• Title/Summary/Keyword: Standard C/T

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Development of Line Density Index for the Quantification of Oceanic Thermal Fronts (해양의 수온전선 정량화를 위한 선밀도 지수 개발)

  • Cho, Hyun-Woo;Kim, Kye-Hyun
    • Journal of the Korean Association of Geographic Information Studies
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    • v.9 no.2
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    • pp.227-238
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    • 2006
  • Line density index(LDI) was developed to quantify a densely isothermal line rate as standard index in the ocean environment. Theoretical background on the LDI development process restricting index range 0 to 100 was described. And validation test was done for the LDI application condition that total line length is not greater than 1/10 of unit area. NOAA SST(Sea Surface Temperature) data were used for the experimental application of LDI in the South Sea of Korea. Using GIS, $0.1^{\circ}C$ isothermal lines were linearized as vector data form SST raster data, and unit area were built as polygon data. For the LDI calculation, spatial overlapping(line in polygon) was implemented. To analyze the effect of unit area size for the LDI distribution, two cases of unit area size were designed and descriptive statistics was calculated including performing normality test. The results showed no change of LDI's essential characteristics such as mean and normality except for the range of value, variance and standard deviation. Accordingly, it was found that complex structure of thermal front and even smaller scale of front width than unit area size could influence on the LDI distribution. Also, correlation analysis performed between LDI and difference of temperature(${\Delta}T^{\circ}C$), and horizontal thermal gradient(${\Delta}T^{\circ}C/km$) on the front was obtained from linear regression model. This obtained value was compared with the results from previous researches. Newly developed LDI can be used to compare the thermal front regions changing spatio-temporally in the ocean environment using absolute index value. It is considered to be significant to analyze the relationship between thermal front and marine environment or front and marine organisms in a quantitative approach described in this study.

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The Evaluation of Recovery Rate of Radioimmunoassay Using Certified Reference Material (CRM) (인증표준물질(CRM)을 이용한 방사면역측정법의 회수율 평가)

  • Choi, Sung Hee;Shin, Sun Young;Lim, So Hee;Hong, Mee Kyung;Noh, Gyeong Woon;Kim, Jin Eui
    • The Korean Journal of Nuclear Medicine Technology
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    • v.18 no.1
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    • pp.158-162
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    • 2014
  • Purpose: Reference material (RM) is defined as material that is safe and homogeneous enough about specified characteristic that is made with a purpose of using test of measurement or nominal characteristic. Certified reference material (CRM), which is issued by authorized organization, is defined as reference material that provides characteristic value, link uncertainty and retroactivity. The purpose of this paper was to evaluate recovery of radioimmunoassay by Certified Reference Material enclosed with a certificate and therefore to enhance reliability of test. Materials and Methods: WHO certified reference material is purchased from NIBSC (National Institute for Biological Standard and Control, United Kingdom) and made of 3 levels that are C-1 (low concentration), C-2 (medium concentration) and C-3 (high concentration) and measured for kit at the Seoul National University Hospital. Recovery rate is evaluated after measurement at four different days. Results: Recovery rate results using WHO certified reference material are T4 90%, Ferritin 88%, PSA 94%, Prolactin 99%, AFP 94% and TSH 93%. Conclusion: A procedure that appropriate accuracy, precision, specificity, sensitivity, reproducibility, and validate on the subject of kit for radioimmunoassay is essential. Recovery rate assay as extraction efficiency of analysis process is percent about already measuring results of analysis result after all measuring process. This is very important assessment standards of performance evaluation of immunoassay kit. Recovery rate results of 6 type used WHO CRM are satisfactory to 88~99%. This demonstrates that the radioimmunoassay is a very accurate measurement, which is very effectively utilized in clinical practice.

