• Natural Product Sciences
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• 제20권4호
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• pp.243-250
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• 2014

A simple GC method with a FID detector was developed in order to determine two main compounds (${\beta}$-sitosterol and lupenone) for Adenophorae Radix. ${\beta}$-Sitosterol and lupenone were analyzed by the gradient thermal ramping method. Nitrogen was used as the carrier gas at 108 kPa. The flow rate of gas was 2.0 mL/min; $2{\mu}L$ of filtered sample was injected at a split ratio of 1 : 80. This method was fully validated with respect to linearity, precision, accuracy and robustness. Further, this GC-FID method was applied successfully in order to quantify two compounds in an Adenophorae Radix extract. The GC analytical method for classification analysis was performed by repeated analysis of 59 reference samples in order to differentiate between Adenophora triphylla var. japonica Hara and 14 Codonopsis lanceolata. The results indicate that the GC-FID method is suitable and reliable for the quality evaluation of Adenophorae Radix.

• 한국연소학회지
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• 제8권3호
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• pp.15-23
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• 2003

Partial quenching structure of turbulent diffusion flames in a turbulent mixing layer is investigated by the method of flame hole dynamics in order to develop a prediction model for turbulent flame lift off. The essence of flame hole dynamics is derivation of the random walk mapping, from the flame-edge theory, which governs expansion or contraction of flame holes initially created by local quenching events. The numerical simulation for flame hole dynamics is carried out in two stages. First, a direct numerical simulation is performed for constant-density fuel-air channel mixing layer to obtain the turbulent flow and mixing fields, from which a time series of two dimensional scalar dissipation rate array is extracted at a fixed virtual flame surface horizontally extending from the end of split plate to the downstream. Then, the Lagrangian simulation of the flame hole random walk mapping projected to the scalar dissipation rate array yields temporally evolving turbulent extinction process and its statistics on partial quenching characteristics. The statistical results exhibit that the chance of partial quenching is strongly influenced by the crossover scalar dissipation rate while almost unaffected by the iteration number of the mapping that can be regarded as a flame-edge speed.

• 소성∙가공
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• 제21권8호
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• pp.473-478
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• 2012

The yoke, a component of conventional motor-driven power steering system, often contains welding defects from its manufacturing process. To eliminate these defects, the precision cold forging process has been tried. In this study, the double-action complex forging has been used to manufacture a torsion joint yoke. The backward extrusion proved faster than the forward extrusion in forging of the product. The double-action complex forging process utilized an upper die composed of a punch, a punch guide, a disc spring and a coil spring. The forged material pushes up the punch guide, and then the disc spring and the coil spring balances the backward extrusion force. Consequently, the flow of material was essentially in the forward direction, resulting in a successful forging operation. The forging load of Al 6061-T6 was higher than that of the automotive structural hot rolled plate.

• Progress in Superconductivity
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• 제3권1호
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• pp.28-30
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• 2001

We studied the flux-flow current-voltage characteristics of microwave-generated fluxons formed in serially stacked intrinsic Josephson junctions fabricated on$ HgI_2$-intercalated $Bi_2$$Sr_2$$CaCu_2$O/8+x/(Bi2212) single crystals. With increasing the irradiation power of 73$\square$76 GHz microwave, the supercurrent branch became resistive and split into multiple sub -branches. Each sub-branch represented a specific mode of collective motion of Josephson fluxons. We also observed similar branch splitting In a mesa prepared on an underdoped Bi2212 single crystal in a static magnetic field.

• 대한기계학회논문집B
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• 제32권9호
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• pp.704-711
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• 2008

Integrated gasification combined cycle (IGCC) is an environment friendly method of using coal. Several commercial IGCC plants have been built worldwide during the past decade, and a domestic development project has also been launched recently. Operation and performance characteristics of a gas turbine in the IGCC plant deviates from those of original gas turbines due to several factors such as increased amount of fuel supply and integration with other components. In this study, performance of a gas turbine in the IGCC plant is analyzed considering its integration with the air separation unit (ASU). Influence of the degree of integration (split of air supplies to ASU from the auxiliary compressor and the gas turbine compressor) on the system performance is investigated. In addition, effect of modulating nitrogen return flow from the gasifier to the gas turbine on the operating characteristics of the gas turbine is examined.

