• 제목/요약/키워드: Step cooling

검색결과 196건 처리시간 0.027초

Al-Mg-Cu-Mn 합금의 초소성 특성 (Superplastic Properties of Al-Mg-Cu-Mn Alloys)

  • 박종우;김희수;문인기;하기윤;이덕열
    • 한국재료학회지
    • /
    • 제5권1호
    • /
    • pp.132-139
    • /
    • 1995
  • Al-Mg-Cu-Mn계 합금을 가공열처리하고 초소성 특성을 조사한 후 광학 및 전자 현미경을 이용하여 초소성에 영향을 미치는 주요한 인자들을 조사하였다. 균질화 과정에서 제거되지 않은 조대한 2차상들은 그 후의 가공열처리 과정에서도 계속 잔류하여 초소성 변형 중 기공을 유발함으로써ㅓ 초소성 신율을 저하시켰다. 반면에 가공열처리 과정에서 생성된 미세한 석출물은 결정립 성장을 억제하여 조직을 안정화함으로써 초소성 특성을 향상시켰다. 균질화처리 조건은 2차상의 크기과 분포에 큰 영향을 주어 2단계 균질화-공냉처리는 1단계 균질화-노냉처리보다 조대한 2차상의 제거와 미세석출물의 생성에 효과적이었다.

  • PDF

경남 하동군 발견 철제무구류의 금속조직 조사 및 성분분석 (Microstructure investigation and component analysis of iron weapons found at Hadong-gun, Kyungnam Province)

  • 유재은;고형순;황진주
    • 보존과학연구
    • /
    • 통권21호
    • /
    • pp.177-206
    • /
    • 2000
  • In the study of iron artifacts, microstructure investigation is an indispensable step to find out the manufacturing method and skill. The iron weapons that we have excavated and investigated at the ruins of Gohyun Castle site, Hadong-gun, Kyungnam Province are traced to the era of Choson Dynasty. By sampling specimens of some artifacts, we have made microstructure investigation and component analysis of them. For microstructure investigation we used metallographic microscopes, and for component analysis we used the methods of C/S analysis and Inductively coupled plasma emission spectrometry (ICP) analysis which is designed to verify components and contenets of a very small amount elememt. Microstructure of the artifacts is mainly divided into three parts. Inner part is Widmanstatten, a typical overheated structure, upon which we can see another part with fine grains and with extremely small quantities of carbon. And on the surface, there is a carbonized part. When the shape is formed through forging process at a high temperature the carbon content of the surface is getting down and the grains come to be finer. Next, carbonizing process is to be done for hardening the surface, which is followed by cooling process. Cooling rates seem to be different from artifacts to artifacts. All artifacts have clearly distinguishable grain boundaries in their unique structure. Since this kind of structure is rarely found, it seems to offer a clue to find out the manufacturing method. The outcome of component analysis is almost the same with that of microstructure investigation. As is demonstrated by C/S analysis, carbon content is 0.39-1.24% and sulfur is contained 0.0005-0.010%.

  • PDF

열-기계 연계 해석을 이용한 에너지 제어 용착 및 담금질 공정으로 제작된 시편의 잔류응력 특성 분석 (Investigation of Residual Stress Characteristics of Specimen Fabricated by DED and Quenching Processes Using Thermo-mechanical Analysis)

  • 황안재;이광규;안동규
    • 한국기계가공학회지
    • /
    • 제20권12호
    • /
    • pp.113-122
    • /
    • 2021
  • Complicated residual stress distributions occur in the vicinity of a deposited region via directed energy deposition (DED) process owing to the rapid heating and cooling cycle of the deposited region and the substrate. The residual stress can cause defects and premature failure in the vicinity of the deposited region. Several heat treatment technologies have been extensively researched and applied on the part deposited by the DED process to relieve the residual stress. The aim of this study was to investigate the residual stress characteristics of a specimen fabricated by DED and a quenching process using thermomechanical analyses. A coupled thermomechanical analysis technique was adopted to predict the residual stress distribution in the vicinity of the deposited region subsequent to the quenching step. The results of the finite element (FE) analyses for the deposition and the cooling measures show that the residual stress in the vicinity of the deposited region significantly increases after the completion of the elastic recovery. The results of the FE analyses for the heating and quenching stages further indicate that the residual stress in the vicinity of the deposited region remarkably increases at the initial stage of quenching. In addition, it is observed that the residual stress for quenching is lesser than that after the elastic recovery, irrespective of the deposited material.