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High-Pressure Synthesis and Chemistry of Amphibole Solid Solutions along the Joint Tremolite-Tschermakite (투각섬석-처마카이트 각섬석 고용체의 고압합성 및 화학적 성질)

  • 조문섭
    • Journal of the Mineralogical Society of Korea
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    • v.3 no.1
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    • pp.1-6
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    • 1990
  • Clacic amphiboles along the tremolite (Tr)-tschermakite(Ts) joint were synthesized using a piston-cylinder appratus. At 750-85$0^{\circ}C$and 12-2 kb, amphibole+corundum coexist with zoisite($\pm$talc, chlorite, and Mg-staurolite), but with anorthite($\pm$cholorite, spinel, pyroxenes, and sapphirine) at lower P. At 90$0^{\circ}C$, amphibole+corundum+clinopyroxene($\pm$anorthite, forsterite, sapphirine, and garnet) are stable over the P range 12-18 kb. These amphibole-bearing assemblages are replaced at high P by clcinopyroxene+talc+chlorite+zoisite at 650-75$0^{\circ}C$, and at higher temperatures by garnet+clinopyroxene($\pm$zoisite, orthopyroxene, and Mg-staurolite). Synthetic amphiboles with Ts>~45 mol% contain as much as 0.15 excess cations per formula unit(pfu) based on 23 oxygens(anhydrous formula), whereas less tschermakitic ones are deficient in cation occupancy by up to 0.18 pfu. This trend is attributed to the 야/trioctahedral substitution in Ca-amphiboles. Compositions of synthetic amphiboles display systematic changes with P and T governed by coexisting mineral assemblages. The Ts content (=[8-Si-Na]/2) increases with increasing T( Ts/ T=~0.1 nik% K-1) in the range 750-85$0^{\circ}C$, but remains nearly constant at 850-90$0^{\circ}C$. Pressure dramatically affects the Ts content of Ca-amphiboles:it increases with P at 8-12 kb( Ts/ T=2-3 mol% K-1), but significantly decreases at 12-21 kb( Ts/ P=-2.5 mol% Kb-1). Hence, the most tschermakitic amphiboles, containing 60$\pm$5 mol % Ts, or 1.2$\pm$0.1 tetrahedral Al, occur at 12 kb and 850-90$0^{\circ}C$. Compositions of Ca-amphiboles defined by a simple reaction, 3 Tr+2 zoisite+7 corundum+H2O=5 Ts, are reversed and used to estimate thermodynamic parameters of tschermakite assuming ideal mixing of Tr-Ts solid solutions. Predicted standard molal entropy and enthalpy of tschermakite are : S$^{\circ}$of Tr-Ts solid solutions. Predicted standard molal entropy and enthalpy of tschermakite are : S$^{\circ}$=566.9$\pm$13.7 J mol-1K, -1and H$^{\circ}$=-12518.36$\pm$15.17 kJ mol.-1

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Crystal and Block Structures of Hexagonal Ferrites (육방정 페라이트의 결정과 Block 구조)

  • Shin, Hyung-Sup
    • Journal of the Korean Ceramic Society
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    • v.49 no.3
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    • pp.205-215
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    • 2012
  • It has been studied the crystal and block structures of the hexagonal ferrites with M, W, Y and Z types prepared by various coprecipitation-oxidation method. The structures have been refined with a Rietveld analysis of the powder X-ray diffraction pattern with high precision ($R_{WP}$ <0.09, $R_I$ <0.03). The density difference between the S-blocks was proportioned to the cobalt contents in hexagonal ferrites, but that between the R or T-blocks was relatively small. Compared with the blocks and cation-oxygen polyhedra in BaM ($BaFe_{12}O_{19}$), those were bulky to the normal direction for the c-axis in $Co_2W$ ($BaCo_2Fe_{16}O_{27}$) and to the parallel direction for the c-axis in $Co_2Y$ ($Ba_2Co_2Fe_{12}O_{22}$) and $Co_2Z$ ($Ba_3Co_2Fe_{24}O_{41}$). The S-blocks of $Co_2W$, $Co_2Y$, and $Co_2Z$ were unstable and distorted. Because the T-block of $Co_2Z$ was unstable, the T-block was decomposed into the Ba-rich phase and $Co_2W$ at high temperatures above $1200^{\circ}C$. A standard powder X-ray diffraction pattern for $Co_2Z$ was proposed as well.

