• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2006.09a
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• pp.49-50
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• 2006

[ $Ti(Al,\;O)-Al_2O_3$ ] composite powders were produced by high energy mechanical milling of a mixture of Al and $TiO_2$ powders followed by a combustion reaction. The powders were subsequently thermally sprayed on H13 steel substrates. Microstructural examination was conducted on the composite powders and thermally sprayed coatings, using X-ray diffractometry (XRD) and scanning electron microscopy (SEM). The performance of the coatings was evaluated in terms of micro-hardness and thermal fatigue. The thermally sprayed coatings performed very well in the preliminary thermal fatigue tests and showed no wetting tendency to molten aluminum.

• Journal of Powder Materials
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• v.30 no.5
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• pp.424-430
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• 2023

YAG phosphor powders were fabricated by the atmospheric plasma spraying method with the spray-dried spherical YAG precursor. The YAG precursor slurry for the spray drying process was prepared by the PVA solution chemical processing utilizing a domestic easy-sintered aluminum oxide (Al₂O₃) powder as a seed. The homogenous and viscous slurry resulted in dense granules, not hollow or porous particles. The synthesized phosphor powders demonstrated a stable YAG phase, and excellent fluorescence properties of approximately 115% compared with commercial YAG:Ce³⁺ powder. The microstructure of the phosphor powder had a perfect spherical shape and an average particle size of approx imately 30 ㎛. As a result of the PKG test of the YAG phosphor powder, the synthesized phosphor powders exhibited an outstanding luminous intensity, and a peak wavelength was observed at 531 nm.

• Proceedings of the KWS Conference
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• 2001.10a
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• pp.220-222
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• 2001

The average grain size, the grain-size distribution, the morphology and the microstructure are fundamental characteristics of a spraying powder. Now that the significance of the grain size for the pattern of properties of the powder has been recognised, greater consideration is also being given to it in standards and regulations. However, unfortunately, the processes according to which the grain size and the grain-size distribution must be determined are specified in the rarest of cases. The contribution therefore dealt with the comparison of different particle-size measuring techniques, such as diffraction spectroscopy, sedimentation, sieving and microscopic measurement. The comparability of the measured results was investigated on twelve plasma spraying powders with different compositions, nominal sizes and morphologies.

• Journal of the Korean institute of surface engineering
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• v.29 no.6
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• pp.695-702
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• 1996

Plasma spraying process was employed to produce HA coating on Ti6A14V alloy for the development of a dental implant. The goal of this research was to find optimum spraying conditions for HA coating on Ti6Al4V. This study was thus designed carefully to evaluate how spraying parameters affect various physical properties of a HA coating layer, such as phase composition and bond strength. In plasma spraying, spraying parameters such as hydrogen flow rates and spraying distances were varied systematically to change the degree of the melting of starting HA powder in plasma jet. It was revealed that the deposition efficiency increased with increasing a hydrogen flow rate, and the bond strength between the HA-coated layer and Ti-alloy substrate increased with hydrogen flow rate, but decreased with spraying distance. Therefore, the hydrogen flow rate and the spraying distance should be carefully controlled to obtain the reasonable bond strength simultaneously.

• Korean Journal of Materials Research
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• v.11 no.11
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• pp.965-971
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• 2001

The objective of this study is to investigate the characteristics - microstructure, hardness, adhesive strength and friction coefficient - of the coatings with aging - treatment after optimizing internal- plasma spraying parameters for Al-30wt%Si powder as a basic research to manufacture the cylinder block bore for Al engine composed of Al-30wt%Si alloy on Al alloy, The optimum internal-plasma spraying parameters of Al-30wt%Si alloy are summarized as follows: voltage: 37.5V, current: 160A, working distance: 25mm, gun traverse speed: 4.5mm/s, rotating speed: 518m/min. The primary Si particles grew aggressively with increasing heat-treating temperature. The hardness of the as-sprayed coating was about Hv=275 but this value was abruptly decreased with increasing heat-treating temperature. And average friction coefficient of the coating was below 0.08 after heat treatment for 48h at $175^{\circ}C$.

• Journal of Welding and Joining
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• v.7 no.3
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• pp.55-62
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• 1989

Variation of the spray droplet velocity with spraying distance and the microstructural characteristics of spray deposits fromed by oxy-fuel thermal spraying with Ni-base alloy powder contained chrome boride for hard facing were examined. Measurements of spray droplet velocity as a function of distance from the nozzle tip were inexcellent agreement with computer simulated predictions. Optimum condition for thermal spray deposits in this experiment was found to be under #10kg/cm^2$ of acceleration gas pressure with 15cm of spraying distance. Fine microstructure and higher microhardness of the initial part of the deposits due to rapid solidification were found to be able to maintained in a thickness up to 0.4mm, and this initial microstructure and properties could be maintained throughout the thickness of a thick spray deposits by performing the multipass spraying with 0.4mm thickness of each pass.

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2006.09a
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• pp.156-157
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• 2006

The preparation of composite powders for plasma spraying by an in-house designed mechanofusion process is investigated. Results show that dry particle coating depends on the chemical and mechanical properties of powders. In metal/oxide and metal/oxide/carbide powder mixtures, fine ceramic particles coat the surface of the metallic coarser particles. A nearly rounded shape of the final composite particles is induced by the mechanical energy input with no formation of new phases. However with the carbide/metal powdered system, only an intimate mixture of components is achieved. It is suggested that the coating mechanism is governed by agglomeration and rolling phenomena.

• Proceedings of the KWS Conference
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• 2001.10a
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• pp.99-102
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• 2001

• Journal of Power System Engineering
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• v.1 no.1
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• pp.70-79
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• 1997

Ni-base self-fluxing alloy powder particles were flame sprayed onto the SS400 mild steel substrate surface. The effects of both substrate temperature and spraying distance on the splat behavior of sprayed particles were examined. The results obtained are summarized as follows: 1) In the splat behavior of Ni-base self-fulxing alloy particles sprayed onto the SS400 mild steel substrate, splashing was observed under the room temperature condition. On the contrary, it showed circular plate pattern in the substrate temperature range over 373K. 2) It was cleared that there was close relationship between mechanical properties of coating layer and splat behavior of sprayed particles. 3) From the experimental results, optimum spraying conditions showed excellent mechanical properties in the case of Ni-base self fluxing alloy sprayed onto the SS400 mild substrate were 473K of substrate temperature and 250mm of spraying distance.

• Journal of the Korean institute of surface engineering
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• v.35 no.1
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• pp.5-10
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• 2002

This study was performed to investigate the influence of spraying condition to the coating layer properties of Fe-Cr-Ni-Mo-Si-B alloy using the HVOF. The investigations, such as thickness measurement, surface roughness, hardness, friction coefficient, resistance of corrosion were carried out. Matrix is prepared by gritting and coating layer is made of Fe-Cr-Ni-Mo-Si-B alloy powder using HVOF. Alumina gritting layers are superior to steel gritting layers. The less spaying distance, the more coating layer properties confirmed. The optimum spraying condition, in this study, was proved as 13inch spraying distance with feed rate 350rpm (78g/min).