• Title/Summary/Keyword: Solid-liquid Interface

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A Study of Carbide Thapping and Growth in the Directional Solidification of MAR-M247 LC Super alloy (Ni기 초내열합금의 일방향 응고에서 탄화물의 Trapping과 성장 거동)

  • Lee, Jae-Hyeon;Jin, Geon;Lee, Yong-Tae;Choe, Seung-Ju
    • 연구논문집
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    • s.26
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    • pp.95-102
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    • 1996
  • The carbide growth behavior of MAR-M247 LC alloy was investigated by directional solidification and quench method. The carbide volume fraction, trapping and growth behavior were correlated with the growth rate. It was found that the carbide volume fraction decreases at slower growth rate. This decreasing was caused by lower solid-liquid interface trapping ability at the slower growth rate.

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Domain Structures of LiNbO3 Single Crystals Grown by Czochralski Method (Czochralski법에 의해 성장시킨 LiNbO3단결정의 Domain Structure)

  • 최종건;오근호
    • Journal of the Korean Ceramic Society
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    • v.25 no.6
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    • pp.699-703
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    • 1988
  • Domain structures of LiNbO3 crystals grown by Czochralski method were examined according to the growth axis and the rotational speed of crystals. Ring shape and split domain structures were revealed in Z-axis and Y-axis grown crystals respectively. It was found that the domain structures of grown crystals were closely related to the solid-liquid interface shape during growth.

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A Study on the Solidification and Purification of High Purity Aluminium Alternate Stirring Method (정역 회전법에 의한 고순도 알루미늄의 응고 및 정련에 관한 연구)

  • Kim, Wook;Lee, Joung-Ki;Baik, Hong-Koo;Heo, Seong-Gang
    • Journal of Korea Foundry Society
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    • v.12 no.3
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    • pp.220-229
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    • 1992
  • The degree of purification and the macrostructure of high purity aluminium were studied through the alternate stirring method in order to improve the nonuniformity of solute concentration in the unidirectional stirring method. The $2^3$ factorial design was done to examine the effects of experimental factors more qualitatively. In the relatively low stirring speed of 1500 rpm with alternate stirring mode, the uniform solute profile and refined grain structure were obtained due to strong washing effect and turbulent fluid flow. It was induced by the transition of the momentum boundary layer by alternation of the stirrer. It was concluded from this study that the alternate stirring mode was more effective to obtain the uniformity of solute even in the stirring speed of 1500 rpm. But the degree of purification decreased below the critical alternating period. When 2N(99.8wt.%) aluminium was used as the starting material the morphology of solid-liquid showed the cellular shape and the columnar grains were inclined to the direction of rotation. This inclined grain growth resulted from the difference of relative velocities of solid and liquid. The inclined angle was increased as the stirring speed increased and solidification proceeded. In the case of 4N aluminium, there was no inclined grain growth and it was confirmed from the macrostructure and SEM work that the morphology of solid-liquid interface was planar. From the factorial design, it was found that the alternate stirring mode showed poorer purification effect than that of unidirectional stirring mode at low speed(500 rpm). In addition, the factor that had the most significant effect on the degree of purification was the stirring speed.

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Numerical Simulation of Transport Phenomena for Laser Full Penetration Welding

  • Zhao, Hongbo;Qi, Huan
    • Journal of Welding and Joining
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    • v.35 no.2
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    • pp.13-22
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    • 2017
  • In laser full penetration welding process, full penetration hole(FPH) is formed as a result of force balance between the vapor pressure and the surface tension of the surrounding molten metal. In this work, a three-dimensional numerical model based on a conserved-mass level-set method is developed to simulate the transport phenomena during laser full penetration welding process, including full penetration keyhole dynamics. Ray trancing model is applied to simulate multi-reflection phenomena in the keyhole wall. The ghost fluid method and continuum method are used to deal with liquid/vapor interface and solid/liquid interface. The effects of processing parameters including laser power and scanning speed on the resultant full penetration hole diameter, laser energy distribution and energy absorption efficiency are studied. The model is validated against experimental results. The diameter of full penetration hole calculated by the simulation model agrees well with the coaxial images captured during laser welding of thin stainless steel plates. Numerical simulation results show that increase of laser power and decrease of welding speed can enlarge the full penetration hole, which decreases laser energy efficiency.

