• Title/Summary/Keyword: Slurry mixing

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Synthesis of Nanostructured Fe-Co Alloy Powders from Metal Salts

  • Lee, Young-Jung;Lee, Jea-Sung;Seo, Young-Ik;Kim, Young-Do
    • Journal of Powder Materials
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    • v.13 no.5 s.58
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    • pp.336-339
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    • 2006
  • Magnetic properties of nanostructured materials are affected in complicated manner by their microstructure such as pain size (or particle size), internal strain and crystal structure. Thus, studies on the synthesis of nanostructured materials with controlled microstructure are necessary fur a significant improvement in magnetic properties. In the present work, nanostructured Fe-Co alloy powders with a grain size of 50 nm were successfully fabricated from the powder mixtures of (99.9% purity) $FeCl_2$ and $CoCl_2$ by chemical solution mixing and hydrogen reduction.

Characteristics of HTS tube fabricated by centrifugal forming process (원심성형법으로 제조한 고온초전도 튜브의 특성 분석)

  • Jang, Gun-Eik;Park, Yong-Min
    • 한국초전도학회:학술대회논문집
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    • v.10
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    • pp.211-215
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    • 2000
  • Bi-2212 HTS tube was fabricated by CFP(Centrifugal Forming Process). Slury was prepared in the mixing ratio of 8:2 between powder and binder and ball-milled for 24 hrs. Slurry was initially charged into the rotating mold with 300${\sim}$450 rpm and heated at the temperature ranges of 840${\sim}$860$^{\circ}$C for partial melting to finally obtain a uniformly textured tube shape. It was observed the plate-like grains with more than 20 ${\mu}$m were well oriented along the rotating axis and the measured T$_c$ was around 67K. In this paper we will discuss and analyze the tube characteristics depending on many different processing parameters such as, powder composition, binder mixing ratio between powder and binder, motor speed, heating temperature and etc.

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Professional Engineer Yard - The construction example of deep cement mixing method for the soil improvement of soft ground in sports center structure foundation work around the mouth of Nakdong River (기술사 마당 - 낙동강(洛東江)주변의 체육센터시설물기초 연약지반(軟弱地盤)처리를 위한 DCMM 시공사례)

  • Cho, Kyoo-Yung;Kim, Jin-Eok;Jeong, Byeong-Chan
    • Journal of the Korean Professional Engineers Association
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    • v.44 no.6
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    • pp.45-50
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    • 2011
  • As the Deep Cement Mixing Method is composed of drilled natural soft soil structure and injected cement slurry to be mix together in it, the nature of excavated ground is influenced directly to the application of constructability. Also the nature of in situ soil is the main material, the mix design and construction work plan should be established before the investigation of soil which is performed through the whole site confirm the soil parameter before construction. The nature of investigated soil and water level as should be performed accurately.

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Effects of Concentrated Pig Slurry Using Membrane Filter on the Growth and Yield of Tomato in Nutriculture (막분리 돈분뇨 농축액비를 이용한 양액재배가 토마토의 생육과 수량에 미치는 영향)

  • Ryoo, Jong-Won;Seo, Woon-Kab
    • Journal of Animal Environmental Science
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    • v.14 no.2
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    • pp.119-128
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    • 2008
  • This experiment was conducted to investigate the effects of concentrated pig slurry using membrane filter on growth of tomato in nutriculture. Pig slurry was filtered by ultra filtration and concentrated by reverse osmosis process. Filtration of pig slurry was necessary to prevent the hose clogging in nutriculture. The concentrated pig slurry (CS) and nutrient solution (NS) were mixed by six different mixing ratios of 0:100, 20:80, 40:60, 60:40%, 80: 20 and 100%:0% based on nitrogen content. The chemical nutrient solution was the solution of National Horticulture Research Station for the growth of tomato. The concentration of nutrient solution was adjusted a range of $1.6{\sim}2.0mS/cm$ in EC. The plant height of tomato treated with CS 20+NS 80% was similar with NS 100% control plot. Plant height was highest in the plot of CS 20+NS 80%. The treatment of 100% concentrated pig slurry was lowest in the gowth characteristics of tomato. Number of cluster was very lower in 100% concentrated pig slurry compared with plot of chemical nutrient solution. In the beginning of growth stage, SPAD reading value was reduced in plot treated with CS 100%, but CS 20+NS 80% plot was higher compared to 100% concentrated pig slurry. SPAD value of tomato leaves was decreased as the amount of CS was increased. The SPAD value also in treatment of concentrated pig slurry was lower in the middle growth stage compared to control plot. The dry weight of stem and leaf were 107.4, 104.2g in plot of NS 100% and CS 20%+NS 80%, respectively. The fruit number and weight were decreased at high application plots of concentrated pig slurry, The fruit setting of tomato showed lowest in the plot treated with 100% concentrated pig slurry, and the growth of tomato severely decreased after application of 100% CS treatment. In conclusion, the growth characteristics such as plant height and fruit weight of tomato were not significantly different between the plots treated with mixture of 20% CS +80%NS and 100% nutrient solution treatment. In conclusion, the mixture solution of 20% of concentrated pig slurry and 80% of nutrient solution could be used as a nutrition solution of tomato nuticulture.

