• 제목/요약/키워드: Size Reduction Ratio

검색결과 496건 처리시간 0.037초

습식분쇄에 의한 입자크기 변화에 따른 분쇄입자의 종횡비 거동 (Aspect Ratio Behavior of Grinding Particles with Variation of Particle Size by Wet Grinding)

  • 최진삼
    • 한국재료학회지
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    • 제30권5호
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    • pp.223-230
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    • 2020
  • As a case study on aspect ratio behavior, Kaolin, zeolite, TiO2, pozzolan and diatomaceous earth minerals are investigated using wet milling with 0.3 mm media. The grinding process using small media of 0.3 pai is suitable for current work processing applications. Primary particles with average particle size distribution D50, ~6 ㎛ are shifted to submicron size, D50 ~0.6 ㎛ after grinding. Grinding of particles is characterized by various size parameters such as sphericity as geometric shape, equivalent diameter, and average particle size distribution. Herein, we systematically provide an overview of factors affecting the primary particle size reduction. Energy consumption for grinding is determined using classical grinding laws, including Rittinger's and Kick's laws. Submicron size is obtained at maximum frictional shear stress. Alterations in properties of wettability, heat resistance, thermal conductivity, and adhesion increase with increasing particle surface area. In the comparison of the aspect ratio of the submicron powder, the air heat conductivity and the total heat release amount increase 68 % and 2 times, respectively.

Na환원법에 의한 희석제량에 따른 탄탈 분말 제조와 특성 (Characteristics and Production of Tantalum Powder on the amount of Diluent By Na Reduction Method)

  • 윤재식;박형호;배인성;김병일;정성만
    • 한국재료학회지
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    • 제12권9호
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    • pp.706-711
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    • 2002
  • High-pure tantalum powder was fabricated through Na reduction process and has been produced by using $K_2$TaF$_{7}$, and KCI, KF for raw material and diluent, respectively. A raw material and diluent were charged at the hestalloy bomb by the weight rate of 1:2, 1:1, 1:0.5 and 1:0.25 each other, investigated properties of morphology, chemical composition and yield and particle size after reduced. Ta metal has been achieved by reduction of $K_2$$TaF_{7}$ 500g with 1% sodium in excess of stoichiometric amount in the charge at a reduction temperature of $850^{\circ}C$ for 3hours. According to amount of the diluent, a formation of the powder doesn't have an effect. The diluent prevented the temperature rising caused from the heat of reaction and it maintained the speed of reducing reaction. But in the mixture ratio of raw material and diluent in the 1 : 2 and 1 : 0.25, an oxide and partially not reacted K were detected. As the amount of diluent increased, the size of tantalum powder decreased. According as raw material and the mixture ratio of diluent change from 1:0.25 to 1:2, the size is decreased from 5$\mu\textrm{m}$ to 1$\mu\textrm{m}$, and a particle size distribution which is below 325 mesh in fined powder increases from 71% to 83%. In the case of average size of Tantalum powder which is the mixture ratio (1:0.5), we would get the Ta powder with grain size about 3$\mu\textrm{m}$, which come close to the average size (2~4$\mu\textrm{m}$) of tantalum powder which is used commonly in the present is Ta powder about 3$\mu\textrm{m}$.

콜로이드 Ag 나노입자 합성시 계면활성제의 영향 (Effect of Surfactant on Synthesis of Colloidal Ag Nanoparticles)

  • 이종국;최남규;서동석
    • 한국재료학회지
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    • 제15권5호
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    • pp.340-347
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    • 2005
  • Silver nanoparticles were synthesized by chemical reduction method from aqueous silver nitrate solution ana hydrazine as a reduction agent. The morphology, particle size and shape were dependent on the mixing method, reaction temperature and time, molar ratio of hydrazine and silver nitrate, the kind of surfactant, and the addition of surfactant. The stability of the colloidal silver was achieved by the adsorption of surfactant molecules onto the particle. Silver nanoparticles have a characteristic absorption maximum at 430 nm under UV irradiation. It was found that the colloid was nanometer m size and formed very stable dispersion of silver. The Ag nanoparticles obtained showed the spherical shape with the size range of 10-30 nm.

