• 제목/요약/키워드: Size-characterization

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졸-겔법에 의한 Mullite 코팅막의 제조 및 특성에 관한 연구 (A Study on Preparation and Characterization of Mullite Coated Film by Sol-Gel Process)

  • 이용택;최영우;양중식
    • 한국세라믹학회지
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    • 제34권6호
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    • pp.611-619
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    • 1997
  • Optimal Mullite sol was synthesized by sol-gel process using Aluminium sec-butoxide(ASB), Tetraethoxysilane(TEOS) and then, Mullite films were dip-coated with various holding time in sol bath and heat-treated at 130$0^{\circ}C$ above for crystallization. The thickness of coated film increased linearly with holding time in sol bath and average pore size was controllable within 20~30$\AA$.

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Determination of the Size Distribution of Magnetite Nanoparticles from Magnetic Measurements

  • Yoon, Sung-Hyun
    • Journal of Magnetics
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    • 제16권4호
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    • pp.368-373
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    • 2011
  • Particle size distributions in 10 nm magnetite ferrofluids are analyzed based on both dc and ac magnetic measurements. Modified log-normal distributions are used for fitting the experimental results, which allows for a proper account of the narrow distributions. The calculated average particle sizes are in good agreement with the TEM results. However the ac method gives a much narrower distribution width than that of the dc magnetization curve fit. The proposed measurements combined with the analysis methods are useful for the characterization of ferrofluids being considered for biomedical applications.

용질배제 곡선에 의한 한외여과 막의 세공특성 예측 (Prediction of Intrinsic Pore Properties of Ultrafiltration Membrane by Solute Rejection Curves)

  • 염경호
    • 한국막학회:학술대회논문집
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    • 한국막학회 1991년도 추계 총회 및 학술발표회
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    • pp.4-8
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    • 1991
  • The characterization of pore properties (mean pore size and pore size distribution) of the active layer in a UF membrane is important not only in order to obtain information about the factors affecting pore formation during membrane manufacturing but also to understand deeply the mechanism of solute and solvent transport through pores. Many methods of characterizing quantitatively the pore properties of UF membranes have been suggested in the literature: solvent and gas flow measurement, bubble point determination, electron microscopy, gas adsorption/desorption measurement, rejection measurement etc. But most of these methods involve time-consuming procedures and involve some wellknown problems and uncertainties.

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저압 임팩터를 이용한 대기 에어로졸 입자의 입경분포 측정과 화학조성 자료의 해석 (Characterization of Chemical Composition and Size Distribution of Atmospheric Aerosols by Low-Pressure Impactor)

  • 박정호;최금찬
    • 한국대기환경학회지
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    • 제13권6호
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    • pp.475-486
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    • 1997
  • The characteristics of atmospheric aerosols were investigated as a function of particle size and water solubility. The atmospheric aerosols were sampled with classifying into 12 size ranges by the use of Andersen low-pressure impactor. Collected aerosol particles were extracted by ultrapure water and filtered to be separated into water-soluble and insoluble components. The concentrations 12 elements in both components were determined by PIXE analysis. And the concentrations of 8 ions in the soluble component were analyzed by ion chromatography. In general, the mass size distribution of particulate matter was represented as a bimodal distribution. The mass size distributions of S$(SO_4^{2-}), K(K^+), Zn and NH_4^+$ skewed to the smaller size range and those of Si, Ca$(Ca^{2+}), Fe, Na^+ and Mg^{2+}$ skewed to the larger size range. They had roughly one peak in the fine and coarse particle region,respectively. On the other hand, the mass size distribution of Ti, Mn, Ni, Cu, $Cl^- and NO_3^-$ were represented as the bimodal distribution. Fe and Si in the aerosol particles extracted into pure water are existing in high insoluble state. Conversely, almost the whole of S is dissolved in water.

