• Title/Summary/Keyword: Solidification behavior

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Real Time Imaging of Solidification Behavior by Synchrotron X-ray Radiography (싱크로트론 X-선 투과영상법을 활용한 응고거동 실시간 관찰)

  • Lee, Sang-Mok;Yasuda, Hideyuki
    • Journal of Korea Foundry Society
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    • v.30 no.1
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    • pp.5-13
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    • 2010
  • This article aims to introduce the synchrotron radiation for its utilization in the casting and solidification fields as an unique tool for observation of real time phenomena of molten metal during solidification. General features of the synchrotron radiation were briefly introduced for readers in the casting and solidification fields, with no background regarding to synchrotron radiation. And basic principles of imaging technologies using synchrotron light for in-situ observation of molten metal were explained together with exemplary research works, which were reported on the casting and solidification fields in recent years. As a practical guide, real time observation of Al-Si casting alloy was introduced with experimental facilities, image acquisition, and processing together with representative results.

Decomposition Behavior of Secondary Solidification Phase During Heat Treatment of Squeeze Cast Al-Cu-Si-Mg (용탕단조 Al-Cu-Si-Mg합금의 열처리시 제2응고상의 분해거동)

  • Kim, Yu-Chan;Kim, Do-Hyang;Han, Yo-Sub;Lee, Ho-In
    • Journal of Korea Foundry Society
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    • v.17 no.6
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    • pp.560-568
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    • 1997
  • The dissolution behavior of secondary solidification phases in squeeze cast Al-3.9wt%Cu-1.5wt%Si-1.0wt%Mg has been studied using a combination of optical microscope, image analyzer, scanning electron microscope(SEM), energy dispersive spectrometer(EDS), X-ray diffractometer(XRD) and differential thermal analyzer (DTA). Special emphasis was placed on the investigation of the effects of the nonequilibrium heat treatment on the dissolution of the second solidification phases. Ascast microstructure consisted of primary solidification product of ${\alpha}-Al$ and secondary solidification products of $Al_2Cu$, $Mg_2Si$ and $Al_2CuMg$. Equilibrium and non-equilibrium solution treatments were carried out at the temperatures of $495^{\circ}C$, $502^{\circ}C$ and $515^{\circ}C$ for 3 to 5 hours. The amount of the dissolved secondary phases increased with increasing solution treatment temperature, for example, area fractions of $Al_2Cu$, $Mg_2Si$ and $Al_2CuMg$ were approximately 0%, 1.6% and 4.2% after solution treatment at $495^{\circ}C$ for 5hours, and were approximately 0%, 0.36% and 2% after solution treatment at $515^{\circ}C$ for 5hours. The best combination of tensile properties was obtained when the as-cast alloy was solution treated at $515^{\circ}C$ for 3hours followed by aging at $180^{\circ}C$ for 10 hours. Detailed DTA and TEM study showed that the strengthening behavior during aging was due to enhanced precipitation of the platelet type fine ${\theta}'$ phase.

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Prediction of Solidification Path in Al-Si-Fe Ternary System and Experimental Verification (Al-Si-Fe 3원계 조성의 응고경로 예측 및 실험적 검증)

  • Lee, Sang-Hwan;Lee, Sang-Mok
    • Journal of Korea Foundry Society
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    • v.30 no.1
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    • pp.34-45
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    • 2010
  • The effects of alloy elements and cooling rate on the solidification path and the formation behavior of $\beta$ phase in Fe-containing Al-Si alloys were studied based on the thermodynamic analysis and the pertinent experiments. The thermodynamic calculation was systematically performed by using Thermo-Calc program. For the thermodynamic analysis in high alloy region of Al-Si-Fe ternary system, a thermodynamic database for Thermo-Calc was correctly updated and revised by the collected up-to-date references. For the thermodynamic-based prediction of various solidification paths in Fe-containing Al-Si system, liquidus projection of Al-Si-Fe ternary system, including isotherms, invariant, monovariant, bivariant reactions and equilibrium temperatures, was calculated and analyzed as functions of composition and temperature. The calculated results were compared to the experimental results using various casting specimens. In order to analyze various solidification sequences as functions of Si and Fe content, 4 representative alloy compositions, low Fe content in both low and high Si contents and high Fe content again in both low and high Si contents, were designed in this study. For better understanding of the influence of cooling rate on the formation behavior of $\beta$ phase, 4 alloys were solidified under furnace and rapidly cooled conditions. Cooling curves of solidified alloys were recorded by thermal analysis. Various important solidification events were evaluated using the first derivative-cooling curves. Microstructures of the casting samples were studied by the combined analysis of optical microscopy (OM) and scanning electron microscopy (SEM).

The Effect of Solidification Rate on Solidification Behavior in IN792+Hf Superalloy (IN792+Hf 초내열합금의 응고거동에 미치는 응고속도의 영향)

  • Bae, Jae-Sik;Kim, Hyeon-Cheol;Lee, Jae-Hyeon;Yu, Yeong-Su;Jo, Chang-Yong
    • Korean Journal of Materials Research
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    • v.11 no.6
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    • pp.502-507
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    • 2001
  • The effect of solidification rate on the microstructure of directionally solidified IN792+ Hf superalloy has been studied. Solidification sequence and precipitation behavior of the alloy have been analysed by microstructural observation. The script carbide transformed to faceted carbide with decreasing solidification rates. The incorporation of ${\gamma}$ phase into the faceted carbide was due to dendritic growth of carbides. Some elongated carbide bars formed along the grain boundaries at a solidification rate of 0.5$\mu\textrm{m}$/s. Two zones, ${\gamma}$' forming elements enriched zone and depleted zone, were found in the residual liquid area. Eutectic ${\gamma}$/${\gamma}$' nucleated in the f forming elements enriched zone. Formation of eutectic ${\gamma}$/${\gamma}$' increased the ratio of (Ti+Hf+Ta+W)/Al and induced η phase precipitation. The ratio of (Ti+Hf+Ta+W)/Al decreased at lower solidification rates due to sufficient back diffusion in the residual liquid area. Hence, the Precipitation of the η Phase efficiently suppressed at the lower solidification rate.

