• Korean Journal of Materials Research
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• v.6 no.1
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• pp.40-48
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• 1996

고주파 저손실 재질로 사용되고 있는 Mn-Zn 페라이트의 제조공정 중 소결조건과 Ta2O5첨가가 Mn-Zn 페라이트의전력손실에 미치는 영향에 대해서 연구하였다. 등조성선을 따라 냉각하기 위하여 컴퓨터를 사용해서 정확하게 산소분압을 조절하였으며 적절한 등조성선을 선택함으로써 보다 좋은 손실특성을 얻을 수 있었다. CaO-SiO2 첨가계에 Ta2O5를 0ppm에서 400ppm으로 변화시켜 가며 첨가하였으며, Ta2O5 가 400ppm 첨가되었을 경우 균일한 grain 성장과 더불어 낮은 전력손실을 나타내었다. 온도에 상응하는 상평형 산소분압을 정확히 맞춰 냉각할 경우 전력손실 최소값이 질소 분위기에서 냉각시킨 시편보다 높은 온도쪽으로 이동됨도 확인할 수 있었다.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2003.10a
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• pp.101-106
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• 2003

Recent electronic equipment becomes smaller, more functional, and more complex. According to these trends, LTCC(low temperature co-fired ceramic) has been emerged as a promising technology in packaging industry. It consists of multi-layer ceramic sheet, and the circuit has 3D structure. In this technology via hole formation plays an important role because it provides an electric path for the packaging interconnection network. Therefore via hole quality is very important for ensuring performance of LTCC product. Via holes are formed on the green sheet that consists of ceramic(before sintering) layer and PET(polyethylene Terephthalate) one. In this paper we found the correlation between hole quality and process condition such as ceramic thickness, and tool size. The shear behavior of double layer sheet by micro hole punching which is different from that of single layer one was also discussed.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 1995.05a
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• pp.9-13
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• 1995

The effect of WO$_3$ addition and sintering condition on the electrical properties of SrTiO$_3$ceramic have been investigated. Resistivity and capacitance of grains and grain boundaries were obtained by applying impedance spectroscopy. From the result it could be concluded that the temperature dependance of capacitance of WO$_3$doped specimens were influenced directly by the variation of grain boundary capacitance. It was also found that the dispersion frequency increased as the degree of reduction of the specimen increased. The dispersion frequency characteristics showed discernably that the resistivity of the specimen varied with WO$_3$ content. The dielectric properties were influenced directly by the reduction of the specimens. The dielectric constant of grain boundaries of BL capacitor could be obtained by Cole-Cole plot and was influeneced by the amount of WO$_3$ added.

• Journal of the Korean Ceramic Society
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• v.25 no.5
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• pp.552-560
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• 1988

ZnO low voltage varistor was obtained by varying a) the amount of seed grains, b) the size of seed grains, and c) sintering temperature. Also, the optimum condition for fabricating the ZnO seed grains was studied. Large ZnO seed grains were obtained by washing a ZnO sintered body containing 1m/of BaCO3 in boiling water. When the seed grains were added, abnormal grain growth occurred, and the varistor voltage sharply decreased. However, when more than 5w/o of seed grain content was added, the varistor voltage gradually increased. When 10w/o seed grains of 75~106${\mu}{\textrm}{m}$ were added and sintered for 2 hours at 1200 to 125$0^{\circ}C$, low voltage varistor properties with V1mA/mm of 19V/mm and nonlinear exponent ($\alpha$) of 12 occurred.

• Transactions of the Korean Society of Machine Tool Engineers
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• v.16 no.3
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• pp.64-74
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• 2007

The continuous chip in turning operation deteriorates precision of workpiece and causes a hazardous condition to operator. Thus the chip form control becomes a very important task for reliable machining process. So, grooved chip breaker is widely used to obtain reliable discontinuous chip. However, developing new cutting insert having chip breaker takes long time and needs lots of research expense due to a couple of processes such as forming, sintering, grinding and coating of product and many different evaluation tests. In this paper, performance of commercial chip breaker is evaluated with neural network which is learned with a back propagation algorithm. For the evaluation, several important elements(depth of cut, land, breadth, radius) which directly influence the chip formation were chosen among commercial chip breakers and were used as input values of neural network. With the results of these input values, the performance evaluation method was developed and applied that method to the commercial tools.

