• Title/Summary/Keyword: Solution Spraying Method

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Characterizations of Two-step Matrix Application Procedures for Imaging Mass Spectrometry

  • Shimma, Shuichi
    • Mass Spectrometry Letters
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    • v.6 no.1
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    • pp.21-25
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    • 2015
  • In this paper, I describe the importance of matrix spraying conditions in imaging mass spectrometry (IMS) to obtain successful imaging results. My developed matrix application methodology, which is a "two-step matrix application" sequentially combined with matrix sublimation and spraying matrix solution can provide high reproducibility and high ion yield compared with a conventional direct spraying method. However, insufficient IMS results were obtained occasionally despite the two-step method. Therefore, I wanted to characterize the methodology to continuously provide high quality data. According to my results, the sublimation time was not a strict parameter, and the most important step was the first spraying condition. This means that the extraction conditions from the tissue section and co-crystallization of the matrix were the most important factors.

Fine Dust Suppression by Enzyme Induced Carbonate Precipitation: Indoor Experiment and Field Application (EICP에 의한 미세먼지 억제: 실내 실험 및 현장 적용)

  • Song, Jun Young;Ha, Seong Jun;Sim, Youngjong;Jin, Kyu-Nam;Yun, Tae Sup
    • Journal of the Korean Geotechnical Society
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    • v.35 no.10
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    • pp.67-78
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    • 2019
  • The efficiency of suppressing fine dust was evaluated by conducting indoor and field experiments for the ground treated with EICP solution, which is an eco-friendly ground improvement method. In laboratory experiments, the EICP solution was prepared with inexpensive materials for the field applicability, and the optimal mixing ratio and optimal spraying volume of EICP solution were calculated. The optimum amount of calcium carbonate was shown when the ratio of urea/calcium chloride and white powder were 1.5 and 15 g/L, respectively. The optimum spraying amount of the EICP solution was $7L/m^2$ determined by fine dust suppression and cone tip resistance experiments. The spraying of water and EICP solution was conducted at the test-bed where dump trucks pass for the effect of suppressing fine dust of each method. The effective fine dust suppression method can be chosen depending on the situation of the site.

Fabrication of Porous Silk Fibroin Microparticles by Electrohydrodynamic Spraying (전기분사법에 의한 다공성 실크 피브로인 미세입자의 제조)

  • Kim, Moo Kon;Lee, Ki Hoon
    • Polymer(Korea)
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    • v.38 no.1
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    • pp.98-102
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    • 2014
  • Nowadays, silk fibroin receives a lot of attention as novel natural biomaterials due to its excellent biocompatibility and biodegradability. Electrohydrodynamic spraying (EHDS) is one of the method for the preparation of micro or nanoparticles by applying high voltage to the polymer solution. In this research, we fabricated silk fibroin porous microparticles by electrohydrodynamic spraying. Poly(ethylene glycol) (PEG) was added to the fibroin solution to give pores to silk fibroin microparticles. By the addition of PEG, the microparticle size was decreased despite of the decrease in conductivity and the increase of viscosity of the spraying solution. It seems that the immiscibility of silk fibroin and PEG affected much more to the microparticle size than the conductivity and viscosity. Immersing the as-sprayed microparticles into the water removed the phase-separated PEG, and finally, porous silk fibroin microparticles were prepared. The porous silk fibroin microparticles are expected to be applied as drug carriers in drug delivery or cell carriers in tissue engineering.

Micro-sized carbon with dimple patterns prepared using an electro-spray method

  • Park, Mi-Seon;Lee, Young-Seak
    • Carbon letters
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    • v.16 no.3
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    • pp.215-218
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    • 2015
  • Carbon micro particles with dimple patterns were produced by electro-spraying a solution of pitch in tetrahydrofuran. Particle formation depended on separation in an electrical field and volatilization of the solvent. More than 80% of the obtained carbon exhibited an average particle size of less than 50 μm. X-ray diffraction analysis suggests that the carbon with dimple patterns has increased crystallinity after heat treatment.

Optical Properties of Spherical YAG:Ce3+ Phosphor Powders Synthesized by Atmospheric Plasma Spraying Method Appling PVA Solution Route and Domestic Aluminium Oxide Seed (PVA 용액법과 국산 산화알루미늄을 적용하여 대기 플라즈마 용사법으로 합성된 구형의 YAG:Ce3+ 형광체의 발광특성)

  • Yong-Hyeon Kim;Sang-Jin Lee
    • Journal of Powder Materials
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    • v.30 no.5
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    • pp.424-430
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    • 2023
  • YAG phosphor powders were fabricated by the atmospheric plasma spraying method with the spray-dried spherical YAG precursor. The YAG precursor slurry for the spray drying process was prepared by the PVA solution chemical processing utilizing a domestic easy-sintered aluminum oxide (Al2O3) powder as a seed. The homogenous and viscous slurry resulted in dense granules, not hollow or porous particles. The synthesized phosphor powders demonstrated a stable YAG phase, and excellent fluorescence properties of approximately 115% compared with commercial YAG:Ce3+ powder. The microstructure of the phosphor powder had a perfect spherical shape and an average particle size of approx imately 30 ㎛. As a result of the PKG test of the YAG phosphor powder, the synthesized phosphor powders exhibited an outstanding luminous intensity, and a peak wavelength was observed at 531 nm.