반연속주조된 대형 블룸에서 발생하는 거시편석 및 석출물 거동 (Behavior of Macrosegregation and Precipitation Developed in Semi-continuously Cast Large Bloom)

  • 김혜주;이형록;김경아;이주동;오경식;권상흠;김동규
    • 한국주조공학회지
    • /
    • 제39권1호
    • /
    • pp.7-13
    • /
    • 2019
  • Few studies of large blooms over 700 mm thick among those used for the forging of raw materials have been reported. The cooling rate difference between the surface and the center of a large bloom is large, and the degradation of the mechanical properties is likely in cases involving excessively coarse precipitates resulted from the slow cooling rate of a large bloom after casting. Therefore, a schematic investigation of the growth behaviors of precipitates while varying their locations in blooms is necessary. The dissolution behaviors of precipitates were investigated by simulating a reheating process during which the bloom is heated to a high temperature. The segregation behavior of the as-cast large bloom was also investigated. Reheating specimens were obtained after an isothermal heat treatment at $1150^{\circ}C$ with various holding times to simulate the reheating process, with the samples undergoing a subsequent water quenching step. The precipitates were extracted using an electrolytic extractor and a particle size analysis was conducted with the aid of SEM, EDS, and TEM. In the present work, Al oxide, MnS and Nb carbide were mainly observed.

Analysis on Green BIM based Atrium Sizes in the Early Design Stage

  • Jeong, Seung-Woo;Lee, Kweon-Hyoyng;Choo, Seung-Yeon
    • 국제학술발표논문집
    • /
    • The 5th International Conference on Construction Engineering and Project Management
    • /
    • pp.260-266
    • /
    • 2013
  • This study for establishing specific standards of atrium design aims to discuss design of atrium to consider energy performance according to the types of atrium of office building. In order to evaluate a type and a scale of atrium at the early design stage, modeling details of mass design were set as standards of conceptual design. In the experiment, Project Vasari was used to analyze modeling and energy consumption, based on the LOD 100-step suggested by AIA, because there is no guideline to specify a level of modeling details at each design process. From this analysis, the correlation among a simple-typed atrium and scale and energy load was understood, and the followings are the considerations for designing an atrium. First, the single-sided atrium reduced energy the most, and it was followed by three-sided, two-sided, four-sided and continuous-typed ones. On the whole, they could decrease energy by up to about 15%. Also, the atrium with a wide facade facing in the south was more favorable to reduce energy. Second, planning an atria within 10~30% of the whole building area was more energy efficient. Third, rather than the depth, adjusting the length in designing an atrium could reduce cooling and heating loads by 1.5% per 1m. As explained above, energy performance evaluation considering types and planning elements of atrium helps to assess alternatives in a reasonable way. In particular, considering the use of building needs to be preceded to select a type of atrium, although it is also important to consider its planning elements.

  • PDF

낙상예방 프로그램이 양로원 여성노인의 보행, 균형 및 근력에 미치는 영향 (Effect of the Fall Prevention Program(EPP) on gait, balance and muscle strength in elderly women at a nursing home)

