• Title/Summary/Keyword: Size-characterization

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Characterization of Microscale Objects based on the Diffraction Pattern Analysis (회절무늬를 이용한 미세물체의 특성 측정)

  • 강기호;전형욱;손정영;오명환
    • Korean Journal of Optics and Photonics
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    • v.2 no.1
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    • pp.1-6
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    • 1991
  • This paper describes the theoretical analysis of a diffraction pattern analyzer for the characterization of microscale object fields and a method for obtaining size and size distribution from the measured diffraction pattern of the object fields. For the experimental verification, a typical optical Fourier transform system was set up and calibrated with 2 5$\mu \textrm m$ and 50$\mu \textrm m$ pinholes. The system responses to distilled water droplets, alcohol, glycerin and silicon oil were imaged with vidicon, and the image was processed to determine the size distribution of each liquid particle field. The energy distribution function which is defined as the total intensity of a circular ring in the diffraction pattern was used to determine the dominant particle size of each liquid particle field.

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In-situ Particle Characterization of Cu Nanopowder using Scanning Mobility Particle Sizer in Pulsed Wire Evaporation Method (전기폭발법에서 SMPS를 이용한 Cu 나노분말의 실시간 입자특성평가)

  • 이창우;맹덕영;박중학;유지훈;이재훈;이창규;김흥회
    • Journal of Powder Materials
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    • v.10 no.4
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    • pp.275-280
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    • 2003
  • Synthesis and characteristics of Cu nanopowder were considered by in-situ characterization method using SMPS in pulsed wire evaporation process. With increasing pressure in chamber, particle size and degree of agglomeration increased by increase of collision frequency. Also, it was found from the XRD analyses and BET measurements that crystallite size and particle size decreased with elevating applied voltage. However, SMPS measurements and TEM observation revealed the increase of particle size and degree of agglomeration with increase of applied voltage. These results suggested that particle growth and agglomeration depend on overheating factor in chamber at the early stage and thermal coagulation in filtering system during powder formation until collection.

Analysis of Discontinuity Distribution Property to Predict Rock Slope Failure (암반 사면의 파괴 예측을 위한 불연속면 분포 특성 분석)

  • 윤운상;김정환;배기훈
    • Proceedings of the Korean Geotechical Society Conference
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    • 1999.10a
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    • pp.147-152
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    • 1999
  • Distribution of fracture system is an important factor to analyse instability of jointed rock slope. In the most case of rock slopes, joint distribution properties are related to potential, shape, size and locality of slope failure. The purpose of this paper is to present an application of fracture characterization related to rock slope failure. Fracture data used in this study are collected by scanline survey. Two aspects of fracture characterization for rock slope are handled in this study First, In order to determine the potential and shape of slope failure, trace length of joints is considered as the weighting factor about collected orientation data. Second, Relationship between trace length and spacing is analysed to estimate failure location and size. The distribution of fracture system is directly influenced on wedge failure. It is effective to analyse the orientation of fractures by using weighting factors associated with the trace length of fractures rather than to analyse only that of fractures. It gives a conclusion that the wedge failure occurred along the peak of fracture density(or intensity) cycles.

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Influence of Silicon and Seed Particles on the Reconstruction Characteristics and Exaggerated Grain Growth of MgO Protective Layer by Over-Frequency Accelerated Discharge in ACPDPs

  • Kwon, Sang-Koo;Kim, Jeong-Ho;Moon, Seung-Kyu;Choi, Jong-Kwon;Park, Kyu-Ho;Han, Sung-Su
    • 한국정보디스플레이학회:학술대회논문집
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    • 2008.10a
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    • pp.957-960
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    • 2008
  • The influences of silicon and MgO seed particle on the reconstruction characteristics of MgO protective layer were investigated to clarify the mechanism of reconstruction and exaggerated grain growth (EGG) in AC-PDP. The reconstruction and EGG are closely correlated with the driving force for nucleation and growth, interface energy and initial size distribution of MgO protective layer in plasma space during discharge in AC-PDP.

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Size Characterization of Urban Airborne Particles Using Sedimentation/Steric Field-Flow Fractionation (Sd/StFFF)

  • Lee, Jae-Yong;Lee, Seung-Ho;Min, Young-Hong;Hyun, Dae-Yeung
    • Bulletin of the Korean Chemical Society
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    • v.24 no.8
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    • pp.1172-1176
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    • 2003
  • This study aims to investigate the applicability of Sd/StFFF and to develop a method for size characterization of urban airborne particles, focusing primarily on particles larger than about 1 mm. It was found that the airborne concentration vary with time, although no particular seasonal trend was observed. When averaged over time, the airborne concentration was the lowest in the park areas with 99 ㎍/m³. The apartment, industrial, and central city area showed similar levels of the airborne concentrations with 166, 170, and 171 ㎍/m³, respectively. The housing area showed the highest airborne concentration with 201 μg/m³ among all tested areas. A power-programmed Sd/StFFF was used for size analysis of airborne particles with the initial field strength of 300 rpm, $t_a$ = 4, $t_i$ = -16, p = 8, and the flow rate of 7 mL/min. It was found that urban airborne samples were mostly populated by particles having diameters between about 5 to 20 ㎛, although all have broad size distributions ranging up to about 50 ㎛. Under the Sd/StFFF condition used in this study, no significant differences were found in size distributions among the airborne particles collected at different urban sites, and also among those collected at different times.

