• Journal of the Korean Ceramic Society
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• v.34 no.10
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• pp.1037-1044
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• 1997

Mechanical properties and water stability of HAC/PVA based MDF cement composite were investigated using polyurethane(PU) resin, silane coupling agent and various PVA. The results were as follows ; The flexural strength of MDF cement composite increased as increasing with PVA content. Low-viscosity PVA developed higher flexural strength than high-viscosity PVA under a drying curing condition. But the strength of water immersed specimen decreased. Water stability of MDF cement improved as increasing with content of PU. Consequently, water stability of polyurethane 7% added MDF cement was about 2 times higher than that of the controlled specimen. Furthermore, the strength and water stability of diamine group based silane couling agent in using MDF cement increased and improved dramatically.

• Korean Journal of Clinical Laboratory Science
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• v.45 no.1
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• pp.5-8
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• 2013

In the specimen of free PSA in the low concentration, the result in % bias from our institution and comparable evaluation institution was -33.7% which is exceeded % bias ${\pm}20%$ ; however, it was the domestically allowable limit recommended by the laboratory accreditation commission for specimen at the low concentration. In this paper, the cause was accredited by instability of free PSA substance within the specimen, and the specimen stability test was performed according to CLSI documents GP29-A2. After the low and high concentration specimen were made, and rapidly cooled down in a deep freezer with $-30^{\circ}C$, serum of two concentrations was measured for 10 consecutive days with 3 times a day by Architect i2000 and observed a change in the mean value. As the results of two groups, there were changes in the established target value, and a change level was evaluated by calculating it with % bias. The low concentration specimen had no significant reduction until the 4 day lapse in cold storage. However, % bias were reduced by -17.5% from the 5 day lapse, by 21.5% after the 7 day lapse, and by -26.9% after the 9 day lapse. The frozen specimen had only intra-day variation for 10 days. In the high concentration specimen, bias began to show as -12.2% from the 3 day lapse in cold storage. There was reduction by -28.9% from the 5 day lapse, by -39% after the 7 day lapse, and by -42.9% after the 9 day lapse. In the frozen specimen, there was only intra-day variation like the low concentration specimen in cold storage.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2000.07a
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• pp.881-884
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• 2000

Recently mobile communication fields need piezoelectric ceramic resonators and filters as possible as small. The length-extensional vibration mode of a rectangular piezoelectric cesamic plate has the advantage of the small size, but the mode has not been studied sufficiently because it was not used extensively until now. In this paper, PZT + x[wt%l $Cr_20_3$ ceramics with rhombohedra1 phase were fabricated. And temperature stability for the mode of the ceramic specimen was investigated. Contrary to our expectations, addition of the stabilizer, $Cr_20_3$ did not promote the temperature stability for the mode in the PZT ceramic specimen with rhombohedra1 phase.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.14 no.12
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• pp.979-986
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• 2001

This paper was researched the effect of slurry stability on the mechanical and electrical property of the porcelain insulator with various raw materials such as feldspar, quartz, clay and l7wt% alumina. The slurry was fabricated after ball milling the mixed raw materials. Green compacts were made by the extrusion and were sintered at 1300$\^{C}$ for 60min in the tunnel kiln. All of the specimens were densified 96% of the theoretical density. The 3-point flexural strength($\sigma$$\_$B/) of the specimen stabilized slurry pH 7.8 was 1650 k9/㎠ and the vickers hardness(Hv) and the fracture toughness(K$\_$IC/) were 27.5 GPa and 2.2 MPa$.$m$\^$$\sfrac{1}{2}$/, respectively. The mechanical properties of the specimen stabilized slurry PH 9.3 were 1716 kg/㎠($\sigma$$\_$B/), 27.6 GPa(Hv) and 3.0 MPa$.$m$\^$$\sfrac{1}{2}$/(K$\_$IC/), respectively. The dielectric strength was increased from 8.3kV/mm to 13.2kV/mm as the increase of the slurry pH from 7.8 to 9.3. Therefore the physical properties of the specimen stabilized slurry pH 9.3 were improved.

• Composites Research
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• v.12 no.3
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• pp.84-90
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• 1999

High alumina cement(HAC) and polyvinyl alcohol(PVA) based macro-defect-free(MDF) cement composites were reinforced using short carbon fibers, 3mm in length, 1-4% in weight fraction and insoluble polymers such as polyurethane, epoxy, phenol resin, in order to increase mechanical properties and water stability. The specimens were manufactured by the low heat-press(warmpress) method. In addition, the interface and the cross-linking reaction of cement and polymers was also studied by the SEM and TEM. Flexural strength of HAC/PVA based MDF cementitious composites was proportionally decreased with increasing fiber contents due to the undensified structure around fibers. The flexural strength of insoluble polymer added specimen was decreased with increasing fiber contents, while water stability was dramatically improved. Epoxy resin added specimen showed the highest strength with increasing fiber contents, compared with other specimens. The water stability of fiber content 4% added specimen immersed in water presented about 95%, 87% at 3 and 7 days immersed in water, respectively. The interfacial adhesive strength of fiber-matrix was very much improved due to cross linking reaction of polymer and metal ions of cement. Tensile strength of insoluble polymers added composites as linearly increased with increasing the fiber contents. The epoxy resin added specimen also showed highest tensile strength. The 4% fiber added specimen presented 30~80% higher strength than controlled specimen.

