• Title/Summary/Keyword: Solidification Rate

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Magnetic separation of Fe contaminated Al-Si cutting chip scraps and evaluation of solidification characteristics (Fe성분이 혼입된 Al-Si 절삭칩 스크랩의 자력선별 및 응고특성 평가)

  • Kim, Bong-Hwan;Kim, Jun-Kyeom;Lee, Sang-Mok
    • Journal of Korea Foundry Society
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    • v.29 no.1
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    • pp.38-44
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    • 2009
  • Magnetic separation of Fe contaminated Al-Si cutting chip scraps was performed for the recyclability assessment. It was also aimed to investigate the casting and solidification characteristics of the cutting chip scraps. The magnetically separated cutting chip scraps were adequately treated for the casting procedure and test specimens were made into a stepped mold inducing different cooling rates. The test specimens were evaluated by the combined analysis of ICP, Spectroscopy, OM-image analyzer, SEM/EDS, etc. Solidification characteristics of cutting chip scraps were examined as functions of Fe content and cooling rate. It is concluded that the magnetic separation process can be utilized to recycle the Fe contaminated Al-Si cutting chip scraps in the high cooling rate foundry process.

The Influence of Cooling Rates on the CFR and the MDE of Al-Si Alloys. (Al-Si합금(合金)의 CFR 과 MDE 에 미치는 냉각속도(冷却速度)의 영향(影響))

  • Kwon, Hyuk-Moo;Kim, Soo-Young
    • Journal of Korea Foundry Society
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    • v.4 no.4
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    • pp.14-19
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    • 1984
  • In order to clarify the solidification mechanism of Al-Si alloy, Mushy Degree of Eutectic Solidification (MDE) and Centerline Feeding Resistance (CFR) were systematically studied by casting with various compositions of $Al-(6{\sim}18%)$ Si alloys into several kinds of molds having different cooling rates. The results are as follows: 1. CFR% increases slightly as solute concentration increases, but decreases remarkably as the cooling rate of the mold increases, that is, the composition dependence of the alloys has more effect on the change of CFR% than that of the mold cooling rate. 2. The composition dependence of MDE value has the same tendency as that of Degree of Eutectic Solidification (DES). MDE value within the range of hypereutectic composition is larger than that of hypoeutectic and it represents the maximum value at eutectic composition. The higher the cooling rate is, the less the MDE value is.

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The structures and mechanical properties of unidirectionally solidified Al-Fe-Ni alloy (일방향응고시킨 Al-Fe-Ni 합금의 조직과 기계적 성질)

  • 김여원;신민교
    • Journal of Advanced Marine Engineering and Technology
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    • v.7 no.1
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    • pp.79-90
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    • 1983
  • The examination for the changes of structures and mechanical properties in directionally solidified Al-Fe-Ni alloys containing the small amount of Fe and Ni was carried out by the varying the composition and solidification rate R of alloy, provided that the temperature gradient was 80 .deg.C/cm. The result were obtained as follows. A) In proportion to the increase of the solidification rate (R), the crystallized phase of this alloy was changed from the Ribbon-type structure to the Rod-type structure. B) The strength was rapidly increased in the changing process of composite shape from the Ribbon-type to the Rod-type with the solidification rate (R) increasing. C) The fiber stress (${\sigma}^f$) and Young's modulus ($E_f$) calculated for the Rod-type structure were 220 kg/$mm^2$ and 11, 800 kg/$mm^2$ respectively, which were in good accord with the rule of Mixtures.

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Analysis of Microstructural Evolution During Directional Solidification of Ni-Base Superalloy CM247LC (니켈계 초내열합금 CM247LC의 일방향응고 시 미세조직 형성거동 분석)

  • Seo, Seong-Moon;Jeong, Hi-Won;Yun, Dae Won;Ahn, Young-Keun;Lee, Je-Hyun;Yoo, Young-Soo
    • Journal of Korea Foundry Society
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    • v.33 no.5
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    • pp.193-203
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    • 2013
  • The Ni-base superalloy CM247LC was directionally solidified (DS) using the Bridgman-type furnace to understand the effect of the chill plate on the microstructural evolution, such as dendrite arm spacing, microporosity, and MC-type carbide. The DS process was also modeled by the PROCAST to predict the solidification rate, thermal gradient, and resultant cooling rate in the entire length of the DS specimen. Due to the quenching effects of chill plate, four distinct areas were found to form in the specimen, in which the solidification rate was changed, during DS at a given withdrawal rate of 0.083 mm/s. Among the microstructural features investigated, the dendrite arm spacings and average size of the MC-type carbide near the chill plate were found to be influenced by the quenching effect of the chill plate. However, no significant influence was found on the size and volume fraction of microporosity, and the volume fraction of the MC-type carbide. The relationship between the microstructural features and the solidification variables was also analyzed and discussed on the basis of a combination of experimental and modeling results.