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Morphological Analysis of Engineered PCC by Gas-Liquid Mixing Conditions (기체-액체 혼합조건에 따른 Engineered PCC의 형태학적 분석)

  • Lee, Tai-Ju;Seo, Jin-Ho;Kim, Hyoung-Jin
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.43 no.3
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    • pp.113-120
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    • 2011
  • Precipitated calcium carbonate(PCC), particularly calcite crystal, is extensively used as a pigment, filler or extender in various industries such as paper, paint, textile, detergents, adhesives, rubber and plastics, food, cosmetics, and biomaterials. PCC is conventionally produced through the gas-liquid carbonation process, which consists on bubbling gaseous $CO_2$ through a concentrated calcium hydroxide slurry. This study is aimed to find some factors for controlling the morphology of engineered PCC in lab-scaled mixing batch. The experimental designs were based on temperature variables, $Ca(OH)_2$ concentration, $CO_2$ flow rate, and electrical conductivity. The model of engineered PCC morphology was finally controlled by adjustment of electrical conductivity(6.0~7.0 mS/cm) and $Ca(OH)_2$ concentration(10 g/L). Orthorhombic calcite crystals were mostly created at high concentration and electrical conductivity conditions because the increased ratio of $Ca^{2+}$ and $CO{_3}^{2-}$ ions affects the growth rate of orthorhombic faces. Excess calcium spices were contributed to the growth of faces in calcium carbonate crystal, and the non-stoichiometric reaction was occurred between $Ca^{2+}$ and $CO{_3}^{2-}$ ions during carbonation process.

Characterization of SiC-SiC Whisker Matrix Retaining Electrolyte in Phosphoric Acid Fuel Cell (인산형 연료전지용 SiC-SiC Whisker 전해질 매트릭스의 특성)

  • 윤기현;이현임;이근행;김창수
    • Journal of the Korean Ceramic Society
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    • v.29 no.8
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    • pp.587-592
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    • 1992
  • Sheets of SiC-SiC whisker maxed matrix were prepared from the mixed slurry of SiC whisker and SiC matrix by the rolling method. With the increase of SiC whisker, the pore size, the porosity and the phosphoric acid absorbency of the matrix were increased, while the bubble pressure was decreased. The activation energy for the transfer of H+ ion was decreased with the increase of mixing ratio of SiC whisker to the SiC matrix from the measurement of hydrogen ion conductivity. The activation energy was evaluated as 0.25 eV when the mixing ratio of SiC whisker to the SiC matrix was 1 : 2 and the activation energy was 0.16 eV for the 2 : 1 matrix. It means that SiC whisker matrix contributes to attain a better microstructure for the diffusion of hydrogen ion. From the measurement of single cell performance of matrix with various mixing ratio, it is concluded that if SiC-SiC whisker maxed matrix has a sufficient bubble pressure to prevent the crossover of H2 gas, the current density of a fuel cell is increased with the increase of acid absorbency of the matrix. Current density was improved from 140 mA/$\textrm{cm}^2$ for 0.25 mm thickness of matrix to 170 mA/$\textrm{cm}^2$ for the 0.20 mm one at 700 mV.

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Impurity Pick-Up for the Preparation of NiCuZn Ferrite Powder Using Ball Milling Process (NiCuZn Ferrite 분말제조에 있어서 Ball Mill 분쇄 공정 중에 혼입되는 불순물의 함량)

  • 고재천;류병환
    • Journal of the Korean Magnetics Society
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    • v.9 no.4
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    • pp.217-222
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    • 1999
  • The pick up impurity was studied for preparing the NiCuZn ferrite powder by a ball milling method that usually uses in the industrial ceramic process. The raw materials of NiO, CuO, ZnO, and $Fe_2O_3$ powder were weighted according to various spinel composition and mixed for 18 hrs by a wet ball milling method after that the slurry was followed by spray dried and calcined at $700^{\circ}C$ 3 hrs. The calcined NCZF powder was finally ball milled during 65 hrs as same method. The stainless steel ball and jar are used as mixing and milling equipment and the solid concentration of the slurry was 25 vol%. The impurities, stainless steel pickup, were effected by the composition of raw materials especially iron oxide, nickel oxide in the mixing process and by the rate of calcine of NiCuZn ferrite in final milling process. The empirical equation of stainless steel pickup was driven in the wet ball milling system. Finally, the composition of NiCuZn ferrite could be controlled by the empirical equation.

