• Title/Summary/Keyword: Size-characterization

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Fabrication and Characterization of MEA (MEA의 제작 및 특성 평가)

  • Seong, Nak-Seon;Pak, Jung-Ho
    • Proceedings of the KIEE Conference
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    • 2000.11d
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    • pp.857-859
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    • 2000
  • A planar MEA(Multi-channel Electrode Array) has been developed for monitoring the electrical activity of electrogenic cells in a cell culture by an extracellular recording. The material, fabrication process, characterization of the array, cleaning effect and impedance according to opening size by impedance measurement are described.

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Fabrication of caterpillar mixer and its surface characterization (캐터필러형 믹서의 제작 및 표면 특성 연구)

  • Han Chang-Soo;Park June-Ki;Yoon Yeo-Hwan
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2006.05a
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    • pp.541-542
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    • 2006
  • A micro-size caterpillar mixer has been recently used fur desktop chemical factory and so attractive due to small investment fund for arranging the factory and high efficiency by mixing in sub micro-level region. We report the fabrication of caterpillar mixer and its surface treatment for enhancement of mixing performance. We used the

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Characterization of Spherical Particles by Light Scattering

  • Sangwook Park;Jungmoon Sung;Taihyun Chang
    • Bulletin of the Korean Chemical Society
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    • v.12 no.3
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    • pp.322-328
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    • 1991
  • We have studied a characterization method of accurate size of spherical particles by fitting experimental light scattering profile to the rigorous theoretical scattering function. An efficient software has been developed for computation of the theoretical scattering function and regression analysis. A light scattering instrument has been built and the necessary data acquisition and analysis are carried out by use of a personal computer with an emphasis on the reduction of analysis and time aiming that this study will be extended toward a development of a practical particle sizing apparatus. The performance of the instrument and the software has been evaluated with latex spheres and found to be satisfactory.

Strategy of the Fracture Network Characterization for Groundwater Modeling

  • Ji, Sung-Hoon;Park, Young-Jin;Lee, Kang-Kun;Kim, Kyoung-Su
    • Proceedings of the Korean Radioactive Waste Society Conference
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    • 2009.06a
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    • pp.186-186
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    • 2009
  • The characterization strategy of fracture networks are classified into a deterministic or statistical characterization according to the type of required information. A deterministic characterization is most efficient for a sparsely fractured system, while the statistics are sufficient for densely fractured rock. In this study, the ensemble mean and variability of the effective connectivity is systematically analyzed with various density values for different network structures of a power law size distribution. The results of high resolution Monte Carlo analyses show that statistical characteristics can be a necessary information to determine the transport properties of a fracture system when fracture density is greater than a percolation threshold. When the percolation probability (II) approaches unity with increasing fracture density, the effective connectivity of the network can be safely estimated using statistics only (sufficient condition). It is inferred from conditional simulations that deterministic information for main pathways can reduce the uncertainty in estimation of system properties when the network becomes denser. Overall results imply that most pathways need to be identified when II < 0.5 statistics are sufficient when II $\rightarrow$ 1 and statistics are necessary and the identification of main pathways can significantly reduce the uncertainty in estimation of transport properties when 0.5$\ll$1. It is suggested that the proper estimation of the percolation probability of a fracture network is a prerequisite for an appropriate conceptualization and further characterization.

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Identification and Three-Dimensional Characterization of Micropore Networks Developed in Granite using Micro-Focus X-ray CT

  • Choo, Chang-Oh;Takahashi, Manabu;Jeong, Gyo-Cheol
    • The Journal of Engineering Geology
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    • v.24 no.2
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    • pp.179-189
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    • 2014
  • We analyzed the three-dimensional distribution of micropores and internal structures in both fresh and weathered granite using micro-focus X-ray computed tomography (micro-CT). Results show that the pore radius in fresh granite is mostly in the range of $17-50{\mu}m$, the throat radius is in the range of $5-25{\mu}m$, and the coordination number (CN) of pores is less than 10. In contrast, the pore radius in weathered granite is mostly in the range of $20-80{\mu}m$, the throat radius is in the range of $8-30{\mu}m$, and the CN is less than 12. In general, a positive linear relationship exists between pore radius and CN. In addition, both the size and the density of pores increase with an increasing degree of rock weathering. The size of the throats that connect the pores also increases with an increasing degree of weathering, which induces fracture propagation in rocks. Micro-CT is a powerful and versatile approach for investigating the three-dimensional distributions of pores and fracture structures in rocks, and for quantitatively assessing the degree of pore connectivity.

