• The KSFM Journal of Fluid Machinery
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• v.13 no.6
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• pp.36-41
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• 2010

Design, manufacture and calibration procedures of a venturi pipe flowmeter for airflow measurement in altitude engine test were discussed. Altitude engine test using venturi pipe was given as an example. The venturi was designed per the ISO standard of ISO5167, and was intented to include the entire airflow range in the test envelope of the gas turbine engine. Measurement uncertainty analysis was performed in the design procedure to investigate the effect of venturi geometry and sensor specification upon the measurement uncertainty. Manufacturing process was designed to minimize the deviation from the geometry of design. Calibration was performed to get the relationship between the discharge coefficient and the pipe Reynolds number. Then the uncertainty was assessed again using real data acquired during engine test. Through these procedures, it was possible to maintain the uncertainty of airflow measurement under 1 % for most of the operating envelope of the gas turbine engine. The discharge coefficient of the venturi pipe showed agreement with the value suggested in the ISO standard ISO5167-4 within 0.6 %.

• YAKHAK HOEJI
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• v.51 no.3
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• pp.206-213
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• 2007

Recently estimating the uncertainty of an analytical result has become an essential part of quantitative analysis. This study describes the uncertainty of the measurement for the determination of methamphetamine and its major metabolite amphetamine in human hair, The method consists of washing, drying, weighing, incubation and extraction with methanolic HCI solution, clean-up, trifluoroacetyl derivatization, and qualification/quantification of residues by gas chromatography/mass spectrometry (GC/MS). Traceability of measurement was established through traceable standards and calibrated volumetric equipment and measuring instruments. Measurement uncertainty associated with each analyte in real samples was estimated using quality control (QC) data. The main source of combined standard uncertainty comprised two components, which are uncertainties associated with calibration linearity and variations in QC, while those associated with preparation of analytical standards and sample weighing were not so important considering the degree of contribution. Relative combined standard uncertainties associated with the described method ranged for individual analytes from 4.99 to5.03%.

• Journal of Climate Change Research
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• v.9 no.1
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• pp.103-115
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• 2018

The uncertainty of climate scenarios, as initial information, is one of the significant factors among uncertainties of climate change impacts and vulnerability assessments. In this sense, the quantification of the uncertainty of climate scenarios is essential to understanding these assessments of impacts and vulnerability for adaptation to climate change. Here we quantified the precision of surface temperature of ensemble scenarios (high resolution (1km) RCP4.5 and 8.5) provided by Korea Meteorological Administration, with spatiotemporal variation of the standard deviation of them. From 2021 to 2050, the annual increase rate of RCP8.5 was higher than that of RCP4.5 while the annual variation of RCP8.5 was lower than that of RCP4.5. The standard deviations of ensemble scenarios are higher in summer and winter, particularly in July and January, when the extreme weather events could occur. In general, the uncertainty of ensemble scenarios in summer were lower than those in winter. In spatial distribution, the standard deviation of ensemble scenarios in Seoul Metropolitan Area is relatively higher than other provinces, while that of Yeongnam area is lower than other provinces. In winter, the standard deviations of ensemble scenarios of RCP4.5 and 8.5 in January are higher than those of December. Especially, the standard deviation of ensemble scenarios is higher in the central regions including Gyeonggi, and Gangwon, where the mean surface temperature is lower than southern regions along with Chungbuk. Such differences in precisions of climate ensemble scenarios imply that those uncertainty information should be taken into account for the implementation of national climate change policy.

• Transactions of the Korean Society of Mechanical Engineers B
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• v.32 no.9
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• pp.712-719
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• 2008

Light Oil Flow Standard System(LOFSS), as a national oil flow standard system, in Korea Research Institute of Standards and Science(KRISS) was developed for oil flowmeter calibration, and the expanded uncertainty of flow quantity determination was estimated within 0.04 %. In order to improve the reliability of the LOFSS measurement, a proficiency test was carried out in the flow range of 20 and $240\;m^3/h$ (Reynolds number $20,000{\sim}900,000$). A turbine flowmeter was used as a transfer package in round robin test. The water flow standard system of KRISS, the pipe prover of the national calibration and test organization and the master meter calibrator of the turbine flowmeter supplier, which used the different working fluid respectively, were compared with the turbine flowmeter measurement. The maximum difference of measurement was 0.15 % between the LOFSS and the pipe prover. The En numbers of the each system measurement were evaluated at the same Reynolds number. It was found that the En numbers were less than 1 in the comparison, which means the procedures of the uncertainty estimation of the each calibrators were reasonable and reliable.

• Proceedings of the KIEE Conference
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• 2009.07a
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• pp.1355_1357
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• 2009

This paper describes the standard system for calibrating pulse generator of partial discharge(PD) and its uncertainty. The system is consisted of digital pulse generator, digital recorder and evaluation software. The uncertainty requirement of calibrator charge is less than $\pm$ (0.1pC + 0.03q) and that of pulse duration is less than $\pm$ 10 %. The system can generate various kind of calibration pulses such as single pulse, double pulses, oscillation pulse, long-duration pulse, random pulses and evaluate their uncertainty.