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A Study on Fabrication and Characterization of Inorganic Insulation Material by Hydrothermal Synthesis Method (1) (수열합성법을 이용한 무기계 단열소재 제조방법 및 특성에 관한 연구 (1))

  • Seo, Sung-Kwan;Chu, Yong-Sik;Lee, Jong-Kyu;Song, Hun;Park, Jae-Wan
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.1 no.3
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    • pp.219-224
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    • 2013
  • In this study, the inorganic insulating material was fabricated with quartzite, ordinary portland cement(OPC), lime and anhydrous gypsum. After characteristic analysis of slurry, the optimum mixing ratio was derived with different $CaO/SiO_2$ mole ratio. Based on derived mixing ratio, the inorganic insulating material was fabricated at different water content and hydrothermal synthesis conditions. Specific gravity was $0.26g/cm^3$, compressive strength was 0.4 MPa, and thermal conductivity was 0.064 W/mK. This properties were enhanced performance of conventional ALC (Autoclaved Lightweight Concrete). And it can replace organic insulation with harmless inorganic insulation through continues research and development.

Treatment of Phenol Contaminated Soil Using Sulfidated Zero-Valent Iron as a Persulfate Activator for Advanced Oxidation Process (황화영가철 기반의 과황산 고도산화공정을 이용한 페놀 오염토양 처리)

  • Hyuk Sung Chung;Nguyen Quoc Bien;Jae Young Choi;Inseong Hwang
    • Journal of Soil and Groundwater Environment
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    • v.28 no.1
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    • pp.15-24
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    • 2023
  • A persulfate(PS)/sulfidated microscale zero-valent iron(S-mZVI) system was tested for treating a soil contaminated with phenol. Sulfidation of bare mZVI was conducted using a mechanochemical process utilizing a ball mill in order to improve persulfate activation capacity and stability of unmodified mZVI. The synthesized S-mZVI performed markedly better than the bare mZVI in activating PS. The optimum molar ratio of sulfur to mZVI was around 0.12. In the soil slurry experiments, a very rapid and complete removal of phenol was observed at the optimum molar ratios of PS to S-mZVI of 2:1 and PS to phenol of 16:1. The phenol removal efficiencies decreased as the water content of the slurries decreased. This was believed to be due to increased soil oxidant demand as the amount of soil was increased as relative to the water content. To evaluate the field applicability of the process, slurry experiments adopting high soil contents were carried out that simulated in-situ soil mixing conditions. These experiments resulted in substantially compromised degradation efficiencies of 54.3% and 43.8% within 4 hours. The current study generally shows that the PS/S-mZVI process has a potential to be developed into a remediation technology for soils contaminated with organics.

The Effect of Storage Container Types on Odor Emission and Quality of Piggery Liquid Slurry Fertilizer in the farms (농가의 돈분액비 저장형태가 악취발생과 액비품질에 미치는 영향)

  • Park, Moo-Eon;Kang, An-Seok;Kim, Si-Chang
    • Korean Journal of Soil Science and Fertilizer
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    • v.39 no.3
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    • pp.136-143
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    • 2006
  • The study was carried out to evaluate odor emission during storage time and quality of liquid slurry fertilizer along with three storage container types installed at farmer's fields in Cheorwon. Liquid slurry manure stored in the liquid-circulated or the air-injected tank was very homogeneous in concentration of nutritional elements because of well mixing operation, while nutritional concentration of the manure stored in the non-treated tank was significantly different from top to bottom in the tank, which may bring about partially irregular growth of plant after its application. The potential capacity of offensive odor emitted from liquid slurry manure stored in the liquid-circulated or the air-injected tank was much lower than that emitted from manure stored in the non-treated tank. Low potential capacity may less emit offensive odor after application of piggery liquid slurry on the field. The efficiency in oder to reduce odor emission from liquid manure was slightly higher in the liquid-circulated tank than the air-injected tank