The control of poly-grain and internal cavities for high-quality $CaF_2$ single crystal growth of 6inch in diameter (고품질의 직경 6 inch 형석($CaF_2$)단결정 성장을 위한 poly-grain 및 내부 cavity제어)

  • Seo, Soo-Hyung;Joo, Kyoung;Auh, Keun-Ho
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.8 no.4
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    • pp.550-554
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    • 1998
  • We suggested the new method of thermal screen in Bridgman-Stockbarger method to control the polygrain, the internal cavities and solid-liquid (SL) interface. $CaF_2$ single crystal of 6 inch was grown perfectly when we adopted to use a graphite pipe and a ceramic warmer in the conditions of growth rate 2 mm/hr, vertical temperature of $14^{\circ}C$ for freezing and temperature of $1324^{\circ}C$ at conical tip of crucible. The light scattering phenomena occurred by internal cavities were controlled as decreasing the freezing rate to 2 mm/hr and/or as adopting the rotation of melt (7 rpm).

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Effects of Natural Convection on Macrosegregation of Directionally Solidified Off-Eutectic Composites (공정복합재료의 일방향응고시 용질편석에 미치는 자연대류의 영향)

  • Kim, Gi-Bae;Yun, Ui-Park
    • Korean Journal of Materials Research
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    • v.5 no.1
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    • pp.123-131
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    • 1995
  • Natural convection in bridgman growth and it's effect on macrosegregation in unidirectionally solidified off-eutectic alloys were examined in this study. AlCu off-eutectic alloys(27.5wt% ~35. 6wt% ) were solidified upward or downward for producing a different natural convection and then Cu concentrations of off-eutectic composites were measured as a function of solidified fraction. Solutal and temperature distributions ahead of the solid/liquid interface were measured on quenched specimen. When hypo-utectic AlCu alloys are directionally solidified with downward growth, considerable macrosegregation occurs due to flow induced by thermal and solutal convection in melt. Soultal convection affects the macrosegregation of hyper-eutectic AlCu alloys more severely than thermal convection. Solute composition at solid/liquid interface of offkutectic composites was eutectic and also temperature was near eutectic point without large undercooling.

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Effect of Na2CO3 Addition on Grain Growth Behavior and Solid-state Single Crystal Growth in the Na0.5Bi0.5TiO3-BaTiO3 System (Na0.5Bi0.5TiO3-BaTiO3 계에서 입자성장 및 고상단결정성장에 미치는 Na2CO3 첨가 효과)

  • Moon, Kyoung-Seok
    • Journal of Powder Materials
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    • v.25 no.2
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    • pp.104-108
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    • 2018
  • Grain-growth behavior in the $95Na_{1/2}Bi_{1/2}TiO_3-5BaTiO_3$ (mole fraction, NBT-5BT) system has been investigated with the addition of $Na_2CO_3$. When $Na_2CO_3$ is added to NBT-5BT, the growth rate is higher than desired and grains are already impinging each other during the initial stage of sintering. The grain size decreases as the sintering temperature increases. With the addition of $Na_2CO_3$, a liquid phase infiltrates the interfaces between grains during sintering. The interface structure can be changed to be more faceted and the interface migration rate can increase due to fast material transport through the liquid phase. As the sintering temperature increases, the impingement of abnormal grains increases because the number of abnormal grains increases. Therefore, the average grain size of abnormal grains can be decreased as the temperature increases. The phenomenon can provide evidence that grain coarsening in NBT-5BT with addition of $Na_2CO_3$ is governed by the growth of facet planes, which would occur via mixed control.