Physical and Biological Performance Evaluation of Disinfection Systems for Transportation Vehicles against AI Virus

  • Chung, Hansung;Choi, Kwanghoon;Kim, Sungkwan;Kim, Sukwon;Lee, Kyungwoo;Choe, Nonghoon
    • Journal of Microbiology and Biotechnology
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    • v.31 no.7
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    • pp.956-966
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    • 2021
  • To prevent the outbreak of infectious diseases that inflict huge economic and social losses, domestic livestock farms and related facilities have introduced automatic and semiautomatic disinfectant solution-spraying systems for vehicles. However, the facility standards and specifications vary by manufacturer, and no scientific performance evaluation has been conducted. The puropose of this study is to develop physical and biological evaluation methods. Physical and biological appraisals were conducted using two types of disinfection facilities (tunnel- and U-type) and two types of vehicles (passenger car, truck). Water-sensitive paper was used to evaluate the physical performance values for the disinfection facilities. In addition, to assess their biological performance, carriers containing low-pathogenic avian influenza virus were attached to vehicles, and the viral reduction was measured after the vehicles moved through the facility. The tunnel-type had rates of coverage in the range of 70-90% for the passenger car and 60-90% for the truck. At least 4-log virus reduction after spraying for 1-5 min was shown for both vehicles. For the U-type facility evaluation, the coverage rates were in the range of 60-90% for the passenger car and at least 90% for the truck. More than 4-log viral reduction was estimated within a spraying time of 5 min. To reduce viruses on the surface of vehicles by at least 4 log within a short period, the disinfectant solution should cover at least 71% of the pathogens. In conclusion, we were able to assess the physical and biological performance criteria for disinfection facilities aboard transportation vehicles.

A Case Study on Corrosion Rates of Concrete Sewer Pipes in Housing Sites (주택단지 오수용 콘크리트 흄관의 부식속도 측정 사례)

  • Kim, Young-Jin
    • Proceedings of the Korea Concrete Institute Conference
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    • 2006.05a
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    • pp.550-553
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    • 2006
  • This study measured corrosion rates for checking and analysis of Hume pipes in the housing sites. According to the result, Concrete pipe is deteriorating for twenty years by hydrogen sulfide(H2S). Investigation method applied phenolphthalein method(depth of neutrality). Phenolphthalein method measured average depth from concrete surface to coloring point by red after spraying phenolphthalein solution. A result of investigation, Life span of Hume pipe in the housing site is investigated of twenty years.

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Studies on Application of Spray of Nano-fibrillated Cellulose to Papermaking Process (분무방식에 의한 NFC(Nano-Fibrillated Cellulose)의 제지공정 적용 방안 탐색 연구)

  • Lee, Kwang Seob;Kim, Chang Geun;Lee, Jae Hoon;Lee, Tai Ju;Ryu, Jeong Yong
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.47 no.4
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    • pp.5-12
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    • 2015
  • In recent years, it had focused on the improvement of paper properties by addition of NFC (Nano-fibrillated Cellulose). Although the addition of NFC to wet-end of papermaking process could be suggested as a new solution to improve the strength properties of paper, it was not possible to avoid the bad drainage caused by the added NFC's chocking pores of wet web. Instead of the direct addition to wet-end, spraying of NFC to web in wire-section was tried in this study and evaluated by checking various paper properties including surface smoothness, tensile strength, folding endurance and stiffness. According to the increase of spraying amount of NFC, above mentioned paper properties were enhanced without excessive deterioration of drainage. Compared with direct introduction to wet-end, spraying could be regarded as a more proper method to enhance the surface smoothness and strength properties of paper.

Tribological Properties of Carbon Nanotube Thin Films by using Electrodynamic Spraying Method (전기 분사 증착 방식을 이용한 탄소 나노 튜브 박막의 트라이볼로지적 특성에 관한 연구)

  • Kim, Chang-Lae;Kim, Dae-Eun;Kim, Hae-Jin
    • Tribology and Lubricants
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    • v.34 no.6
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    • pp.313-317
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    • 2018
  • Carbon-based coatings, including carbon nanotubes (CNTs), graphene, and buckyball ($C_{60}$), receive much interest because of their outstanding mechanical and electrical properties for a wide range of electromechanical component-based applications. Previous experimental results demonstrate that these carbon-based coatings are promising solid lubricants because of their superior tribological properties, and thus help prolong the lifetime of silicon-based applications. In this study, CNT coatings are deposited on a bare silicon (100) substrate by electrodynamic spraying under different deposition conditions. During the coating deposition, the applied voltage, CNT concentration of the solution, distance between the injecting nozzle and the substrate and diameter of the injecting nozzle are optimized to control the thickness and surface roughness of the CNT coatings. The surface morphology and thickness of the coatings are characterized by scanning electron microscopy (SEM) and atomic force microscopy (AFM), respectively. The friction and wear properties of the coatings are investigated by using a pin-on-reciprocating-type tribotester under various experimental conditions. The friction coefficient of the CNT coating is as low as 0.15 under high normal loads. The overall results reveal that CNT coatings deposited by electrodynamic spraying provide relatively uniform with superior lubrication performance.

A study on ice-slurry production by water spray (수분무에 의한 아이스 슬러리 생성에 관한 연구)

  • Kim, B.S.;Lee, Y.P.;Yoon, S.Y.;Lee, J.H.
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.9 no.2
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    • pp.134-143
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    • 1997
  • A theoretical and experimental study has been performed to investigate the characteristics of ice-slurry product. By diffusion-controlled model, the possibility of ice slurry has been theoretically anticipated. The water vapor evaporated from the surface of droplets is extracted continuously from the chamber by a vacuum pump. The droplet diameter was measured by silion immersed method. The ice slurry has been obtained by spraying droplets of ethylene-glycol aqueous solution in the chamber where pressure is maintained under the triple point of water. The droplet of which the diameter is $300{\mu}m$, and the initial temperature is $20^{\circ}C$, was changed into ice particle within the chamber of which the height is 1.33m.

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