• Structural Engineering and Mechanics
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• v.29 no.3
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• pp.301-310
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• 2008

Applications of fracture mechanics in the strength analysis of ceramic materials have been lately studied by many researchers. Various test specimens have been proposed in order to investigate the fracture resistance of cracked bodies under mixed mode conditions. Double Cleavage Drilled Compression (DCDC) specimen, with a hole offset from the centerline is a configuration that is frequently used in subcritical crack growth studies of ceramics and glasses. This specimen exhibits a strong crack path stability that is due to the strongly negative T-stress term. In this paper the maximum tensile stress (MTS) criterion is employed for investigating theoretically the initiation of brittle fracture in the DCDC specimen under mixed mode conditions. It is shown that the T-stress has a significant influence on the predicted fracture load and the crack initiation angle. The theoretical results suggest that brittle fracture in the DCDC specimen is controlled by a combination of the singular stresses (characterized by KI and KII) and the non-singular stress term, T-stress.

• Advanced Composite Materials
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• v.17 no.4
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• pp.359-372
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• 2008

The moisture absorption behavior of carbon fiber-reinforced plastic (CFRP) and its effect on dimensional stability were examined. Moisture diffusivity in CFRP was determined by measuring a specimen's weight during the moisture absorption test. Three types of CFRP specimens were prepared: a unidirectionally reinforced laminate, a quasi-isotropic laminate and woven fabric. Each CFRP was processed into two geometries - a thin plate for determination of diffusivity and a rod with a square cross-section for the discussion of two-dimensional diffusion behavior. By solving Fick's law expanded to 3 dimensions, the diffusivities in the three orthogonal directions were obtained and analyzed in terms of the anisotropy of CFRP moisture diffusion. Coefficients of moisture expansion (CMEs) were also obtained from specimen deformation caused by moisture absorption. During moisture absorption, the specimen surfaces showed larger deformation near the edges due to the distribution of moisture contents. This deformation was reasonably predicted by the finite element analysis using experimentally determined diffusivities and CMEs. For unidirectional CFRP, the effect of the fiber alignment on CME was analyzed by micromechanical finite element analysis (FEA) and discussed.

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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• 2000.06a
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• pp.173-179
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• 2000

The friction and wear characteristics of brake friction materials reinforced with aramid fiber, carbon fiber, glass fiber, and potassium titanate whiskers were investigated using a pad-on-disk type friction tester. In particular, the morphology of rubbing surfaces was carefully investigated to correlate the friction performance and properties of transfer films. The aramid fiber reinforced specimen showed severe oscillation of friction coefficient at low speed and low applied pressure. The carbon fiber reinforced specimen showing better friction stability exhibited uniform and stable transfer film than any other specimens. The glass fiber reinforced specimen showed unstable friction changes at high speed and high-applied pressure and the non-uniform transfer film was observed in both friction material and rotor surface. The potassium titanate whiskers reinforced specimen showed stable coherent transfer film. The wear test exhibited the potassium titanate whiskers reinforced specimen was lowest in wear amount and glass fiber reinforced specimen showed the severe wear.

• Korean Journal of Materials Research
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• v.28 no.3
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• pp.129-134
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• 2018

This study was carried out to investigate the effect of grain size on the damping capacity of the Fe-26Mn-4Co-2Al damping alloy. ${\alpha}^{\prime}$ and ${\varepsilon}-martensite$ were formed by cold working, and these martensites were formed with a specific direction and surface relief. With an increase in grain size, the volume fraction of ${\alpha}^{\prime}$ and ${\varepsilon}-martensite$ increased by decrement the austenite phase stability. This volume fraction more rapidly increased in cold-rolled specimen than in the specimen that was not cold-rolled. The damping capacity also increased more with the augmentation an increased grain size and more rapidly increased in cold-rolled specimen than in the specimen that was not cold rolled. The effect of grain size on the damping capacity was larger in the cold-rolled specimen than the specimen that was not cold-rolled. Damping capacity linearly increased with an increase in volume fraction of ${\varepsilon}-martensite$. Thus, the damping capacity was affected by the ${\varepsilon}-martensite$.

• Proceedings of the Korean Geotechical Society Conference
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• 2003.03a
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• pp.189-196
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• 2003

Soil-cement column is often used as a contaminant barrier. This study presents the results of experimental study performed to investigate the changes of properties of soil-cement column under the attack of acids. Sulfuric nitric, and ascetic acid were used as contaminants. Specimen were made of clayey and sandy soils with addition of cement and water Permeability of soil-cement decreased with time during permeability test. When significant amount of acid percolated the specimen, permeability increased and compressive strength decreased due to the dissolution and leaching of cement and its chemical reaction compounds. Sulfuric and nitric acid were more effective than ascetic acid in deteriorating soil-cement column. Amount of acid required to lower the pH of soil cement below 12 was calculated from the results of permeability tests. This leads to a conclusion that, under the conditions employed in this study, the chemical stability of soil-cement column could be maintained against acid attack for longer than generally accepted lifetime of contaminant barriers.