Preparation of Transparent ${\gamma}$-$6Bi_2O_3$.$GeO_2$ Polycrystals by Unidirection Solidification of Melt (융액 일방향 응고법에 의한 ${\gamma}$-$6Bi_2O_3$.$GeO_2$ 투명 다결정체의 제조)

  • 김호건;김명섭;류일환
    • Journal of the Korean Ceramic Society
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    • v.27 no.4
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    • pp.567-573
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    • 1990
  • Solidification condition for preparing transparent ${\gamma}$-6Bi2O3.GeO2 polycrystals by unidirectional solidification of melt, were investigaetd and the properties of the polycrystals prepared were measured. The ${\gamma}$-6Bi2O3.GeO2 polycrystals showing transparency like a single crystal were obtained by the unidirectional solidification of ${\gamma}$-6Bi2O3.GeO2 melt at a solidification rate of 0.5mm/h under a thermal gradient of 12$0^{\circ}C$/cm. The transparent polycrystals obtained showed the same photoconduction and optical activity as the ${\gamma}$-6Bi2O3.GeO2 single crystals grown by Czochralski method. But the electro-optic effect of polycrystals was heterogeneous because the colummar ${\gamma}$-6Bi2O3.GeO2 crystals were not oriented to the particular crystallographic direction.

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Finite Element Analysis of Compression Holding step Considering Solidification for Semi-Solid Forging (반용융 단조에서 응고 현상을 고려한 가압유지 단계의 유한요소해석)

  • Park, J.C.;Park, H.J.;Cho, H.Y.
    • Journal of the Korean Society for Precision Engineering
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    • v.14 no.10
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    • pp.102-108
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    • 1997
  • The technology of Semi-Solid Forging (SSF) has been actively developed to fabricate near-net- shape products using light and hardly formable materials. Generally, the SSF process is composed of slug heating, forming, compression holding and ejecting step. After forming step in SSF, the slug is compressed during a certain holding time in order to be completely filled in the die cavity and be accelerated in solidification rate. This paper presents the analysis of temperature, solid fraction and shrinkage at compression holding step for a cylindrical slug, then predicts the solidification time to obtain the final shaped part. Enthalpy-based finite element analysis is performed to solve the heat transfer problem considering phase change in solidification.

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Effect of Processing Parameters on Direct Fabrication of Polycrystalline Silicon Wafer (다결정 실리콘 웨이퍼 직접제조에 대한 공정변수 영향)

  • Wi, Sung-Min;Lee, Jin-Seok;Jang, Bo-Yun;Kim, Joon-Soo;Ahn, Young-Soo;Yoon, Woo-Young
    • Journal of Korea Foundry Society
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    • v.33 no.4
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    • pp.157-161
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    • 2013
  • A ribbon-type polycrystalline silicon wafer was directly fabricated from liquid silicon via a novel technique for both a fast growth rate and large grain size by exploiting gas pressure. Effects of processing parameters such as moving speed of a dummy bar and the length of the solidification zone on continuous casting of the silicon wafer were investigated. Silicon melt extruded from the growth region in the case of a solidification zone with a length of 1cm due to incomplete solidification. In case of a solidification zone wieh a length of 2 cm, on the other hand, continuous casting of the wafer was impossible due to the volume expansion of silicon derived from the liquid-solid transformation in solidification zone. Consequently, the optimal length of the solidification zone was 1.5 cm for maintaining the position of the solid-liquid interface in the solidification zone. The silicon wafer could be continuously casted when the moving speed of the dummy bar was 6 cm/min, but liquid silicon extruded from the growth region without solidification when the moving speed of the dummy bar was ${\geq}$ 9 cm/min. This was due to a shift of the position of the solid-liquid interface from the solidification zone to the moving area. The present study reports experimental findings on a new direct growth system for obtaining silicon wafers with both high quality and productivity, as a candidate for an alternate route for the fabrication of ribbon-type silicon wafers.