척추측만증보조기 착용에 따른 만곡각도와 체질량지수의 관계 (Relationship Between Curvature Angle and BMI According to Wearing a Scoliosis Brace)

  • 이광호
    • 대한통합의학회지
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    • 제7권3호
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    • pp.149-157
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    • 2019
  • Purpose : This study aims to check the relationship between the size of curvature in scoliosis patients and the reduction rate of curvature after wearing a brace and the relationships of the size of curvature and correction angle with Body Mass Index (BMI). Methods : With 30 adolescent girls who had never worn a brace, their Cobb angle and BMI were measured before manufacturing braces, and their corrected Cobb angle was measured after wearing the manufactured scoliosis braces. Results : The size of the major curvature before wearing the brace and the reduction rate of the curvature after putting it on had a negative correlation in both the major curvature (r=-.465, p<.01) and the minor curvature (r=-.516, p<.01). The size of the minor curvature and the reduction rate of the minor curvature before and after putting it on also had a negative correlation (r=-.429, p<.05). As for the relationship between the size of curvature and BMI, they had a negative correlation in both the major curvature (r=-.141) and the minor curvature (r=-.123), and as for the relationship between the reduction rate of curvature and BMI after wearing the brace, they had a positive correlation in both the major curvature (r=.251) and the minor curvature (r=.136); however, it was not statistically significant (p>.05). Conclusion : In conclusion, the larger the size of curvature, the lower the reduction rate of curvature after wearing the brace became. The larger the size of curvature, the lower the BMI became. The higher the BMI, the higher the correction ratio of the brace became. Therefore, it is judged that it is necessary to provide early treatment and manage body composition before scoliosis progresses.

DEA 용액에서 암모니아를 함유한 염화니켈 수용액으로부터 니켈 분말의 입경 제어 (Size Control of Nickel Powders from Nickel Chloride Solution Containing Ammonia in DEA Solutions)

  • 최은영;이윤복;윤석영;김광호;김진천;임영목;김형국;김양도
    • 한국분말재료학회지
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    • 제12권3호
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    • pp.201-207
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    • 2005
  • Nickel powders were synthesized by the hydrazine reduction of nickel chloride solution containing ammonia in DEA solutions. The size distribution of nickel powders were investigated as a function of ammonia concentration, hydrazine concentration and the mixed composition ratio of diethanolammine (DEA) and triethanolammine (TEA). Nickel powders with the size in submicron range were obtained at $185^{\circ}C$ for 45 minutes by hydrazine reduction of nickel chloride solution in DEA solutions. The hydrazine concentrations showed significant effects on the particle size and shape distribution of nickel powders under $NH_3/Ni^{2+}$ molar ratio of 2.0 condition. As the mixed volume ratio of TEA and DEA increased, nickel powders with relatively larger particle size and low agglomeration were obtained. Nickel powders with particle size in the ranged from 0.4 to $0.9\;{\mu}m$ were obtained at the 50 $vol.%$ of TEA.

다중압출공정을 이용한 Cu-Ni-Zr-Ti 비정질 복합재의 미세조직제어 (Microstructure Control of Cu-Ni-Zr-Ti Metallic Glass Composites by Multi-Pass Extrusion Process)

  • 김택수;이진규
    • 소성∙가공
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    • 제16권5호통권95호
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    • pp.386-390
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    • 2007
  • In order to, simultaneously, synthesize and control the size of microstructure of amorphous/crystalline composites, a repeated extrusion process was performed using the gas atomized $Cu_{54}Ni_6Zr_{22}Ti_{18}$ metallic glass powders and the crystalline brasses. The size of microstructure in the resultant composites was varied depending on the pass of extrusion as well as on the area reduction ratio. The microstructure could be estimated using an equation of $r_n=r_{n-1}/R^{1/2}$, where R is reduction ratio and $r_n$ is the resultant radius of the extruded bar after n pass. Theory of microstructural refinement as well as the relationship between the resultant microstructures and mechanical properties was discussed.

FT-ICR 질량분석기의 신호 충실성 향상 (The Improvement in Signal Integrity of FT-ICR MS)

  • 김승용;김석윤;김현식
    • 전기학회논문지
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    • 제60권1호
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    • pp.201-204
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    • 2011
  • For efficient noise reduction in a Fourier transform ion cyclotron resonance (FT-ICR) mass spectrum, a new algorithm was proposed. The suggested algorithm reduces white and electrical noise, and it improves signal-to-noise ratio. This algorithm has been optimized to reduce the noise more efficiently using the traces of signal level. The algorithm has been efficiently combined with derivative window to improve the resolution as well S/N. Time domain data was corrected for DC voltage interference. $t^n$ window was applied in time domain data to improved the resolution. However, $t^n$ window can improve the signal resolution, it will also increase the noise level in frequency domain. Therefore, newly developed noise reduction algorithm will be applied to make a balance between resolving power and S/N ratio for magnitude mode. The trace algorithm can determine the current data point with several data points (mean, past data, calculated past data). In the current calculations, we assumed data points with S/N ratio more than 3 were considered as signal data points. After the windowing and noise reduction, both resolution and signal-to-noise ratio were improved. This algorithm is applicable more efficiently to frequency dependent noise and large size data.