• The Transactions of The Korean Institute of Electrical Engineers
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• v.63 no.11
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• pp.1622-1625
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• 2014

The main measurement uncertainty factors in DC high-voltage dividers for a national high-voltage standard are the measurement uncertainty of low-voltage arm and the stability of a high-voltage supply. In this study, the uncertainties by the two factors are greatly improved. As a result the measurement uncertainty for the DC high-voltage divider is reduced from $16{\times}10^{-6}(k=2)$ to $8{\times}10^{-6}(k=2)$ which is at international level.

• Bulletin of the Korean Chemical Society
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• v.31 no.11
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• pp.3139-3144
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• 2010

A model system has been established for the evaluation of the uncertainty of the value from measurements of multiple subsamples by isotope dilution mass spectrometry (IDMS). In this report, we apply this model system for the evaluation of measurement uncertainty in determination of folic acid in infant formula. Five subsamples were analyzed by IDMS. The mean of the measurement results of the five subsamples was assigned as the final measurement value. The standard deviation (s) of the results from five subsamples was attributable to repeatability of the measurement. The uncertainty components in the IDMS measurement methods were categorized into two groups. Group I includes uncertainty components which give common systematic effects to all subsamples and do not contribute to the variation among multiple measurements (repeatability). Group II includes uncertainty components that give random effects on the measurement results, and are related with the measurement repeatability. These random effects are attributed to s. Therefore, the uncertainty of the final value was calculated by combining the standard deviation of the mean of multiple measurements, $s/{\surd}n$ (where n = 5), and the measurement uncertainty associated with the uncertainty components that give systematic effects.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2003.06a
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• pp.264-267
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• 2003

Pitch measurements of 150 nm pitch one-dimensional grating standards were carried out using an contact mode atomic force microscopy(C-AFM) with a high resolution three-axis laser interferometer. It was called as 'Nano-metrological AFM' In Nano-metrological AFM, Three laser interferometers were aligned well to the end of AFM tip. Laser sources of the three-axis laser interferometer in the nano-metrological AFM were calibrated with an I$_2$-stablilzed He-Ne laser at a wavelength of 633 nm. So, the Abbe error was minimized and the result of the pitch measurement using the nano-metrological AFM has a traceability to the length standard directly. The uncertainty in the pitch measurement was estimated in accordance with the Guide to the Expression of Uncertainty in Measurement(GUM). The Primary source of uncertainty in the pitch-measurements was derived from repeatability of pitch-measurement, and its value was approx 0.186 nm. Expanded uncertainty(k=2) of less than 5.23 nm was obtained. It is suggested that the metrological AFM is a useful tool for the nano-metrological standard calibration.

• Journal of the Korean Vacuum Society
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• v.14 no.4
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• pp.186-194
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• 2005

A Spinning Rotor Gauge was calibrated between $4.04\times10^{-3}$ Pa and $1.11\times10^{-2}$ Pa at the high vacuum standard by static expansion method. The results were analysed according to the document of 'Guide to the Expression of Uncertainty in Measurement' of ISO. The expanded uncertainty was $3.0035\times10^{-3}$ Pa at $7.5448\times10^{-3}$ Pa. $95\%$ confidence level, and coverage factor of k = 1.

• Korean Journal of Food Science and Technology
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• v.40 no.2
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• pp.152-159
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• 2008

The purpose of this study was to determine the accurate quantification of vitamin A in infant formula by comparing two different standard stock solutions as well as various sample weights using high performance liquid chromatography. The sources of uncertainty in measurement, such as sample weight, final smaple vloume, and the instrumental results, were identified and used as parameters to determine the combined standard uncertainty based on GUM(guide to the expression of uncertainty in measurement) and the Draft EURACHEM/CITAC Guide. The uncertainty components in measuring were identified as standard weight, purity, molecular weight, dilution of the standard solution, calibration curve, recovery, reproducibility, sample weight, and final sample volume. Each uncertainty component was evaluated for type A and type B and included to calculate the combined uncertainty. The analytical results and combined standard uncertainties of vitamin A according to the two different methods of stock solution preparation were 627 ${\pm}$ 33 ${\mu}$g R.E./100 g for 1,000 mg/L of stock solution, and 627 ${\pm}$ 49 ${\mu}$g R.E./100 g for 100 mg/L of stock solution. The analytical results and combined standard uncertainties of vitamin A according to the various sample weighs were 622 ${\pm}$ 48 ${\mu}$g R.E./100 g, 627 ${\pm}$ 33 ${\mu}$g R.E./100 g, and 491 ${\pm}$ 23 ${\mu}$g R.E./100 g for 1 g, 2 g, and 5 g of sampling, respectively. These data indicate that the preparation method of standard stock solution and the smaple amount were main sources of uncertainty in the analysis results for vitamin A. Preparing 1,000 mg/L of stock solution for standard material sampling rather than 100 mg, and sampling not more than 2 g of infant formula, would be effective for reducing differences in the results as well as uncertainty.