• 청정기술
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• 제2권1호
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• pp.80-95
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• 1996

반건식 배연탈황공정에서 사용되는 spray dryer absorber(SDA)에 대한 수치모사를 행하였다. 기본 방정식으로는 기체와 액적의 각 성분들의 물질수지식, 에너지수지식과 액적의 운동 방정식등이 포함되었다. 만들어진 모델은 대부분이 기존의 SPRAYMOD-M보다 실제의 pilot plant data를 더 잘 모사하였다. 실제 pilot plant에서 사용되는 값의 범위 내에서 선정된 공정변수가 SDA의 성능에 미치는 효과를 계산하고, 이를 $SO_2$의 흡수속도, 배연기체의 체류시간, 그리고 액적의 건조시간 및 속도 등에 의해 검토하였다. 또 $SO_2$ 제거율을 두 개의 독립된 공정 변수의 함수로 구하였으며, 그 결과를 3차원 또는 2차원의 등가선으로 표시하여 SDA의 설계에 쉽게 적용될 수 있도록 하였다.

• 한국세라믹학회지
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• 제41권12호
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• pp.873-879
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• 2004

In all major industries ranging from powder industries and advanced ceramics, to the food and pharmaceutical manufacture powder industries, the main production process is the spray dryers. In this paper, a systematic approach is used and six rules are obtained for the basis of the fuzzy model. A fuzzy model is based on the past behavior of the target system and expected to be able to reproduce the behavior of the target system. The output of the developed fuzzy model shows, graphically and statistically, a high level of face validity. Therefore, it is concluded that the developed fuzzy model mimics the actual process and can be considered, with confidence, as a reliable model to study, analyze, and improve the existing process.

• 대한기계학회논문집B
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• 제22권8호
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• pp.1064-1072
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• 1998

The evaporation of sludge particles in a sludge dryer has been numerically investigated with commercial CFX4.1 code. Gas flow field, gas temperature field, sludge particle trajectories, and the moisture content variation of sludge particles are calculated fort various influencing factors, i. e., gas swirl velocity, initial particle distribution, gas temperature. Evaporation of sludge particles increases with gas swirl velocity, several supplying positions, and gas temperature, respectively due to increased residence time, increased contacting surface area, and increased temperature difference between gas and particle.

• 한국식품과학회지
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• 제41권1호
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• pp.27-31
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• 2009

식품의 원료인 참기름을 캡슐화하기 위해 전보(11)에서 최적화한 model system을 기초로 피복물질을 선정하고 이에 3%의 gellan gum을 첨가한 후 유화압력을 20.7 MPa로 하여 유화액을 제조하였다. 이를 top spray dryer와 fluidized bed granulator에 의한 공정으로 캡슐을 제조하여 캡슐화 수율, surface oil, 수분함량, 입자 크기, 캡슐의 저장 안정성 및 제품 응용성을 비교하였다. Fluidized bed granulator에 의한 캡슐은 top spray dryer에 의한 캡슐보다 상대적으로 surface oil 함량이 낮고 수율이 높으며 입자 크기가 컸다. 제조한 캡슐을 $37^{\circ}C$에서 저장하면서 flavor retention을 측정한 결과 참기름 원료 자체를 저장한 경우 향기 성분은 1% 이하의 잔존 함량을 나타내어 대부분의 향기 성분이 소실되었다고 보았으나, top spray dryer와 fluidized bed granulator에 의한 캡슐은 각각 37%, 42%의 향기성분을 보유하여 향기 성분 포집성 및 보존성이 우수하였다. 또한 쇠고기 죽 제품에 응용한 후 관능검사 결과에서도 참기름 캡슐을 사용한 제품들이 모두 참기름 원료 자체를 사용한 제품보다 풍미의 강도 및 기호도면에서 모두 높았고 특히 fluidized bed granulator를 이용하여 제조한 캡슐을 사용한 제품이 가장 우수하게 평가되었다. 따라서 참기름 원료와 같이 향기 성분이 소실 되기 쉬운 소재를 fluidized bed granulator를 이용하여 저온 미세 캡슐화하면 풍미의 안정성 증대에 효과가 있을 것으로 판단된다.