A Study on Cooling Rate and Dendrite Arm Spacing of Gas Atomized $Al_{87.3}misch$ $metal_{8.3}Ni_{4.4}$ Powder (가스아토마이징된 $Al_{87.3}misch$ $metal_{8.3}Ni_{4.4}$ 분말의 냉각속도와 수지상 가지 가격에 관한 고찰)

  • Kim, Ji-Hun;Ye, Byung-Joon;Kim, Young-Hawn
    • Journal of Korea Foundry Society
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    • v.19 no.1
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    • pp.54-65
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    • 1999
  • The present work is an attempt to evaluate the relationship between dendrite arm spacing and average cooling rate in gasatomized $Al_{87.3}misch$ $metal_{8.3}Ni_{4.4}$ powder by means of the following methods. One is calculation of heat transfer coefficient and average cooling rate, which are derived from estimated particle velocity during gas-atomization. The other is measurement of secondary dendrite arm spacing, which are observed on the particle surface. Then, we make experimental equation for this relationship in case of permanent mold casting and compare it with similar equation in case of rapidly solidified powder. Both average cooling rates and solidification rates are considered to represent the variance of dendrite arm spacings in two types soidification route. Even though there is a considerable difference in each average cooling rate, the dendrite arm spacing values are similar in two cases; particle diameter, $100\;{\mu}m$, and casting width, 2.05 mm. It is because that each solidification route has similar solidification rate.

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Segregation Phenomenon of As-Cast and Heat Treatment Microstructures in Investment Casting of IN738LC Superalloy (IN738LC 초내열합금 정밀 주조의 주조 및 열처리 미세조직에 구성되는 성분 편석 현상)

  • Choe, Byung Hak;Han, Sung Hee;Kim, Dae Hyun;Ahn, Jong Kee;Lee, Jae Hyun
    • Korean Journal of Materials Research
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    • v.31 no.7
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    • pp.409-419
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    • 2021
  • The effect of solidification rate on micro-segregation in investment casting of IN738LC superalloy was studied. In Ni-based superalloys, the micro-segregation of solute atoms is formed due to limited diffusion during cast and solidification. The microstructure of cast Ni-based superalloys is largely divided into dendrite core of initial solidification and interdendrite of final solidification. In particular, mosaic shaped eutectic γ/γ' and carbides are formed in the interdendrite of the final solidification region in some cases. The micro-segregation phenomena formed in regions of dendrite core and interdendrite including eutectic γ/γ' and carbides were analyzed using OM, SEM/EDS and micro Vickers hardness. As a result of analysis, the lack of (Cr, W) and the accumulation of Ti were measured in the eutectic γ/γ', and the accumulation of (Cr, Mo) and the lack of Ti were measured in the interdendrite between dendrite and eutectic. Carbides formed in interdendritic region were composed of (Ti, W, Mo, C). The segregation applied to each microstructure is mainly due to the formation of γ' with Ni3(Al,Ti) composition. The Ni accumulation accompanied by Cr depletion, and the Ti accumulated in the eutectic region as a γ' forming elements. The Mo tends to diffuse out from the dendrite core to the interdendrite, and the W diffuse out from the interdendrite to the dendrite core. Therefore, the accumulation of Mo in the interdendrite and the deficiency of W occur in the eutectic region located in the interdendrite. Heat treatment makes the degree of the micro-segregation decrease due to the diffusion during solid solution. This study could be applied to the heat treatment technology for the micro-segregation control in cast Ni-based superalloys.

Heat Transfer Analysis on the Rapid Solidification Process of Atomized Metal Droplets (분무된 금속액적의 급속응고과정에 관한 열전달 해석)

  • 안종선;박병규;안상호
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.18 no.9
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    • pp.2404-2412
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    • 1994
  • A mathematical model has been developed for predicting kinematic, thermal, and solidification histories of atomized droplets during flight. Liquid droplet convective cooling, recalescence, equilibrium-state solidification, and solid-phase cooling were taken into account in the analysis of the solidification process. The spherical shell model was adopted where the heterogeneous nucleation is initiated from the whole surface of a droplet. The growth rate of the solid-liquid interface was determined from the theory of crystal growth kinetics with undercooling caused by the rapid solidification. The solid fraction after recalescence was obtained by using the integral method. The thermal responses of atomized droplets to gas velocity, particle size variation, and degree of undercooling were investigated through the parametric studies. It is possible to evaluate the solid fraction of the droplet according to flight distance and time in terms of a dimensionless parameter derived from the overall energy balance of the system. It is also found that the solid fraction at the end of recalescence is not dependent on the droplet size and nozzle exit velocity but on the degree of subcooling.