Prediction of Failure Behavior for Nuclear Piping Using Curved Wide-Plate Test (흰 광폭평판 시험을 이용한 원자력 배관의 파괴거동예측)

  • Huh, Nam-Su;Kim, Yun-Jae;Choi, Jae-Boong;Kim, Young-Jin;Lim, Hyuk-Soon;Chung, Dae-Yul
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.28 no.4
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    • pp.352-361
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    • 2004
  • One important element of the Leak-Before-Break analysis of nuclear piping is how to determine relevant fracture toughness (or the J-resistance curve) for nonlinear fracture mechanics analysis. The practice to use fracture toughness from a standard C(T) specimen is known to often give conservative estimates of toughness. To improve the accuracy, this paper proposes a new method to determine fracture toughness using a nonstandard testing specimen, curved wide-plate in tension. To show validity of the proposed curved wide-plate test, the J-resistance curve from the full-scale pipe test is compared with that from the curved wide-plate test and that from the C(T) specimen. It is shown that the J-resistance curve form the curved wide-plate tension test is similar to, but that from the C(T) specimen is lower than, the J-resistance curve from the full-scale pipe test. Further validation is performed by investigating crack-tip constraint conditions via detailed 3-D FE analyses, which shows that the crack-tip constraint condition in the curved wide-plate tension specimen is indeed similar to that in the full-scale pipe under bending.

Thermus caldophilus GK24로부터 내열성 $\beta$-galactosidase의 최적 생산

  • Yoo, Jinsang;Kim, Hyunkyu;In, Man-Jin;Kim, Min-Hong;Kwon, Suk-Tae
    • Microbiology and Biotechnology Letters
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    • v.25 no.3
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    • pp.298-304
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    • 1997
  • Thermus caldophilus GK24 was selected as sources of thermostable $\beta$-galactosidase from a survey of genus Thermus. T. caldophilus GK24 (Tca) $\beta$-galactosidase was found to be inducible. The enzyme was optimally active at 75$\circ$C. Enzyme induction was achieved by addition of lactose, galactose and cellobiose to basal media. The addition of glucose to culture media had a repressive effect on further enzyme synthesis. T caldophilus GK24 was tested for production of $\beta$-galactosidase by addition of various concentration of lactose, galactose and cellobiose to standard media. Cellobiose was found to be effective for the $\beta$-galactosidase induction. The optimal induction medium for production of $\beta$-galactosidase was composed of 0.2% cellobiose, 0.3% bactotryptone, 0.3% yeast extract, basal salts and Tris/HCI(pH 7.8). The activity of the enzyme in the optimal induction medium increased nearly 16.5-fold compared to the standard medium. Tca $\beta$-galactosidase was detected when cell extracts was subjected to electrophoresis in a nondenaturing polyacryamide gel and stained for activity with 6-bromo-2-naphtyl-$\beta$-D-galactopyranoside(BNG).

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Specimen Thickness and Crack Depth Effects on J Testing and Crack Tip Constraint for Non-standard Specimen (시편두께 및 균열깊이 영향을 고려한 비표준시편의 J 시험법 및 구속효과의 정량화)

  • Kim, Jin-Su;Cho, Soo-Man;Kim, Yun-Jae;Kim, Young-Jin
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.27 no.9
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    • pp.1531-1538
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    • 2003
  • This paper compiles solutions of plastic $\eta$ factors and crack tip stress triaxialites for standard and nonstandard fracture toughness testing specimens, via detailed three-dimensional (3-D) finite element (FE) analyses. Fracture toughness testing specimens include a middle cracked tension (M(T)) specimen, SE(B), single-edge cracked bar in tension (SE(T)) and C(T) specimen. The ligament-to-thickness ratio of the specimen is systematically varied. It is found that the use of the CMOD overall provides more robust experimental J estimation than that of the LLD, for all cases considered in the present work. Moreover, the J estimation based on the load-CMOD record is shown to be insensitive to the specimen thickness, and thus can be used for testing specimen with any thickness. The effects of in-plane and out-of-plane constraint on the crack tip stress triaxiality are also quantified, so that when experimental J value is estimated according to the procedure recommended in this paper, the corresponding crack tip stress triaxiality can be estimated. Moreover, it is found that the out-of-plane constraint effect is related to the in-plane constraint effect.