• Advances in concrete construction
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• 제4권1호
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• pp.49-69
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• 2016

This work investigates the mechanical properties of conventional concrete (CC) and self compacting concrete (SCC) using fine rubber and silpozz were accompanied by a comparative study between conventional rubberized concrete (CRC) and self compacting rubberized concrete (SCRC). Fine rubber (FR) from scrap tires has replaced the fine aggregate (FA) and Silpozz has been used as a replacement of cement at the proportions of 5, 10 and 15%. Silpozz as a partial replacement of cement in addition of superplasticiser (SP) increases the strength of concrete. Fresh concrete properties such as slump test, compaction factor test for CRC, whereas for SCRC slump flow, $T_{500}$, V-funnel, L-box, U-box, J-ring tests were conducted along with the hardened properties tests like compressive, split tensile and flexural strength test at 7, 28 and 90 days of curing. The durability and microstructural behavior for both CRC and SCRC were investigated. FR used in the present study is 4.75 mm passing with fineness modulus 4.74.M30 grade concrete is used with a mix proportion of 1:1.44:2.91 and w/c ratio as 0.43. The results indicate that as FR quantity increases, workability of both CRC and SCRC decreases. The results also show that the replacement of natural fine aggregate (NFA) with FR particles decreases the compressive strength with the increase of flexural strength observed upto 5% replacement of FR. Also replacement of cement with silpozz resulted enhancement of strength in SCRC.

• Computers and Concrete
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• 제23권1호
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• pp.37-47
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• 2019

In view of the increasing utility of concrete as a construction material, the major challenge is to improve the quality of construction. Nowadays the common problem faced by many of the concrete plants is the shortage of river sand as fine aggregate material. This led to the utilization of locally available materials from quarries as fine aggregate. With the percentage of fines present in Crushed Rock Fines (CRF)or crushed sand is more compared to river sand, it shows a better performance in terms of fresh properties. The present study deals with the formulation of SCC mix design based on the chosen plastic viscosity of the mix and the measured plastic viscosity of cement pastes incorporating supplementary cementitious materials with CRF and river sand as a fine aggregate. Four different combinations including two binary and one ternary mix are adopted for the current study. Influence of plastic viscosity of the mix on the fresh and hardened properties are investigated for SCC mixes with varying water to cement ratios. It is observed that for an increasing plastic viscosity of the mix, slump flow, T500 and J-ring spread increased but V-funnel and L-box decreased. Compressive, split tensile and flexural strengths decreased with the increase in plastic viscosity.

• Nuclear Engineering and Technology
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• 제56권4호
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• pp.1125-1134
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• 2024

This paper presents a validation study of the subchannel analysis code SLTHEN used for the core thermal-hydraulic design of the Prototype Gen-IV sodium-cooled fast reactor (PGSFR). To assess the performance of the ENERGY model of SLTHEN, four liquid metal heating experiments conducted by ORNL, WARD, and KIT with hexagonal assemblies of wire-wrapped rod bundles were analyzed. These experiments were performed with 19-and 61-pin bundles and varying power distributions of axial and radial peaking factors up to 1.4 and 3.0, respectively. The coolant subchannel temperatures measured at different axial locations were compared with the SLTHEN predictions with the Novendstern, Chiu-Rohsenow-Todreas (CRT), and Cheng-Todreas (CT) correlations for flow split and mixing in wire-wrapped pin bundles. The results showed that the SLTHEN predicts the measured subchannel temperatures reasonably well with root-mean-square errors of ~10 % and maximum errors of ~20 %. It was also observed that the CRT and CT correlations consistently outperform the Novendstern correlation.

• Journal of Oral Medicine and Pain
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• 제30권3호
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• pp.375-381
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• 2005