• Journal of Microbiology and Biotechnology
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• 제15권6호
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• pp.1178-1182
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• 2005

Survival of thermotolerant Lactobacillus reuteri KUB-AC5 in $20\%$ (w/v) skim milk was found to be $11.3\%$ after spray drying by using a pilot scale spray dryer with inlet temperature at $170^{\circ}C$ and outlet temperature at $85^{\circ}C$. The ability of dried cell to produce antimicrobial activity was not affected by the spray drying. The model system for predicting viability of spray-dried L. reuteri KUB-AC5 during long-term storage was established, based on the Arrhenius equation, and verified by experimental data, because the viability of cells during storage can be correlated with storage temperature. The viability during storage at $30^{\circ}C$ declined more rapidly than that storage at $4^{\circ}C$.

• Journal of Biosystems Engineering
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• 제17권3호
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• pp.229-236
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• 1992

In an effort to localize the spray-dryer which is markedly used for drying food materials, a experiment was carried out with a wheel type atomizer locally designed and manufactured to evaluate the effect of rotational speed, feed rate and physical properties of liquid food material on the droplet size, and to develop a model to predict the droplet size sprayed at various operational conditions. The result are summarized as follows. 1. The frequency of droplet size sprayed from the atomizer at every treatment were similar to normal distributions. 2. Under the test conditions adopted in this study, that is, rotational speed of the atomizer ranging from 15,000 to 20,000 rpm (55.0 m/sec - 73.3 m/sec), feed rate from 14 to 37 kg/hr and viscosity of the material from 1.14 to 350 cP, the mean volume-surface dia. of droplets was decreased as increase in rotational speed and was not affected significantly by the feed rate and viscosity. 3. Through the dimensional analysis, a prediction model was developed as follows : $$\frac{Dvs}{r}=K[\frac{Q}{{\mu}r}]^a[\frac{rN^2}{g}]^b[\frac{{\rho}^2r^3g}{{\mu}^2}]^c[\frac{L}{r}]^d$$ and it was proved that the above model was better in degree of fitness than other models reported. 4. A prediction equation for the droplet size sprayed from the atomizer under the test was expressed as follows : $$\frac{Dvs}{r}=0.0215[\frac{Q}{{\mu}r}]^{0.06}[\frac{rN^2}{g}]^{0.3314}[\frac{{\mu}^2}{{\rho}^2r^3g}]^{0.0158}$$.

• 한국대기환경학회지
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• 제6권1호
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• pp.85-96
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• 1990

Simultaneous removal efficiencies of hydrophilic and hydrophobic gaseous pollutants are experimentally determined, and the macroscopic removal mechanism of pollutants in a dry scrubber is analyzed using the extended model of three phase equilibrium distribution of pollutant at high temperatures that can describe the different morphological conditions of adsorbent and water at varying relative humidities. For the simplicity, the inside of spray dryer is divided into three regions of ; (1) absorption, (2) three-phase equilibrium, and (3) adsorption, and the removal efficiencies of each pollutants at three regions are observed at different experimental conditions to estimate the effects of important parameters of dry scrubber. The laboratory experiments simulate the three regions of spray dryer with the temperature control and thus evaporation rate of water from the slurry particle. $SO_2$ as a hydrophilic gaseous pollutant and vinyl chloride as a hydrophobic toxic gas are selected for the future field application to soid waste incineration, and the two types of slurry are made of the two sorbents ; 10 wt.% $Ca(OH)_2$, and 10 wt.% NaOH. Result of temperature effect shows the height of absorption plus three-phase region is decreased as the operation temperature is increased, which results in the lower removal efficiency of $SO_2$ but higher removal for vinyl chloride in the adsorption region of dry scrubber. The removal efficiency of $SO_2$ is higher by NaOH slurry than by $Ca(OH)_2$ slurry due to the hygroscopic nature of NaOH, while the removal of vinyl chloride is higher in $Ca(OH)_2$ case. From the analysis of redults using three-phase equilibrium distribution model, the effective two-phase partition coefficients can be obtained, and the possible extention in the application of the three-phase equilibrium model in a dry scrubber design has been demonstrated.