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Isolation and Characterization of the Smallest Bacteriophage P4 Derivatives Packaged into P4-Size Head in Bacteriophage P2-P4 System

  • Kim, Kyoung-Jin;Song, Jae-Ho
    • Journal of Microbiology
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    • 제44권5호
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    • pp.530-536
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    • 2006
  • Bacteriophage P4, a satellite phage of coliphage P2, is a very useful experimental tool for the study of viral capsid assembly and cos-cleavage. For an in vitro cos-cleavage reaction study of the P2-P4 system, new shortened and selectable markers containing P4 derivative plasm ids were designed as a substrate molecules. They were constructed by swapping the non-essential segment of P4 DNA for either the kanamycin resistance (kmr) gene or the ampicillin resistance (apr) gene. The size of the genomes of the resulting markers were 82% (P4 ash8 delRI:: kmr) and 79% (P4 ash8 delRI:: apr) of the wild type P4 genome. To determine the lower limit of genome size that could be packaged into the small P4-size bead, these shortened P4 plasmids were converted to phage particles with infection of the helper phage P2. The conversion of plasmid P4 derivatives to bacteriophage particles was verified by the heat stability test and the burst size determination experiment. CsCl buoyant equilibrium density gradient experiments confirmed not only the genome size of the viable phage form of shortened P4 derivatives, but also their packaging into the small P4-size head. P4 ash8 delRI:: apr turned out to be the smallest P4 genome that can be packaged into P4-sized head.

폴리에테르술폰 정밀여과막의 제조 및 특성 연구 (Preparation and Characteristics of Polyethersulfone Microfiltration Membranes)

  • 김노원
    • 멤브레인
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    • 제17권4호
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    • pp.329-337
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    • 2007
  • 본 연구에서는 p-toluenesulfonic acid (TSA)와 polyvinylpyrrolidone (PVP)를 함유한 polyethersulfone (PES) 고분자 용액을 이용하여 PES 멤브레인 내에 최소 공경을 갖는 내부 분리층을 만드는 방법에 관한 새로운 방법을 제시하고자 한다. 팽윤제로 사용된 PVP와 응고제로 사용된 TSA를 함유한 평막형 PES 멤브레인의 제조 및 구조적인 특성 조사가 수행되었으며, 상업용 막에 대등할 만한 투과 성능과 좁은 pore size distribution을 가지는 멤브레인을 제조할 수 있음을 확인하였다. 또한 PVP의 첨가는 멤브레인의 단면구조와 투과 성능에, TSA는 투과 성능보다는 pore size distribution에 영향을 준다는 것을 확인하였으며 이는 FE-SEM 결과와 TSA를 첨가한 멤브레인의 단면 사진에서 내부 최소 기공층의 두께가 두꺼워짐을 확인할 수 있었다.

저방사화 페라이트강(RAFs)의 파괴인성 및 피로균열진전 특성 (Characterization of the fracture toughness and fatigue crack propagation of reduced activation ferritic steel(RAFs))

  • 김동현;윤한기;김사웅
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2004년도 춘계학술대회
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    • pp.13-18
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    • 2004
  • The objective of this study is to investigate fracture toughness and fatigue crack propagation behavior in the Reduced Activation Ferritic Steel (RAFs) JLF-I. The fracture toughness tests were performed with various size(plane size and thickness) and various side groove of specimens. The fatigue crack propagation behavior of the JLF-I steel was investigated by the constant-amplitude loading test for the stress ratios R=O.I, 0.3 and 0.5 respectively. The effects of stress ratios and specimen size on the fatigue crack growth behaviors for JLF-I steel were discussed within the Paris law. The test results showed the standard CT specimen with the side groove of 40 % represented a valid fracture toughness. The fracture resistance curve increased with increasing plane size and decreased with increasing thickness. However, the fracture resistance curve of half size specimen was similar to that of the standard specimen. The fatigue crack propagation rate of a half size specimen was similar to that of a full size specimen at the stress ratios of 0.1, 0.3 and 0.5 respectively. The fatigue crack propagation behavior of this material were evaluated by using a half size specimen.

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Enhancement of Dissolution from Pharmaceutical Preparation of Hydrophobic Drugs ( I ) -Characteristics of Sulpiride-Polyethylene Glycol Coprecipitates-

  • Ku, Young-Soon
    • Journal of Pharmaceutical Investigation
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    • 제12권4호
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    • pp.145-152
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    • 1982
  • Data from IR spectroscopy and X-ray diffractometry were used for the characterization of sulpiride polyethylene glycol coprecipitates related with polymorphism of sulpiride. Sulpiride Form II transformed to Form I during coprecipitating with polyethylene glycol and the transformation rate is increased in proportion to molecular size of polyethylene glycol and the content of polyethylene glycol in coprecipitate.

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