기존의 치과용 핸드피스를 대체할 수 있는 효과적인 치아 삭제 방법인 Er:YAG 레이저를 이용하여 보다 효과적으로 치아를 삭제하기 위해 여러 가지 변수들, 즉 펄스에너지, 조사반복율 및 레이저 조사 동안의 물분사량에 대한 다양한 연구가 진행되어 왔다. 특히 이 중에서도 물분사량은 삭제 효율이 높이면서 치수를 보호할 수 있는 중요한 요소로 여겨지고 있다. 레이저 조사 동안 분사되는 물의 양이 적으면 치아에 균열이나 탄화를 유발하고 치수손상을 야기할 수 있는 위험이 있는 반면, 물의 양이 지나치게 많으면 삭제효율이 저하되고 레이저 시술동안 치과의사의 시야확보를 방해할 수 있으므로, 조사조건에 따른 가장 적절한 물 분사량을 결정하는 것이 아주 중요하다. 본 연구에서는 특정조사조건에서 치아법랑질 삭제에 가장 효과적인 물분사량을 결정하고, 그 물분사량을 적용하였을 때 치수내에서 발생하는 온도변화를 측정하여 안전성 여부를 함께 평가하고자 하였다. 발거된 건전치아를 표본으로 하여, 20 Hz의 조사반복율, 200 mJ 및 300 mJ의 펄스에너지의 조사조건에서 1.6, 3.0, 5.0, 7.0, 10.0 ml/min의 서로 다른 물분사량을 적용하여 치아삭제 효과를 평가하였다. 이때 레이저 조사시간은 3초로 고정하였다. 삭제효율은 조사 전후의 치아무게를 측정하여 그 차이로 결정하였으며 온도측정을 위해서는 별도의 치아를 준비하여 온도측정장치를 조사측과 반대측의 치수벽에 위치하여 레이저조사 동안의 온도변화를 추적하였다. 실험결과, 200 mJ과 300 mJ 모두에서 1.6 ml/min의 가장 적은 물분사량이 치아삭제효율이 가장 좋았다. 또한 이 조건에서의 온도변화를 측정한 경우에도 치수손상을 일으키지 않을 정도의 미미한 온도상승만을 보여주었다. ANOVA 분석의 결과 조사부위(조사측과 비조사 반대측)에 따른 유의한 차이가 나타났으나(p<0.05), 펄스에너지에 따라 각각 비교하였을 때는 유의한 차이를 보여주지 않았다. 그러므로 본 실험의 결과에 따르면, 1.6 ml/min의 비교적 적은 양의 물을 레이저 조사시에 함께 분사해 준다면 200$\sim$300 mJ의 펄스에너지, 20 Hz의 조사반복율, 3초의 레이저조사시간이라는 조건에서는 치수손상을 일으키지 않는 안전한 범위에서 가장 효과적으로 치아를 삭제할 수 있을 것으로 생각된다.

• 분석과학
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• 제27권1호
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• pp.34-40
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• 2014

SPLITT 분획법(Split-flow thin cell fractionation, SF)은 입자성 물질이나 거대분자를 크기에 따라 연속적으로 분획할 수 있는 유용한 기술이다. SF에서는 얇은 리본 모양 채널의 입구와 출구에 존재하는 흐름분할기(flow stream splitter)에 의하여 시료의 분리가 이뤄진다. 대용량 중력장 FFD-SF 시스템(New large scale splitter-less FFD-SF system)은 흐름분할기를 사용하지 않고, 전액공급 모드(FFD mode) 로 작동하도록 디자인되었다. 전액공급 모드는 용매의 공급 없이 시료만을 채널 내로 주입함으로써 시료의 희석을 방지할 수 있는 장점을 가진다. 본 연구에서는 산업용 polyurethane (PU)입자를 시료로 이용하여, FFD-SF 장치의 성능에 미치는 시료의 주입유속과 채널두께의 영향을 확인하였다. Carrier 용액으로는 시료간 응집과 박테리아 생성을 방지하기 위하여 0.1% FL-70와 0.02% sodium azide ($NaN_3$)를 함유하는 수용액을 사용하였다. 시료농도는 0.02% (wt/vol)로 고정, 주입 양은 4.2~7.2 L/hr, 채널두께는 $900{\sim}1300{\mu}m$의 범위에서 실험하였다. 분획효율(Fractionation efficiency, FE)은 optical microscopy (OM)을 사용하여 입자의 수를 확인하여 계산하였으며, 시료회수율(sample recovery)은 membrane filter를 이용하여 분획된 시료의 무게로부터 계산하였다. 채널두께가 두꺼울수록 fraction-a의 분획효율이 증가하였고, 유속이 증가할수록 fraction-b의 분획효율 증가하였다. 시료회수율은 평균 95%를 보였다. 본 연구 결과는 새로운 splitter-less FFD-SF system은 다양한 마이크론 크기의 입자의 분획에 유용한 방법임을 보여준다.