Solvothermal synthesis and characterization of silver nanoparticles

  • Guptha, K. Venkateswara;Nesaraj, A. Samson
    • Advances in nano research
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    • v.2 no.3
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    • pp.147-155
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    • 2014
  • Among the various nanoparticles reported for commercial applications, considerable interest has been generated by the use of silver nanoparticles. Owning to extremely small size, silver nanoparticles exhibit enhanced properties when compared with the bulk material. In this research work, silver nanoparticles were prepared by the reduction of silver salt with a reducing agent by a solvothermal method using different solvent mediums such as ethanol, hexane, toluene and acetone with water. The prepared silver nanoparticles were characterized systematically by X-ray diffraction (XRD), particle size analysis and scanning electron microscope (SEM). The results revealed the formation of pure silver phase and nano-sized particles. Among the different solvent mediums used, the silver nanoparticles prepared by hexane and water as solvent mixture resulted in very low particle size.

A New Algorithm for Ghost Cancellation System (새로운 고스트 제거 알고리즘)

  • Park, Kyung-Bae;Hwang, Hu-Mor
    • Proceedings of the KIEE Conference
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    • 1995.07b
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    • pp.904-906
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    • 1995
  • Based on the detection of the size of datas of multipath channel characterization, we propose a new algorithm. called the impulse size based adaptive median filter(ISMF), for ghost cancellation system. The ISMF consists of two levels. The first one is the impulse noise size detection level and the second one is the adaptive median filtering level to remove the impulse noise detected. Test results confirm that the proposed ISMF removes impulse noise due to multipath channel characterization while preserving signal as well as ghosts so that the LMS algorithm performs effectively.

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Synthesis of Tungsten Carbide Powders by SHS Method (SHS법에 의한 탄화텅스텐 분말 합성)

  • Jun, H.B.;Cho, D.H.;Lee, H.B.;Park, S.
    • Journal of the Korean Ceramic Society
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    • v.31 no.10
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    • pp.1159-1168
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    • 1994
  • We powders were synthesized from W powders in differnet particle sizes by Self-propagating High-temperature Synthesis process (SHS) using a chemical furnace. The effects of the mole ratio of chemical fuel content, pellet thickness and the mole ratio between carbon and tungsten (C/W Ratio) on synthesis were investigated with the tungsten powders have different particle size each other. Compositional and structural characterization of these powders was carried out by scanning electron microscope (SEM0 and x-ray diffractometer. Powder characterization was carried out by the measurement of particle size distribution with laser-particle size analyzer. The amounts of WC obtained by SHS process depend very much on the particle size of tungsten powder and heat contents given in a product, i.e. as the particle size of W powder is smaller, the amounts of WC produced increase. Also the more heat contents is given, the more amounts of WC increase. By optimizing the synthesis conditions, it is possible to fabricate WC powders which have little secondary phases (W2C, C).

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The Influence of Aerosol Source Region on Size-resolved Hygroscopicity During the Asian Pacific Regional Aerosol Characterization Experiment (ACE-Asia) Campaign

  • Lee, Yong-Seob
    • Journal of Korean Society for Atmospheric Environment
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    • v.22 no.E1
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    • pp.9-18
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    • 2006
  • Aerosol hygroscopic properties were measured by a tandem differential mobility analyzer (TDMA) system during the Aerosol Characterization Experiment (ACE)-Asia campaign from 31 March to 1 May 2001. Two high flow differential mobility analyzers (DMAs) were used to maximize the count rate on board the Center for Interdisciplinary Remotely Piloted Aircraft (CIRPAS) Twin Otter aircraft. Hygroscopic growth factor distributions of particles having initial dry nanoparticle diameters of 0.040, 0.059, 0.086, 0.126, 0.186, 0.273, 0.400, and $0.586{\mu}m$ were measured during 19 research flights. Data collected during 12 of those flights were used to investigate aerosol mixing state and the influence of aerosol source region on size-resolved hygroscopicity. The uniformity in size-resolved hygroscopicity was quantified to facilitate comparison between measurements made in different air masses. Hygroscopic growth factors are strongly dependent on source region and sizes. Mean hygroscopic growth factors were observed to be greatest when the air mass origin was from the south. The mean growth factors for continental sources decreased with initial size from 1.47 to 1.27 for $0.040{\mu}m\;and\;0.586{\mu}m$, but increased with initial size from 1.44 to 1.8 for $0.040{\mu}m\;and\;0.400{\mu}m$ dry diameters for marine sources.