• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
• /
• 1997.04a
• /
• pp.53-61
• /
• 1997

The effect of sintering condition on tribological behavior in the Cu-base sintered friction materials was studied through pin-on-disk type wear tester. Especially, the experiment was focused on making a comparative study between presstwed sintering and pressureless sintering. Pressureless sintering process showes more stable friction coefficient and lower wear rate than pressure sintering process. This result is related to pore size and density of pore in the sintered materials.

• Journal of the Korean Ceramic Society
• /
• v.28 no.10
• /
• pp.824-830
• /
• 1991

$\alpha$-SiC(B; 0.4 wt, C; 3 wt%) was sintered in Ar atmosphere from 205$0^{\circ}C$ to 220$0^{\circ}C$ by means of pressureless sintering and gas pressure sintering in order to find optimum sintering condition of $\alpha$-SiC. Mechanical properties and microstructures of sintered bodies were investigated according to sintering method. The effect of sintering condition on sinterability of $\alpha$-SiC was also examined by using the dilatometer. 97.5% and 98.8% of theoretical density were obtained from pressureless sintering and gas pressure sintering of $\alpha$-SiC powder, respectively. And modulus of rupture was measured as 270~350 MPa and 420 MPa respectively.

• Journal of the Korean Ceramic Society
• /
• v.29 no.12
• /
• pp.956-962
• /
• 1992

The predominant sintering mechanisms of low firing temperature ceramic substrate which consists of borosilicate glass containing alumina as a filler are the rearrangement of alumina particles and the viscous flow of glass powders. In this system, sintering condition depends on the volume ratio of alumina to glass and on the particle size. When the substrate contains about 35 vol% alumina filler and the average alumina particle size is 4 $\mu\textrm{m}$, the best firing condition is obtained at the temperature range of 900∼1000$^{\circ}C$. The extensive rearrangement behavior occurs at these conditions, and the optimum sintering condition is attained by smaller size of glass particles, too. The formation of cristobalite during sintering causes the difference of thermal expansion coefficient between the substrate and Si chip. This phenomenon degradates the capacity of Si chip. Therefore, the crystallization should be prevented. In the alumina filled borosilicate glass system, the crystallization does not occur. This effect may have some relation with aluminum ions in alumina. For aluminum ions diffuse into glass matrix during sintering, functiong as network former.

• 한국기계연구소 소보
• /
• s.20
• /
• pp.89-104
• /
• 1990

This study was carried out to obtain the most optimum conition in vacuum sintering of M2 HSS powder, by analysis of sintering characteristics and fracture strength in several conditions. The conclusion deduced from this study are as follows; -Boron was more effective element than graphite; at this time, the optimum amount of addition was 0.05 wt% -The optimum condition of sintering temperature and time were 1190- $1200^{\circ}C$ and 1-1.25hr, respectively -Fracture strength of vacuum sintered and heat-treated specimen in the most optimum condition was 2-2.5KN/ $mm^2$

• Journal of the Korean Ceramic Society
• /
• v.27 no.4
• /
• pp.473-480
• /
• 1990

Low-voltage ZnO-based varistors were made by seed grain method at various sintering conditions. Their microstructure and electrical properties were investigated and comlpared with those of the ZnO varistors made by a conventional method at the same sintering condition. During the sintering process, the added seed ZnO grain rapidly grew to be a gaint grain(above 500$\mu\textrm{m}$) provinding easy current path. Therefore the breakdown voltage was lowered as much as the order of 1/10-1/5 in comparison to that of the varistor made by a conventional method. But the grain size of the giant ZnO was little influenced by sintering condition, so the breakdown voltate was also little influenced. The weight loss was decreased by the addition of the seed grain, because the giant grain decreased the evaporation area. Therefore the nonobmic property of the specimen made by seed grain method was little influencedby sintering condition. In this research the low-voltage varistor made by seed grain method showed the least leakage current when sintered at 1150$^{\circ}C$ for zero hour.