The Measurement of Electromagnetic Wave in Power Cable Tunnel of Underground Utility Tunnel (전력구 내 전자기파에 대한 작업 환경 측정)

  • Kang, Dae Kon;Park, Jai Hak
    • Journal of the Korean Society of Safety
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    • v.34 no.1
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    • pp.1-7
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    • 2019
  • Electromagnetic measurements of the power cable tunnel were conducted from August 10 to 20, 2018, in the ${\bigcirc}{\bigcirc}$ city underground utility tunnel. During this period, the average temperature was $31.89^{\circ}C$ and the humidity was 67.56% in power cable tunnel. As a result of the electromagnetic measurement, the highest electric field was 25.3 V/m and the magnetic flux density was $42.6{\mu}T$. The average electric field was 18.56 V/m and the magnetic flux density was $29.32{\mu}T$ in the power cable tunnel. As a result of comparison with the electric equipment technical standard, the electric field in the power cable tunnel was 0.5% of the electric equipment standard and 35.2% of the magnetic flux density. It's similar value that electric field is about robotic vacuum(15.53 V/m), and magnetic flux density is similar value about capsule- type coffee machine ($23.07{\mu}T$). The number of cable lines and the size of the electromagnetic waves were not proportional to each other through comparison of cable lines in the power cable tunnel. It was confirmed that 154 kV, rather than 22.9 kV, could have a greater influence on occupational.

EPMA quantification on the chemical composition of retained austenite in a Fe-Mn-Si-C-based multi-phase steel

  • Yoon‑Uk Heo;Chang‑Gon Jeong;Soo‑Hyun Kim;Gun‑Young Yoon;T. T. T. Trang;Youngyun Woo;Eun Yoo Yoon;Young‑Seon Lee
    • Applied Microscopy
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    • v.52
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    • pp.14.1-14.10
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    • 2022
  • An electron probe X-ray microanalyzer (EPMA) is an essential tool for studying chemical composition distribution in the microstructure. Quantifying chemical composition using standard specimens is commonly used to determine the composition of individual phases. However, the local difference in chemical composition in the standard specimens brings the deviation of the quantified composition from the actual one. This study introduces how to overcome the error of quantification in EPMA in the practical aspect. The obtained results are applied to evaluate the chemical com position of retained austenite in multi-phase steel. Film-type austenite shows higher carbon content than blocky-type one. The measured carbon contents of the retained austenite show good coherency with the calculated value from the X-ray diffraction.

$J_{c}$ control ofNb/$Al_{2}$$O_{3}$ /Nb Josephson junction (Nb/$Al_{2}$$O_{3}$ /Nb 조셉슨 접합의 임계전류밀도 제어)

  • 김규태;홍현권;이상길;이규원
    • Proceedings of the Korea Institute of Applied Superconductivity and Cryogenics Conference
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    • 2002.02a
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    • pp.10-12
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    • 2002
  • Single Josephson junctions of 50 $\mu$m $\times$ 50 $\mu$m were fabricated for several oxidation conditions to investigate controllabilities of critical current density ($J_{c}$) with the standard KRISS processes. Considering the self-field effect suppressing the observed critical current ($I_{c}$) at high $J_{c}$ region, we could reasonably estimate $J_{c}$ values from I-V observations. The dependence of the estimated $J_{c}$ as a function of exposure, which is equal to pressure(P) times time(t), was well fitted to a curve of $J_{c}$ ~ $(Pt)^{-0.36}$. The maximum $J_{c}$ value at the controllability margin was found to be 4 kA/$cm^{2}$ with the current equipment set up.

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