaces) each. Group 1: two-step light curing; Group 2: pulse-delay cure; Group 3: low curing-light intensity; Group 4: moderate curing-light intensity; Group 5: high curing-light intensity. After 500 thermocycling between $5^{\circ}C$ and $55^{\circ}C$, the 60 teeth were placed in 2% methylene blue dye for 24 hours, then rinsed with tab water. The specimens were embedded in clear resin, then sectioned buccolingually through the center of restoration with a low speed diamond saw. The dye penetration on each of the specimen was then observed with a stereomicroscope at ${\times}20$. The composite resin/tooth interfaces were examined under Scanning Electron Microscopy. The results were statistically analyzed using the Kruskal-Wallis One Way ANOVA and Dunn's Method. The results of this study were as follows. 1. In all groups, the leakage values seen at the enamel margin were significantly lower than those seen at the dentin margin(P<0.05). 2. No group in this study showed significant differences in leakage values at both the enamel and the dentin margins(P<0.05). 3. In all groups, the gaps seen at the enamel margin were significantly lower than those seen at the dentin margin(P<0.05). 4. The gaps in this study showed significant differences and two-step light-curing and low curing-light intensity produced significant less gap than high curing-light intensity(P<0.05).

• 한국환경과학회지
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• 제27권11호
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• pp.1023-1028
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• 2018

Shape memory materials are widely used in high-tech industries. Although shape memory polymers have been developed, they have a disadvantage, only unidirectional resilience. Shape memory polymers with bi-directional recovery resilience have been actively studied. In this study, a bidirectional shape memory polyurethane was synthesized using poly(${\varepsilon}$-caprolactone) diol, methylene dicyclohexyl diisocyanate, and hydroxyethyl acrylate. The first physical curing occurred between hard segments and hydrogen bondings when the solution was dried. The second curing in acrylate groups was performed by UV exposure. A degree of curing was analyzed by infrared spectroscopy. The shape memory properties of 2 step-cured polyurethanes were investigated as a function of UV curing time.

• 대한소아치과학회지
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• 제33권2호
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• pp.221-232
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• 2006

본 연구는 단계별 광중합 방법이 복합레진의 중합 및 수축 응력에 미치는 효과를 비교, 평가하고자 자연치를 대상으로 와동을 형성하고 할로겐 광중합기와 LED 광중합기의 통법에 의한 연속 조사 및 단계별 조사법으로 각각 복합레진을 중합시킨 후 수축 응력을 측정하고 주사전자현미경을 통해 수복물과 와동의 계면부에서 접착 상태를 관찰하여 다음과 같은 결과를 얻었다. 1. 모든 군에서 광중합 직후에는 일시적으로 팽창되었다가 초기에는 급격한 수축 응력의 증가를 보였고 시간이 경과될수록 수축 응력의 증가가 완만해지는 경향을 보였다(P<0.05). 2. 동일한 광조사 군내에서는 hybrid형인 Filtek $Z-250^{TM}$군보다는 flowable형인 $Filtek\;flow^{TM}$군이 더 적은 수축 응력을 보였다. 3. Filtek $Z-250^{TM}$군에서는 LED 단계별 조사군이 수축 응력 이 가장 적게 나타났다(P<0.05) 4. $Filtek\;flow^{TM}$군 역시 LED단계별 조사군이 수축 응력이 가장 작게 나타났으나(P<0.05) Filtek Z-250군에서와 같이 다른 조사군에 비해 많은 차이를 보여주지는 못했다. 5. 주사전자현미경으로 관찰한 복합레진과 와동벽과의 접합 상태는 긴밀한 상태를 보였으나 LED 조사군에서 일부 틈이 관찰되었다. 이상의 결과를 종합해 보면 hybrid형 복합레진의 경우 단계별 중합방식을 사용할 경우 단일광도의 중합방식에 비해 수축 응력을 감소시킬 수 있고 적절한 변연 적합상태를 유지시킴으로써 임상적으로 고광도 LED 광중합기의 경우 단계별 중합방식의 사용이 유리하다고 사료된다.