  • 전미양;최명애
    • Journal of Korean Biological Nursing Science
    • /
    • 제4권1호
    • /
    • pp.5-23
    • /
    • 2002
  • Purpose: To determine the effect of the Fall Prevention Program(EPP) on gait, balance and muscle strength in elderly women at a nursing home. Method: The subjects of this consisted of 38 elderly women between the ages of 70 to 89 years living at a nursing home located in Seoul. Each of the experimental group and control group was composed of 19 subjects. The subjects in experimental group have participated in FPP for the 8 weeks which consisted of exercise, education and foot care. They started to exercise for 40 minutes per session, 3 sessions a week during the 1st week at 40% of age adjusted maximum heart rate. From the 2nd week to the 4th week, they increased the duration of exercise to 50 minutes per session and the intensity to 60% of age-adjusted maximum heart rate. They participated in 50 minutes at 60% of age-adjusted maximum heart rate from the 5th week to the 8th week. Each exercise session consisted of 10 minutes of warming-up exercise, 30 minutes of conditioning exercise and 10 minutes of cooling-down exercise. They participated in education for 20 minutes per week from the 1st week to the 4th week. Then they participated in a 30-minute foot care program per week from the 5th week to the 8th week. Gait, balance and muscle strength for each subject were measured before and after FPP. Gait was evaluated by step length, step width, gait speed and walking distance. Balance was measured by the duration of standing on one leg with their eyes closed and open each, and a get-up and go test. Grip strength was measured by hand dynamometer. Hip extensor and flexor strength, knee extensor and flexor strength and ankle plantarflexor and dorsiflexor strength were measured by manual muscle tester. Data was analyzed using SPSS form Windows. t-test and Chi square test were utilized as a homogeneity test. Repeated measure ANOVA was used to test the effect of FPP. Result: 1) Step width significantly decreased, and step length, gait speed and walking distance significantly increased in the experimental group compared with the control group after FPP(p<0.005). 2) There was no significant change in standing time on one leg with their eyes closed after FPP. The standing time on leg with their eyes open and the time of "get-up and go" significantly decreased in the experimental group compared with the control group after FPP(p<0.005). 3) Muscle strength-grip strength, hip extensor and flexor strength-significantly increased in the experimental group compared with the control group after FPP(p<0.005). 4) There was no significant difference of frequency of fall between the experimental group and control group during the period of FPP. Conclusion: These results suggest that FPP can increase gait, balance and muscle strength of elderly women at a nursing home.

  • PDF

Development of a new vitrification solution, VSL, and its application to the cryopreservation of gentian axillary buds

  • Suzuki, Mitsuteru;Tandon, Pramod;Ishikawa, Masaya;Toyomasu, Takayuki
    • Plant Biotechnology Reports
    • /
    • 제2권2호
    • /
    • pp.123-131
    • /
    • 2008
  • Vitrification methods are convenient for cryopreserving plant specimens, as the specimens are plunged directly into liquid nitrogen (LN) from ambient temperatures. However, tissues and species with poor survival are still not uncommon. The development of vitrification solutions with high survival that cover a range of materials is important. We attempted to develop new vitrification solutions using bromegrass cells and found that VSL, comprising 20% (w/v) glycerol, 30% (w/v) ethylene glycol, 5% (w/v) sucrose, 10% (w/v) DMSO and 10 mM $CaCl_2$, gave the highest survival following cryopreservation, as determined by fluorescein diacetate staining. However, the cryopreserved cells showed little regrowth, for unknown reasons. To check its applicability, VSL was used to cryopreserve gentian axillary buds and the performance was compared with those of conventional vitrification solutions. Excised gentian stem segments with axillary buds (shoot apices) were two-step precultured with sucrose to induce osmotic tolerance prior to cryopreservation. Gentian axillary buds cryopreserved using VSL following the appropriate preculturing approach exhibited 78% survival (determined by the regrowth capacity), which was comparable to PVS2 and PVS1 and far better than PVS3. VSL had a wider optimal incubation time (20-45 min) than PVS2 and was more suitable for cryopreserving gentian buds. The optimal duration of the first step of the preculture was 7-11 days, and preculturing with sucrose and glucose gave a much higher survival than fructose and maltose. VSL was able to vitrify during cooling to LN temperatures, as glass transition and devitrification points were detected in the warming profiles from differential scanning calorimetry. VSL and its derivative, VSL+, seem to have the potential to be good alternatives to PVS2 for the cryopreservation of some materials, as exemplified by gentian buds.

토끼의 정상 및 핵이식배의 유리화 및 완만동결에 따른 융해 후 발달율 (Post-thaw Embryo Development following Vitrification or Slow Freezing of Rabbit Normal and Nuclear Transplant Embryos)