Performances of Anaerobic Sequencing Batch Reactor for Digestion of Municipal Sludge at the Conditions of Critical Solid-liquid Separation (혐기성 연속 회분식 공정에 의한 도시하수슬러지 소화시 고액분리 특성에 따른 처리효율평가)

  • Hur, Joon-Moo;Park, Jong-An
    • Journal of Environmental Health Sciences
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    • v.28 no.5
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    • pp.77-85
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    • 2002
  • The objective of this study was to evaluate the performances of the ASBR under critical conditions of solid-liquid separation, caused by extremely high solids concentration, for wider application of the ASBR to various wastes. The ASBRs and completely-mixed daily-fed control runs were operated using a municipal mixed sludge at 35$^{\circ}C$ and 55$^{\circ}C$. Conversion of completely-mixed daily-fed reactor to sequencing batch mode and changes in HRT of all ASBRs were easily achieved without adverse effect, regardless of digestion temperature. Solids accumulation was remarkable in the ASBRs, and directly affected by settleable solids concentration of the feed sludge. Noticeable difference in solids-liquid separation was that flotation thickening occurred in the mesophilic ASBRs, while gravity thickening was a predominant solid-liquid separation process in the thermophilic ASBRS. Solids profiles at the end of thickening step dramatically changed at solid-liquid interface, and slight difference in solids concentrations was observed within thickened sludge bed. Organics removals based on subnatant or supernatant after thickening always exceeded 80% in all reactors. Thickened sludge volume and gas production of the ASBRs affected mutually. Gas production increased as thickened sludge accumulated, and continuous gas evolution during thickening could cause thickened sludge to expand or resuspend. Thickened sludge volume exceeding a predetermined withdrawal level resulted in loss of organic solids as well as biomass during withdrawal step, leading to decrease in gas production ind SRT. Such an adverse mutual effect was significant in gravity thickening, while it was not sensitive in flotation thickening. Changes in organic loading had no significant effect on organic removals and gas production after build-up of solids in the ASBRs.

A Large Slipping Finite Element Model for Geosynthetics Interface Modeling

  • Yi, Chang-Tok
    • Geotechnical Engineering
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    • v.12 no.3
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    • pp.35-48
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    • 1996
  • Reinforced soil structures may experience large local movements between soil and reinforcement. The failure modes of a reinforced structure depend on several factors which are governed by deformation and slipping of the reinforcement. In some cases, pulling out of the reinforcement may occur instead of rupturing, The growing use of geosynthetic liner system for storage of solid and liquid wastes has led to a number of slope instability problems where the synthetic liner may undergo a large amount of stretching and slipping as a result of the loading. The conventional finite element model for the soil-reinforcement interface uses a zero thickness joint element with normal and shear stiffnesses and can only accommodate a small amount of deformation. When a large slippage occurs, the model provides an i ncorrect mechanism for deformation. This paper presents a new interface finite element model which is able to simulate a large amount of slippage between soil and reinforcement. The formulation of the model is presented and the capability of the model is demonstrated using illustrative examples.

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Modelling of ZMR process for fabrication of SOI (SOI소자 제죠를 위한 ZMR공정의 모델링)

  • 왕종회;김도현
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.5 no.2
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    • pp.100-108
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    • 1995
  • Heat transfer plays a critical role in determining interface location and shape in ZMR process, which is used for the fabrication of silicon - on - insulator structure. In this work, the two - dimensional pseudo - steady - state ZMR model has been developed that can simulate the heat transfer process during ZMR process. It contains the radiation, convection and conduction heat transfer and determines the interface shapes. Numerical solutions from the model include flow field in the molten zone, temperature field in the full SOl structure and the location of solid/liquid interface in the silicon thin film and silicon substrate. We examined the effects of the various system parameters on the temperature profiles and the interface shape.

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