• 한국세라믹학회지
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• 제41권1호
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• pp.1-8
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• 2004

The microstructural features and mechanical behavior of directionally solidified $(Y_2O_3)ZrO_2/Al_2O_3$ eutectic fibers after extended beat treatment in oxidizing environment were investigated. The fiber was grown continuously by an Edge-defined Film-fed Growth (EFG) technique. The microstructure was characterized using X-Ray Diffraction (XRD) and Scanning Electron Microscopy(SEM). The microstructure of the fiber in the as-fabricated state consists of highly oriented colonv and fine lamellar microstructure along the fiber axis. Tensile strength of the $(Y_2O_3)ZrO_2/Al_2O_3$ eutectic fiber remained unchanged with heat treatment at temperatures between $1200^{\circ}C$ and $1500^{\circ}C$ up to 300h. The weibulls modulus remained fairly constant after extended thermal exposure. The fracture toughness and crack propagation behavior were investigated. The fracture toughness ($K_{1C}$) of the $(Y_2O_3)ZrO_2/Al_2O_3$ eutectic fiber in the as-fabricated state were measured to be 3.6 ${\pm}$ 0.5 MPa${\cdot}m^{1/2}$ by an indentation technique and 2.2 ${\pm}$ 0.2 MPa${\cdot}m^{1/2}$ by assuming elliptical flaw of a semi-infinite solid, respectively. The $(Y_2O_3)ZrO_2/Al_2O_3$ eutectic fiber showed a radial (Palmqvist) crack type and exhibited an orthotropic crack growth behavior under 100 g load.

• 보존과학회지
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• 제35권2호
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• pp.145-152
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• 2019

The metal-manufacturing method and smelting temperature of ancient metal-production processes have been studied by analyzing the principal elements and microstructures of slag. However, the microstructure of slag varies according to the solidification cooling rate and types and relative amounts of various oxides contained within the smelting materials. Hence, there is a need for accurate analysis methods that allow slag to be distinguished by more than its composition or microstructure. In this study, the microstructures of slag discharged as a result of smelting iron sands collected from Pohang and Gyeongju, as well as the slag excavated from the Ungyo site in Wanju, were analyzed by using metalloscopy, scanning election microscopy-energy dispersine X-ray spectroscopy(SEM-EDS) and wavelength dispersive X-ray fluorenscence(WD-XRF). Furthermore, the microcrystals were accurately characterized by performing Raman micro-spectroscopy, which is a technique that can be used to identify the microcrystals of slags. SEM-EDS analysis of Pohang slag indicated that its white polygonal crystals could be Magnetite; however, Raman micro-spectroscopy revealed that these crystals were actually $ulv{\ddot{o}}spinel$. Raman micro-spectroscopy and SEM-EDS were also used to verify that the coarse white dendritic structures observed in the Gyeongju-slag were $W{\ddot{u}}stites$. Additionally, the Wanju slag was observed to have a glassy matrix, which was confirmed by Raman micro-spectroscopy to be Augite. Thus, we have demonstrated that Raman micro-spectroscopy can accurately identify slag microcrystals, which are otherwise difficult to distinguish as solely based on their chemical composition and crystal morphology. Therefore, we conclude that it has excellent potential as a slag analysis technique.

• Nuclear Engineering and Technology
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• 제54권11호
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• pp.4072-4083
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• 2022

Ultrasonic impact treatment (UIT) is carried out on the Ni-based alloy stainless steel pipe gas tungsten arc welding (GTAW) girth weld, the differences of microstructure, microhardness and shear strength distribution of the joint before and after ultrasonic shock are studied by microhardness test and shear punch test. The results show that after UIT, the plastic deformation layer is formed on the outside surface of the Ni-based alloy overlayer, single-phase austenite and γ type precipitates are formed in the overlayer, and a large number of columnar crystals are formed on the bottom side of the overlayer. The average microhardness of the overlayer increased from 221 H V to 254 H V by 14.9%, the shear strength increased from 696 MPa to 882 MPa with an increase of 26.7% and the transverse average residual stress decreased from 102.71 MPa (tensile stress) to -18.33 MPa (compressive stress), the longitudinal average residual stress decreased from 114.87 MPa (tensile stress) to -84.64 MPa (compressive stress). The fracture surface has been appeared obvious shear lip marks and a few dimples. The element migrates at the fusion boundary between the Ni-based alloy overlayer and the austenitic stainless steel joint, which is leaded to form a local martensite zone and appear hot cracks. The welded joint is cooled by FA solidification mode, which is forming a large number of late and skeleton ferrite phase with an average microhardness of 190 H V and no obvious change in shear strength. The base metal is all austenitic phase with an average microhardness of 206 H V and shear strength of 696 MPa.