• Proceedings of the Korean Powder Metallurgy Institute Conference
• /
• 2006.09a
• /
• pp.621-622
• /
• 2006

In this paper, we show some experimental results of binder-free WC sintered by Pulsed Electric Current Sintering (PECS) also known as Field Assisted Sintering Technology (FAST). These binder-free WC have extremely hardness and stiffness. However, these mechanical properties are dependent on the sintering condition, e.g., maximum temperature, applied pressure, etc. We show some relationship between mechanical properties and sintering condition to improve to sinter the binder-free WC.

• Journal of the Korean Ceramic Society
• /
• v.23 no.1
• /
• pp.1-6
• /
• 1986

The shrinkage rate of solid state sintering has been theoretically derived by combining the rate equation of material transport and the net free energy change resulting from the decrease of solid-vapor interface and the increase of grain boundary during sintering. For a sinteing model an idealized situation of the spherical particles with BCC packing was taken as the initial condition and the shrinkage was assumed to occur by forming the flat circualr grain boundaries on each particle. The plotted shrinkage rates as a function of grain boundary to surface energy ratio $(gamma_g/gamma_s)$ have shown that the relative density increases linearly at the initial stage of sintering but the shrinkage rate is decreased upon further sintering due to a decrease in driving force for densificaton. It has been also shown that the densification is critically affected by the $gamma_g/gamma_s$ ratio. In order to get the complete densificatin the ratio should be less than $sqrt{3}$. Any additive or atmospheric condition causing the decrease of$_g/gamma_s$ ratio will enhance sintering.

• Journal of the Korean Ceramic Society
• /
• v.34 no.6
• /
• pp.601-610
• /
• 1997

In cofiring of multilayered alumina with tungsten, the change of camber with lamination condition was experimented and the effect of sintering shrinkage of alumina and tungsten was investigated. From the exact measurement of sintering shrinkage of tungsten thick film, as lamination pressure increased, the sintering shrinkage of alumina decreased but that of tungsten thick film was not changed. So it was though that the main factor which induced the sintering shrinkage difference between ceramics and metal with lamination condition was the change of sintering shrinkage of ceramics. In case of high lamination pressure, high green sheet density, the cofired specimen showed low camber due to low shrinkage difference between alumina and tungsten and there was a linear relation between camber and shrinkage difference. It was found that this shrinkage difference could change the thickness of tungsten film and the microstructure within via hole during cofiring.

• Proceedings of the Korea Committee for Ocean Resources and Engineering Conference
• /
• 2006.11a
• /
• pp.162-165
• /
• 2006

In this study, Liquid Phase Sintered SiC (LPS-SiC) was fabricated by hot pressing method with $\beta$-SiC powder whose a particle size is 30nm and less on the average in argon condition at 1780 and $1800^{\circ}C$ under 20MPa. Alumina ($Al_2O_3$), yttria ($Y_2O_3$) and silica ($SiO_2$) were used for sintering additives. To investigate effects of particle-size and temperature on $SiO_2$, LPS-SiC was fixed $Al_2O_3$, $Y_2O_3$ and then particle-size of $SiO_2$ were changed as two kinds. The system of particle-size and temperature on sintering additives which affects a property of sintering os well os the influence depending on particle-size and temperature of sintering additives were investigated by measurement of sintering properties. Such as measurement of sintering density, vikers hardness and observing of microstructure were investigated to make sure of the optimum condition which is about matrix of $SiC_f/SiC$ composites. Base on the composition of sintering additives, microstructure and sintering property correlation, the effect of particle-size of sintering additives are discussed. An experimental method to investigate the dynamic characteristics of bums in extreme environmental condition is established.

• Journal of Industrial Technology
• /
• v.27 no.B
• /
• pp.137-144
• /
• 2007

Sintering condition and various chemical composition of bond materials for micro-blades were studied. The methods mixing of pure powders and using pre-alloyed powders for compaction and sintering were compared and optimized in terms of the evaluation of bending strength and fractographic study. The effect of the amount of graphite as a lubricant and diamond abrasive on the strength of sintered bond materials and fracture toughness was investigated. The strength decreased with increasing the amount of graphite and diamond abrasive.