• 대한소아치과학회지
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• 제32권2호
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• pp.332-343
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• 2005

본 연구에서는 기존의 할로겐 광중합기를 이용하여 40초간 조사하여 복합레진을 중합한 경우와 플라즈마 광중합기를 이용한 고강도의 중합 및 완속기시 중합 방식, 그리고 LED 광중합기를 이용한 통법의 중합과 완속기시 중합 방식으로 복합레진을 중합하여 발생되는 수축응력을 비교하고 미세경도를 측정하여 중합도를 평가하였다. 내경 7mm, 외경 10mrn의 아크릴릭 주형을 제작하고 외면에 스트레인게이지를 부착시킨 뒤 각각의 광원에 따른 중합모드로 광중합 하였다. 광조사 시점부터 1초 간격으로 600초간 수축응력을 측정하였으며, 중합 24시간 후 각 군의 미세경도를 측정하여 통계 분석하였다. 수축응력 측정 후 시편을 종단하여 주사전자현미경으로 레진수복물과 아크릴릭 주형 계면을 관찰하였다. 이상의 실험을 통해 얻은 결과는 다음과 같다. 1. 플라즈마 광과 LED 광원의 완속기시 중합방식은 각각의 기본 중합방식에 비해 중합 10분 후에 수축응력 감소를 보였다(P<0.05). 2. 완속기시 중합방식의 플라즈마 광이 가장 낮은 수축응력을 보였으나 미세경도 또한 가장 낮았다(P<0.05). 3. 완속기시 중합방식의 LED 광중합은 기존의 할로겐 광과 LED 광중합 방법에 비하여 낮은 수축응력을 보였다(P<0.05). 4. 완속기시 중합방식의 LED 광으로 조사한 시편의 미세경도는 단일광도로 조사한 할로겐 광과 LED 광중합과 비교하여 유의할만한 차이가 나타나지 않았다(P>0.05). 5. 기존의 할로겐 광과 완속기시 중합방식의 LED로 중합한 시편이 플라즈마 광과 단일강도의 LED로 조사한 군보다 더 나은 변연봉쇄를 보였다.

• 한국연초학회지
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• 제22권2호
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• pp.133-137
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• 2000

The bulk curing experiment to improve the quality of flue-cured leaves were carried out to evaluate relationship between the modified(3 step-up) drying and conventional drying method in bulk curing process. Modified drying method was somewhat higher values in yellowing color index of cured leaves, and less brittle than those in conventional drying program. As to the chemical properties, there was no difference in chemical component levels in cured leaves between the modified and the conventional methods, while the major chemical compounds in relation to aromatic essential oil of cured leaves showed mostly higher level in the modified method than that in conventional drying method. Additionally 3 step-up drying method increased the tobacco quality by 2 % in price per kg compared with conventional drying method.

• 한국전산구조공학회:학술대회논문집
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• 한국전산구조공학회 1996년도 가을 학술발표회 논문집
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• pp.184-191
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• 1996

In curing Process of tire, Contact and slip occurs between green tire and curing bladder. The curing process is a critical step in the manufacture of tires. In this investigation, curing bladder shaping is examined using a finite element method. Specifically, a finite element model between the inner part of green tire and the outer part of curing bladder is generated using contact element and curing bladder is generated using incompressible element, The experimental tensile tests are used to get the material properties of bladder rubber on practical conditions. Numerical analyses are performed on two different bladder types, different overall outer diameters of curing bladder and different heights of curing bladder.

• Advances in concrete construction
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• 제9권1호
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• pp.33-41
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• 2020

In this study, polyethylene glycol (PEG) and polyacrylamide (PAM) have been used as self-curing agents to produce self-curing concrete (SC). Compressive strength, ultrasonic pulse velocity (UPV), bulk electrical resistivity, chloride ion penetrability, water permeability, and main microstructural characteristics were examined under different curing regimes, and compared to those of the control concrete mixture with no self-curing agents. One batch of a control mixture and one batch of a SC mixture were air-cured in the lab to act as non-water-cured samples. The water curing regimes for the control mixture included continuous water curing for 3, 7, and 28 days and periodical moist curing using wetted burlap for 3 and 7 days. Curing regimes for the SC mixtures included 3 days of water curing and periodical moist curing for 3 and 7 days. SC mixtures showed better microstructure development and durability performance than those of the air-cured control mixture. A short water curing period of 3 days significantly improved the performance of the SC mixtures similar to that of the control mixture that was water cured for 28 days. SC concrete represents a step towards sustainable construction due to its lower water demand needed for curing and hence can preserve the limited water resources in many parts of the world.

• 대한기계학회논문집A
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• 제21권3호
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• pp.378-384
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• 1997

In curing process of tire, contact and slip occurs between green tire and curing bladder. The curing process is a critical step in the manufacture of tires. In this investigation, curing bladder shaping is examined using a finite element method. Specifically, a finite element model between the inner part of green tire and the outer part of curing bladder is generated using contact element and curing bladder is generated using incompressible element. Numerical analysis are performed on two different bladder types, different overall outer diameters of curing bladder and different heights of curing bladder. Numerical results show that contact pressure is increased by using toroidal type of curing bladder, increasing overall diameter and increasing height of curing bladder. To obtain natural equilibrium carcass line, there is a requirement in increasing contact pressure of the section between side and bead.