• 한국주조공학회지
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• 제14권6호
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• pp.566-575
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• 1994

The effects of varying the pouring temperature and the die preheating temperature in producing centrifugally cast HP alloy modified with Nb was evaluated on the basis of the resultant macrostructure, microstructure and hardness of these castings. Increased die preheating temperatures and pouring temperatures resulted in an increase in the thickness of the columnar dendritic zone, the primary and secondary dendrite arm spacing and the thickness of the zone of porosity at the casting I.D.(inner diameter). Lower die preheating temperature and pouring temperatures result in increased grain fineness and an increased zone of equiaxed grains. A higher hardness was achieved toward the casting O.D.(outer diameter) compared to the casting I.D., attributable to alloy segregation toward the casting I.D. and segregation differences resulting from reduced solidification cooling rates toward the casting I.D. Also, a higher hardness was realized at the cold end of the casting attributed to a more uniform distribution of carbides.

• 한국결정성장학회지
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• 제15권6호
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• pp.229-233
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• 2005

Novel process was tried to obtain micro-porous ceramic body containing continuous pore channel. $MgAl_2O_4/MgO$ eutectic fibers and rods have been grown successfully by the micro-pulling-down method, and the microstructures and optical characterizations of grown crystals were performed. $MgAl_2O_4/MgO$ eutectic fibers of $0.3{\sim}1mm$ in diameter and about 500 mm in length, and the rods having 5 mm in diameter with approximately 60 mm in length have been grown with the $6{\sim}120mm/hr$ of growth speed. The eutectic fibers showed homogeneous microstructure in which MgO fiber aligned to the growth direction in the $MgAl_2O_4$ (spinel) matrix. The grown crystals looked semitransparency under naked eyes. Optical and orientational characterizations were performed. The second phase of MgO (periclase) was easily removed by selective etching with hydrochloric acid, and then porous bodies were obtained.

• 한국레이저가공학회지
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• 제4권1호
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• pp.39-48
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• 2001

This study was performed to evaluate basic characteristics of electron beam weldability for high strength aluminum alloys. The aluminum alloys used were A5083 and A6N01, and A7N01. The principal welding process parameters, such as accelerating voltage, beam current, welding speed and chamber pressure were investigated. The dimension and microstructure of welds were evaluated with OLM, and SEM (EDAX). In addition, weldability variation(cracking) due to process parameters was also evaluated. The degree of cracking in the EB fusion zone appears to be affected mainly by aspect ratio, such that as aspect ratio increases the cracking tendency also increases. The alloying element itself may also affect the hot cracking resistance, but its role is considered to be indirect effect such that the relatively higher vaporization pressure elements of Zn and Mg give deeper weld penetration and thus results in greater cracking tendency.

• 한국공작기계학회논문집
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• 제12권1호
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• pp.45-49
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• 2003

Tensile strength of the woven glass fiber reinforced PET (Poly-Ethylene-Terephthalate) matrix composite manufactured by rapid press consolidation technique was investigated and evaluated. During pre-heating, consolidation and solidification stages, the optimal manufacturing conditions for this composite were discussed based on the void content and tensile properties depending on vacuum condition. It is found that the effect of vacuum condition during preheating gives a substantial difference on the strength as well as microstructure. It is also found that the failure micromechanism shows several energy absorption processes enhancing fracture toughness.

• 한국분말재료학회지
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• 제18권4호
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• pp.340-346
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• 2011

In order to improve the weak mechanical properties of cast Mg alloys, Mg-$Zn_1Y_2$ (at%) alloy powders were synthesized using gas atomization, a typical rapid solidification process. The powders consist of fine dendrite structures less than 3 ${\mu}m$ in arm spacing. In order to fabricate a bulk form, the Mg powders were compacted using magnetic pulse compaction (MPC) under various processing parameters of pressure and temperature. The effects of the processing parameters on the microstructure and mechanical properties were systematically investigated.

• 한국주조공학회지
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• 제9권3호
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• pp.221-227
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• 1989

The effect of sulfur content and inoculant on solidification microstructure and mechanical properties of gray cast iron have been investigated. The main results obtained are as follows, 1. In the FeSi3Ca1Ba inoculated irons, with the variation of sulfur content, low sulfur levels (${\sim}0.03%$) yield low chill depth, high tensile strength, good wear resistance and type A graphite with a pearlite matrix. High sulfur levels( >0.08%) provide high chill depth, low mechanical proper ties and type D graphite with small amount ferrite. 2. In case of inoculant variation with normal FeSi, FeSi3Ca1Ba, 30CaSi and uninoculation at 0.03%S level, lower chill depth and higher tensile strength was obtained in the order ; 30CaSi, FeSi3Ca1Ba normal FeSi, uninoculation.

• 한국주조공학회지
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• 제7권3호
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• pp.192-198
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• 1987

Commercial semicontinuous cast ingots of aluminum alloys often exhibit large grains composed of parallel arrays of continuous lamellae. Each lamella consists of a central {111} coherent twin boundary and wavy solidification boundary. This microstructure is referred to as a twin columnar growth(TCG) structure. The factors influencing the formation of a TCG structure include a unidirectional thermal gradient and the critical range of the alloying element content. The higher the thermal gradient is, the shorter the twin plane spacings are. The composition profile for an untwinned dendrite shows maximums at the positions of the interdendritic channels and the minimum appears at the center of the dendrite. While for twinned dendrite, it has wavy apperance. This profile has two local minimums instead of one shown in the untwinned.