  • 강다원;최창용;하란조;강태영;심보웅;최상용;이효종;박충생
    • 한국수정란이식학회지
    • /
    • 제13권1호
    • /
    • pp.1-9
    • /
    • 1998
  • In order to improve the cryopreservation by vitrification or slow freezing of nuclear transplant rabbit embryos, the effects of factors affecting embryo cryopreservation such as cryoprotectants, equilibration, cooling rate and post-thaw dilution on post-thaw survial and development were determined using intact embryos of morular stage. And the post-thaw development of nuclear transplanted embryos cryopreserved under the optimal conditions examined was compared between vitrification and slow freezing. The cryoprotectant solution used was ethyleneglycol-ficoll-sucrose (EFS) or ethyleneglycol-poly-vinylpyrrolidone-galactose- I (EPG- I ) for vitrification, and EPG- II for slow freezing. To examine the viability of frozen-thawed embryos, the nuclear transplanted embryos were co-cultured in TCM-199 plus 10% FBS with bovine oviduct epithelial cells(BOEC) for 24 hrs and the intact morulae were co-cultured with BOEC for 5 days and 3 days to hatching blastocyst stage in 39 ˚C 5% $CO_2$ incubator. The results obtained were as follows: Following vitrification with EFS, the post-thaw development of rabbit morulae to hatching blastocyst was significantly(P<0.05) higher in compacted stage(82.4%) than in early morular stage(60.0%). The post-thaw development of compacted morulae to hatching blastocyst was similarly high in vitrification with EFS(82.4%), EPG- I (85.0%) and in slow freezing with EPG- II (83.3%). Following vitrification with EPG- I, the post-thaw development of intact rabbit morulae to hatching blastocyst was similar as 78.0% and 85.0% in 1-step and 2-step post-thaw dilution, respectively. The post-thaw development of nuclear transplanted rabbit embryos of compacted morulae stage to hatching blastocyst was similarly 43.6% and 40.0% in vitrification with EPG- Iand slow freezing with EPG- II, respectively. These results indicated that the rabbit nuclear transplant and intact embryos of morulae stage could be well cryopreserved with either vitrification or slow freezing procedure.

  • PDF

다양한 첨가 성분을 함유한 ZnO 바리스터의 미세구조 (Microstructure of ZnO Varistors with Various Additives)

  • 이훈;조성걸;김창조;김형식
    • 한국세라믹학회지
    • /
    • 제32권12호
    • /
    • pp.1323-1330
    • /
    • 1995
  • The effects of various additives on the microstructures of sintered ZnO varistors were examined. Bi2O3, Sb2O3 and Cr2O3 were added to ZnO step by step to identify the effect of each component. The specimens were prepared by sintering at 110$0^{\circ}C$ and 120$0^{\circ}C$ in ambient atmosphere. In ZnO-Bi2O3-Sb2O3 ternary system, decrease of averge grain size due to antimony oxide addition depends on sintering temperature as well as Bi2O3 content. When Sb2O3 was partly or completely replaced by Cr2O3, grain size was further reduced. A significant amount of pyrochlore phase which was not transformed to spinel and Bi2O3-rich liquid phase seemed to remain during sintering at 110$0^{\circ}C$. Unlike ZnO-Bi2O3-Sb2O3 system, the $\alpha$-spinel phase containing significant amount of Cr did not transform to pyrochlore during furnace cooling. Fine spinel particles around 1${\mu}{\textrm}{m}$ size were ovserved within ZnO grains and grain boundaries, which were believed to be responsible for grain-growth inhibition in ZnO-Bi2O3-Sb2O3.

  • PDF

Validation of spent nuclear fuel decay heat calculation by a two-step method

  • Jang, Jaerim;Ebiwonjumi, Bamidele;Kim, Wonkyeong;Park, Jinsu;Choe, Jiwon;Lee, Deokjung
    • Nuclear Engineering and Technology
    • /
    • 제53권1호
    • /
    • pp.44-60
    • /
    • 2021
  • In this paper, we validate the decay heat calculation capability via a two-step method to analyze spent nuclear fuel (SNF) discharged from pressurized water reactors (PWRs). The calculation method is implemented with a lattice code STREAM and a nodal diffusion code RAST-K. One of the features of this method is the direct consideration of three-dimensional (3D) core simulation conditions with the advantage of a short simulation time. Other features include the prediction of the isotope inventory by Lagrange non-linear interpolation and the use of power history correction factors. The validation is performed with 58 decay heat measurements of 48 fuel assemblies (FAs) discharged from five PWRs operated in Sweden and the United States. These realistic benchmarks cover the discharge burnup range up to 51 GWd/MTU, 23.2 years of cooling time, and spanning an initial uranium enrichment range of 2.100-4.005 wt percent. The SNF analysis capability of STREAM is also employed in the code-to-code comparison. Compared to the measurements, the validation results of the FA calculation with RAST-K are within ±4%, and the pin-wise results are within ±4.3%. This paper successfully demonstrates that the developed decay heat calculation method can perform SNF back-end cycle analyses.