• Journal of the Korean Ceramic Society
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• v.29 no.5
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• pp.341-346
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• 1992

The effects of CaO addition on the low temperature degradation behavior of 2.5Y-TZP ceramics were investigated. Y2O3-CaO-ZrO2 ceramics were prepared from the commercial Y-TZP powder added within 1 mol% of CaO. Fully tetragonal phase could be obtained at each composition under sintering condition of 1500$^{\circ}C$ for 1 hour. As the amount of CaO increased, grain size was decreased. From the result of heat treatment at 200$^{\circ}C$, volume fraction of monoclinic phase formed on the surface of each specimen was decreased with higher CaO amount. Stability of tetragonal ZrO2 phase for low temperature heat treatment was increased by CaO addition without the degradation of mechanical properties.

• Journal of the Korean Ceramic Society
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• v.35 no.3
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• pp.264-272
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• 1998

The effect of catalytic condition on the properties of SiO2 aerogels has been investigated and then the dri-ed aerogels were partially densified to induce mechanical strength by heat treatment in order to prepare Type-VI silica by Sol-Gel method. Aerogel made by 1-step base process had the highest skeletal density lowest shrinkage and the smallest particle size. But in case of using acid catalyst in both 1st and 2nd step had the lowest skeletal density highest shrinkage and the largest particle size The aerogel synthesized by 1-step base process was most transparent because of its homogeneous microstructure. During heat treatments cracks occurred below 200$^{\circ}C$ for aerogel with the skeletal density lower than 1.9 g/cm3 but the with the higher skeletal density did not cracked up to 800$^{\circ}C$ shrinkage and skeletal density increased as heating temperature increased due to condensation and viscous sintering mechanism.

• Journal of Energy Engineering
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• v.20 no.3
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• pp.252-258
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• 2011

Nickel fiber mat was investigated as a potential structured catalyst for steam reforming of biogas in the temperature range of $600-700^{\circ}C$. The activity of as-received catalyst was very low owing to the smooth surface of fibers. Pretreatment of the catalyst by oxidation followed by reduction under methane partial oxidation condition significantly improved the catalytic activity, although degradation of the activity was found during the reaction due to oxidation and sintering. This deactivation was retarded by supplying additional hydrogen in the inlet gases or by coating $CeO_2$ over the catalyst surfaces.

• Journal of Powder Materials
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• v.5 no.4
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• pp.329-333
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• 1998

Copper-10 wt. % tungsten alloyed powder was obtained by co-reduction of mixed tungsten-trioxide and copper oxide powders at 973 K for 7.2 Ks. In the alloy obtained by pressure-assisted sintering of this co-reduced powder, ultra fine tungsten particles (about 100nm) were dispersed uniformly in the copper matrix. At room temperature, the hardness of this alloy was Hv151 and the electrical conductivity was 85% IACS. After annealing at 1173 K for 3.6 Ks, the hardness and electrical conductivity were Hv147 and 84% IACS, respectively, and were same as before annealing. It was confirmed that the hardness and electrical conductivity of this alloy were hardly influenced by annealing condition since the microstructure of this alloy is highly stabilized.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 1995.11a
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• pp.347-350
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• 1995

In this paper, we fabricated fuel shortage detecting sensor, utilizing NTC thermistor concerned with Mn-Ni-Co system. We would be obtained B constant value of 1930∼2080 and resistivity 387∼430(ohm-cm) additive Bi$_2$O$_3$0∼0.5 wt% to Mn$_3$O$_4$:9wt%, Co$_3$O$_4$:61wt%, NiO:28wt% under 1150∼1250$^{\circ}C$ of sintering temperature. In sensor, we obtained characteristics, which we want, in resistance range 850∼l150$\Omega$, B constant 2000${\pm}$5%. we can see 15 multiplied differences between gasoline and heat dissipation coefficient of air condition.