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Effect of Laser Pulse Shaping on Reduction in Defects of Stainless Steel Sport Weld Metals (스텐레스 강 용접부에 형성되는 결함의 저감에 미치는 레이저 펄스 파형의 영향)

  • 김종도;카따야마세이지
    • Journal of the Korean Society of Marine Environment & Safety
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    • v.3 no.2
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    • pp.13-21
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    • 1997
  • This paper describes the effectiveness of laser pulse shaping in eliminating weld defects such as porosity, cracks and undercuts in pulsed Nd:YAG Laser welding. A large porosity was formed in a keyhole mode of deep penetration weld metal of any stainless steel. Solidification cracks were present in Type 303 with about 0.3%s. The conditions for the formation of porosity were determined in further detail in Type 316. With the objectives of obtaining a fundamental knowledge of formation and prevention of weld defects, the fusion and solidification behavior of a molten puddle was observed during laser spot welding of Type 310S. through high speed video photographing technique. It was deduced that cellular dendrite tips grew rapidly from the bottom to the surface, and consequently residual liquid remained at the grain boundaries in wide regions and enhanced the solidification cracking susceptibility. Several laser pulse shapes were investigated and optimum pulse shapes were proposed for the reduction and prevention of porosity and solidification cracking.

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The Effect of Cooling Rate on the Solidification Behavior and Segregation of 7075 and 7050 Aluminum Alloys (7075 및 7050 알루미늄 합금의 응고 거동 및 편석에 미치는 냉각 속도의 영향)

  • Choi, Jeong-Yun;Kwon, Young-Dong;Lee, Joo-Won;Lee, Zin-Hyoung
    • Journal of Korea Foundry Society
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    • v.21 no.6
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    • pp.343-349
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    • 2001
  • The effect of cooling rate on the solidification microstructure and segregation behavior of 7075 and 7050 aluminum alloy was investigated. Samples were solidified with cooling rates from 0.3 to $17^{\circ}K/sec$. Using the cooling curves of each sample, liquidus, eutectic and intermetallic reaction temperatures were estimated. The microstructures were characterized in terms of dendrite arm spacing and eutectic volume fraction. The segregation behavior of each alloying element of these alloys in various cooling rates was discussed.

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A Study on the Optimal Design and Forming of the Alternator Housing

  • Han, Kyu-Taek;Park, Jung-Sik
    • Journal of Advanced Marine Engineering and Technology
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    • v.28 no.2
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    • pp.361-366
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    • 2004
  • The die casting process was used to manufacture an automotive alternator housing. Generally automobile parts are required to be light and have high strength. The control of casting defects is important but has usually been depended only on the experience of the foundry engineer. Therefore simulations have been carried out on the die casting process of alternator housing. In this paper. we investigated the characteristics of the die casted alternator housing with the HPDC(High Pressure Die Casting) process. We presented the results of filling behavior and solidification process of the cast, The analysis results obtained from the filling behavior and solidification of cast agreed with test results.

The Effects of Pattern Coatings on the Solidification of Pure Aluminum Castings and the Thermal Behavior of Molds in FMC Processes (FMC법에서 모형 도형제가 순알루미늄 주물의 응고와 주형의 열적거동에 미치는 영향)

  • Cho, N.D.;Kim, Y.N.
    • Journal of Korea Foundry Society
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    • v.7 no.2
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    • pp.122-132
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    • 1987
  • Full mold casting process is a new technique offering numerous advantages and promising possibilities. The present study is aimed to bring out the results of experiments carried out to study the effect of pattern coatings on the solidification of 99.5% pure aluminum plate-shaped castings in the various sand molds and the thermal behavior of the molds. The results of the investigation indicate that (i) with increase in pattern coating thickness, the relative chilling power decreases gradually for silica and increases for zircon coating, and (ii) the application of a pattern coating significantly reduces the maximum interface temperature by the mold which is more pronounced in the case of thinner mold wall. The investigation also indicates that Chvorinov's rule is not found to be valid for the casting in the full mold, with or without pattern coating. Therefore in full mold process, the pattern coating thickness will be a very important parameter in the study of thermal behavior.

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Solidification Process of an Al-Cu Alloy in a Vertical Annular Mold and Effects of Cooling Rate on Macrosegregation (수직환상주형내 Al-Cu합금의 응고과정 및 냉각속도의 조대편석에 대한 영향)

  • 유호선
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.18 no.7
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    • pp.1818-1832
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    • 1994
  • Transport process during solidification of an AI-CU alloy in a vertical annular mold of which inner wall is cooled is numerically simulated. A model which can take account of local density dependence on the solute concentration is established and incorperated in the analysis. Results show that thermally and solutally induced convections are developed in sequence, so that there is little interaction between them. Thermal convection effectively removes the initial superheat from the melt and vanishes as solidification proceeds from the cooling wall. On the other hand, solutal convection which is developed later over the meshy and the pure liquid regions leads to large-scale redistribution of the consituents. The degree of the initial superheating hardly affects overall solidification behavior except the early stage of the process, when the cooling rate is kept constant. Macrosegregation is reduced remarkably with increasing cooling rate, because not only the liquidus interface advances so quickly that time available for the solute transport is not enough, but also the interdendritic flow is strongly damped by rapid crystal growth within the mushy region.