• Journal of Microbiology and Biotechnology
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• 제27권4호
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• pp.768-774
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• 2017

Horseradish peroxidase (HRP) catalyzes the oxidation of aromatic compounds by hydrogen peroxide via insoluble polymer formation, which can be precipitated from the wastewater. For HRP immobilization, poly(lactic-co-glycolic acid) (PLGA) fine carrier supports were produced by using the Nano Spray Dryer B-90. Immobilized HRP was used to remove the persistent 2,4-dichlorophenol from model wastewater. Both extracted (9-16 U/g) and purified HRP (11-25 U/g) retained their activity to a high extent after crosslinking to the PLGA particles. The immobilized enzyme activity was substantially higher in both the acidic and the alkaline pH regions compared with the free enzyme. Optimally, 98% of the 2,4-dichlorophenol could be eliminated using immobilized HRP due to catalytic removal and partly to adsorption on the carrier supports. Immobilized enzyme kinetics for 2,4-dichlorophenol elimination was studied for the first time, and it could be concluded that competitive product inhibition took place.

• Journal of Pharmaceutical Investigation
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• 제32권3호
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• pp.191-197
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• 2002

Polymer based physical mixtures or solid dispersions containing solubilizing compositions[OA, tween80 and SLS] were prepared using a spray-dryer. Lovastatin(LOS), simvastatin(SIMS), aceclofenac(AFC) and cisapride(CSP) were selected as poorly water-soluble drugs. Dextrin, poly(vinylalcohol) (PVA), poly(vinylpyrrolidone)(PVP) and polyethylene glycol(PEG) were chosen as solubilizing carriers for solid dispersions. The solid dispersions containing solubilizing compositions without drug were prepared without using organic solvents or tedious changes of formulation compositions. This system could be used to quickly screen the dissolution profiles of poorly water-soluble drugs by simply mixing with drugs thereafter. In case of solid dispersion containing drug, organic solvent systems could be used to solubilize model drugs. The dissolution rates of the drugs were higher when mixed with drug and solid dispersions containing solubilizing compositions. However, solid dispersions of LOS, AFC, and CSP simultaneously containing drug and solubilizing compositions in organic solvent systems were more useful than physical mixtures of drug and solid dispersions without drug except SIMS. Based on solubilizing capability of polymer based physical mixtures in gelatin hard capsules, optimal solid dispersion system of poorly water-soluble drugs could be formulated. However, it should be noted that dissolution rate of poorly water-soluble drugs were highly dependent on drug properties, solubilizing compositions and polymeric carriers.

• Journal of Microbiology and Biotechnology
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• 제29권12호
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• pp.1982-1992
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• 2019

The alkaliphilic, calcium carbonate precipitating Bacillus sp. strain AK13 can be utilized in concrete for self-repairing. A statistical experimental design was used to develop an economical medium for its mass cultivation and sporulation. Two types of screening experiment were first conducted to identify substrates that promote the growth of the AK13 strain: the first followed a one-factor-at-a-time factorial design and the second a two-level full factorial design. Based on these screening experiments, barley malt powder and mixed grain powder were identified as the substrates that most effectively promoted the growth of the AK13 strain from a range of 21 agricultural products and by-products. A quadratic statistical model was then constructed using a central composite design and the concentration of the two substrates was optimized. The estimated growth and sporulation of Bacillus sp. strain AK13 in the proposed medium were 3.08 ± 0.38 × 10⁸ and 1.25 ± 0.12 × 10⁸ CFU/ml, respectively, which meant that the proposed low-cost medium was approximately 45 times more effective than the commercial medium in terms of the number of cultivatable bacteria per unit price. The spores were then powdered via a spray-drying process to produce a spore powder with a spore count of 2.0 ± 0.7 × 10⁹ CFU/g. The AK13 spore powder was mixed with cement paste, yeast extract, calcium lactate, and water. The yeast extract and calcium lactate generated the highest CFU/ml for AK13 at a 0.4:0.4 ratio compared to 0.4:0.25 (the original ratio of the B4 medium) and 0.4:0.8. Twenty-eight days after the spores were mixed into the mortar, the number of vegetative cells and spores of the AK13 strain had reached 10⁶ CFU/g within the mortar. Cracks in the mortar under 0.29 mm were healed in 14 days. Calcium carbonate precipitation was observed on the crack surface. The mortar containing the spore powder was thus concluded to be effective in terms of healing micro-cracks.