Synthesis of Nanosized Titanium-Colloid by Sol-Gel Method and Characterization of Zinc Phosphating (졸-겔법에 의한 나노크기의 티탄-콜로이드 합성 및 인산염 피막 특성)

  • Lee Man Sig;Lee Sun-Do
    • Journal of the Korean institute of surface engineering
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    • v.38 no.1
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    • pp.37-43
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    • 2005
  • Nanosized titanium-colloid particles were prepared by sol-gel method. The physical properties, such as thermal stability, crystallite size and crystallinity according to synthesis condition have been investigated by TEM, XRD, SEM, TGA and DTA. In addition, Zinc phosphating has been studied in order to compare the phosphating characterization of prepared nanosized titanium-colloid particles. The major phase of all the prepared titanium-colloid particles was an amorphous structure regardless of synthesis temperature and the structure was composed of phoshate complex and titanium. The micrographs of HR- TEM showed that nanosized titanium-colloid particles possessed a spherical morphology with a narrow size distribution. The crystallite size of the titanium-colloid particles synthesized at 80℃ was 4-5 nm and increased to 8-10 nm with an increase of synthesis temperature (150℃). In addition, the coating weight increased with an increase of temperature of phosphating solution and when the concentration of titanium-colloid was 2.0 g/l, the coating weight was 1.0 g/㎡.

Characterization of a Begomovirus-Betasatellite Complex, Producing Defective Molecules in Spinach (Spinacia oleracea L.), a New Host for Begomovirus and Betasatellite Complex in Pakistan

  • Tahir, Muhammad Nouman;Hameed, Amir;Amin, Imran;Mansoor, Shahid
    • The Plant Pathology Journal
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    • v.33 no.5
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    • pp.514-521
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    • 2017
  • Spinach is a vegetable crop which is widely grown over a large area especially in Punjab province of Pakistan. Leaf curling and enations on spinach plant collected shown to be associated with the begomovirus Pedilanthus leaf curl virus (PeLCV) and Shahdadpur strain of Cotton leaf curl Multan betasatellite ($CLCuMB^{Sha}$). Defective molecules of half and quarter size derived from monopartite begomoviruses are usually generated by the deletion of virion-sense sequences. Characterization of defective molecules of PeLCV from spinach revealed that the molecules of half the size are derived from the deletion of complementary-sense genes while quarter size molecule appears to have evolved by further deletion. This is the first report of the begomovirus-betasatellite complex on spinach and unusual defective molecules derived from deletion of complementary-sense genes in Pakistan.

PHYSICOCHEMICAL CHARACTERIZATION OF UASB GRANULAR SLUDGE WITH DIFFERENT SIZE DISTRIBUTIONS

  • 안영희;송영진;이유진;박성훈
    • Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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    • 2001.04a
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    • pp.172-181
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    • 2001
  • Upflow anaerobic sludge blanket (UASB) system employs granular sludge to treat various wastewaters including landfill leachate. CH$_4$ production of the granules determines overall performance of a UASB reactor. Sludge granules are developed by self-granulation of microorganisms and dynamic balance between granule growth and decay results in coexistence of granules with different sizes in the reactor. In this study, granules taken from a laboratory-scale UASB reactor were classified into 4 groups based on their diameters and their Physicochemical characteristics we were investigated. Each group was analyzed for settling ability, specific methanogenic activity (SMA), and elemental content. Settling ability was proportional to granule diameter. suggesting effective detainment of larger granules in the reactor. When acetate or glucose was used as a substrate, all groups showed relatively slight difference in SMA. However SMA with a volatile fatty acid mixture showed significant increase with granule diameter, suggesting better establishment of syntrophic relationship in larger granules. Larger granules showed higher value of SMA upon environmental changes (i.e., PH, temperature, or toxicant concentration). Comparative analysis of elemental contents showed that content (dry weight %) of most tested elements (iron, calcium, phosphorus, zinc, nickel. and manganese) deceased with granule diameter, suggesting importance of these elements for initial granulation. Taken together, this study verified experimentally that Physicochemical Properties of granules are related to granule size distributions. Overall results of physicochemical characterization supports that larger.

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Characterization of Photoelectron Behavior of Working Electrodes with the Titanium Dioxide Window Layer in Dye-sensitized Solar Cells

  • Gong, Jaeseok;Choi, Yoonsoo;Lim, Yeongjin;Choi, Hyonkwang;Jeon, Minhyon
    • Proceedings of the Korean Vacuum Society Conference
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    • 2014.02a
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    • pp.346.1-346.1
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    • 2014
  • Porous nano crystalline $TiO_2$ is currently used as a working electrode in a dye-sensitized solar cell (DSSC). The conventional working electrode is comprised of absorption layer (particle size:~20 nm) and scattering layer (particle size:~300 nm). We inserted window layer with 10 nm particle size in order to increase transmittance and specific surface area of $TiO_2$. The electrochemical impedance spectroscope analysis was conducted to analysis characterization of the electronic behavior. The Bode phase plot and Nyquist plot were interpreted to confirm the internal resistance caused by the insertion of window layer and carrier lifetime. The photocurrent that occurred in working electrode, which is caused by rise in specific surface area, increased. Accordingly, it was found that insertion of window layer in the working electrode lead to not only effectively transmitting the light, but also increasing of specific surface area. Therefore, it was concluded that insertion of window layer contributes to high conversion efficiency of DSSCs.

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