Ultimate strength of stiffened plates with pitting corrosion

  • Rahbar-Ranji, Ahmad;Niamir, Nabi;Zarookian, Arvin
    • International Journal of Naval Architecture and Ocean Engineering
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    • 제7권3호
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    • pp.509-525
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    • 2015
  • Predicting residual strength of corroded plates is of crucial importance for service life estimation of aged structures. A series of nonlinear finite element method is employed for ultimate strength analysis of stiffened plates with pitting corrosion. Influential parameters, including plate thickness, type and size of stiffeners, pit depth and degree of pitting are varied and more than 208 finite element models are analyzed. It is found that ultimate strength is reduced by increasing pit depth to thickness ratio. Thin and intermediate plates have minimum and maximum reduction of ultimate strength with stronger stiffeners, respectively. In weak stiffener, reduction of ultimate strength in thin and intermediate plates depends on DOP. Reduction of ultimate strength in thick plates depends on thickness of plate and DOP. For intermediate plates, reduction for all stiffeners regardless of shape and size are the same.

정상인의 자세에 따른 자침 효과의 차이 (The Differential Effects of Acupuncture on Postures of Healthy Subjects)

  • 김지은;박경모
    • 대한의용생체공학회:의공학회지
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    • 제28권1호
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    • pp.46-54
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    • 2007
  • Objective: The first aim of this study is to determine the effects of acupuncture on the autonomic nervous system (ANS) via Heart Rate (HR) and Pupil Size (PS), and to compare the effects of acupuncture on the subjects' ANS when they are in a sitting position with the effects when they are in a supine position. Methods: Ten healthy male subjects were randomized to receive either verum acupuncture stimulation in a sitting position (SitV), verum acupuncture stimulation in a supine position (SupV), sham acupuncture stimulation in a sitting position (SitS), and sham acupuncture stimulation in a supine position (SupS). Acupuncture stimulation was applied to Neguan point (PC6) on the forearm. The subject's electrocardiogram (ECG) and pupil size were recorded continuously from 5 min before stimulation to 12 min after stimulation. Results: Verum and sham acupuncture stimulation were found to have reduced heart rate (p<0.01) and to have increased pupil size (p<0.01) in all the subjects. But when the reduction in HR and the increment in PS after verum acupuncture stimulation (both sitting and supine position) were compared with those after sham acupuncture stimulation, it was found that the reduction in HR (74.48 and 73.47 bpm, p<0.063) and the increment of PS (7.32 and, 6.10 mm, p<0.001) after verum acupuncture stimulation were greater than those after sham acupuncture stimulation, and that the corresponding values were statistically significant. In addition, at the baseline, it was found that the subjects had a larger PS and a faster HR in a sitting position than when they did so in a supine position. And then the reduction and increment ratio in the subject's HR and PS when they underwent acupuncture stimulation in a sitting position was significantly different from the reduction and increment in their HR and PS when they underwent the procedure in a supine position-i.e., the reduction ratio in HR was greater when they underwent the procedure in a sitting position, and such reduction ratio was statistically significant (p<0.05). As for the increment in PS, it was greater when the subjects underwent the procedure in a supine position, and such increment was significant (p<0.05). Conclusion: Manual acupuncture stimulation on Neguan point (PC6) has more significant influence on the autonomic nervous system rather than sham acupuncture (tactile stimulation). And the position-induced different states of ANS have different influence on the acupuncture effect.

날개형 및 격막형 배플을 이용한 유체저장탱크 내부의 슬로싱 저감 연구 (A Study on the Reduction of the Sloshing of Storage Tank Using Wing and Diaphragm Baffle)

  • 이영신;김현수;이재형;김영완;고성호
    • 대한기계학회논문집A
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    • 제27권12호
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    • pp.2039-2046
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    • 2003
  • Storage tank filled with fluid has unique dynamic characteristics compared to general structures, due to the interaction between fluid and structure. The oscillation of the fluid surface caused by external forces is called sloshing, which occurs in moving vehicles with contained liquid masses, such as trucks, railroad cars, aircrafts, and liquid missles. In this study, the evaluation method for the reduction of sloshing, the optimized size and location of wing and diaphragm baffles are suggested based on the experimental results. The experimental device can simulate the translation motion. A rectangular tank and various baffles are fabricated to study on the sloshing characteristics. The forces measured using the load cell at tank wall and those are compared with each other through the Fourier transformation for various conditions. The study of the sloshing of the rectangular tank equipped with baffles is conducted under the same conditions with non-baffled rectangular tank experiment. From the experimental results, the sloshing reduction effect by the baffles is observed. In conclusion in case of diaphragm baffles, the optimized size ratio of the width of baffle to the water height is 0.44 and the installation location has no effect to the damping of sloshing. In case of wing baffles, the optimized size ratio of the width of baffle to the length of a rectangular tank is 0.1 and the optimized location ratio of the baffle to the water height is 0.9.