• Title/Summary/Keyword: Sintered density

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Effect of Er2O3 Content on Nonlinear Properties and Impulse Clamping Characteristics of Pr/Co/Cr/Al Co-doped Zinc Oxide Ceramics

  • Nahm, Choon-Woo
    • Journal of the Korean Ceramic Society
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    • v.51 no.6
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    • pp.612-617
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    • 2014
  • The microstructure, nonlinear properties, and impulse clamping characteristics of Pr/Co/Cr/Al co-doped zinc oxide ceramics were investigated with various contents of $Er_2O_3$. Increasing $Er_2O_3$ content increased the density of the sintered pellets from 5.69 to $5.83g/cm^3$, and decreased the average grain size from 10.6 to $6.5{\mu}m$. With increased $Er_2O_3$ content, the breakdown field increased from 2318 to 4205 V/cm, and the nonlinear coefficient increased from 19.4 to 40.2. The clamp characteristics were improved with the increase of the content of $Er_2O_3$. The varistors doped with 2.0 mol% exhibited the best clamp characteristics, in which the clamp voltage ratio was 1.40-1.73 at 1-50 A in an impulse current.

Microwave dielectric properties of the BSST ceramics with BaO compositional ratio (BSST계 세라믹스의 BaO 조성비에 따른 마이크로파 유전특성)

  • 박인길;정장호;이성갑;이영희
    • The Transactions of the Korean Institute of Electrical Engineers
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    • v.45 no.1
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    • pp.81-85
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    • 1996
  • Microwave dielectric properties of 0.15(B $a_{x}$S $r_{0.05}$)O-0.15(S $m_{2}$(1-y)N $d_{2y}$) $O_{3}$-0.7Ti $o_{2}$(x=o.9~0.1[mol.], y=6[m/o]) ceramics were investigated with BaO compositional ratio. Sintered density and resistivity of specimens were independent on the BaO compositional ratio. In the specimen with x=0.975[mol.], dielectric constant, quality factor and temperature coefficient of resonant frequency had good values of 76.52, 3001(at 3[GHz]) and +0.71[ppm/.ceg. C], respectively. By comparing with the stoichiometric compositions of 78.14, 2938(at 3[GHz])+14.19[ppm/.ceg. C], dielectric constant and quality factor showed similar properties, but the temperature coefficient of resonant frequency was highly improved. (author). refs., figs., tabs.s.s.

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Effect of CuO on the Microstructural and Electrical Properties of (Pb)(La,Nd)$TiO_3$ Ceramics (CuO가 (Pb)(La,Nd)$TiO_3$ 세라믹스에 첨가시 미세구조와 전기적 특성에 미치는 영향)

  • 민석규;류주현;박창엽;윤현상
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.11a
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    • pp.446-450
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    • 2001
  • In this study, microstructural and electrical properties of (Pb)(La,Nd)TiO$_3$ ceramics were investigated as a function of CuO addition. Taking into consideration Tc of 3$25^{\circ}C$, dynamic range of 49dB( at the wafer form) and density of 7.71g/㎤, it can be concluded that the specimen S2 sintered at 120$0^{\circ}C$ is the best for the resonator application. Dynamic characteristics of energy-trapped 20MHz SMD type resonator as a function of internal dot size variation were also investigated. Dynamic range characteristics showed the highest value of 60.72dB at S2-4(dot size 1.13mm).

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Electrical Properties of (Pb, LaITiO$_3$ Thin Films fabricated by Sol-Gel Processing (Sol-Gel 법에 의한 (Pb, La)TiO$_3$ 박막의 전기적 특성)

  • 구본혁;박정흠;장낙원;마석범;박창엽
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1997.11a
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    • pp.48-51
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    • 1997
  • (Pb. La)TiO$_3$ thin films were fabricated by sol-gel Processing and spin-coated on the Pt substrate. The spin-coated PLT films were sintered at 75$0^{\circ}C$ for 5min by rapid thermal ann La content dependence of the electrical properties of the PLT thin films are discussed. Wit La mole% from 20 to 36mo1e%. the dielectric constant of the PLT thin films decreased f 570. P-E hysteresis loops changed from ferroelectric to paraelectric. and the charge storage charging time decreased. The Curie Point decreased with increasing La content. The leak density also decreased and La 36mo1% species shows mood characteristics less than 10- electric field 500 (KV/cm) Because of the broad range of composition-controlled ferroelectric PLT thin films are suitable for memory application.

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Nozzles from Alumina Ceramics with Submicron Structure Fabricated by Radial Pulsed Compaction

  • Kaygorodov, Anton;Rhee, Chang;Kim, Whung-Whoe;Ivanov, Viktor;Paranin, Sergey;Spirin, Alexey;Khrustov, Vladimir
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.368-369
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    • 2006
  • By means of magnetic pulsed compaction and sintering of weakly aggregated alumina based nanopowders the jet forming nozzle samples for the hydroabrasive cutting were fabricated. The ceramics was obtained from pure alumina, as well as from alumina, doped by $TiO_2$, MgO and AlMg. It was shown that the samples sintered from AlMg doped $Al_2O_3$ powder have the best mechanical properties and structural characteristics: relative density ${\sim}0.97$, channel microhardness. - 18-20 GPa, channel surface roughness ${\sim}0.7\;{\mu}m$, average crystallite size ${\sim}1\;{\mu}m$.

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Microstructure and Mechanical Properties of Nanostructured Aluminum Consolidated by SPS

  • Zadra, Mario;Casari, Francesco;Molinari, Alberto
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.360-361
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    • 2006
  • Nanostructured aluminum powders were obtained by means of planetary ball milling with methanol as the Process Control Agent (PCA). The behavior, during milling, was considered measuring the microhardness and grain size at different milling times. Bulk near-full density samples were sintered using the Spark Plasma Sintering technology with different schedules: temperature of $500^{\circ}C$ and $550^{\circ}C$, pressure of 30 MPa and 60 MPa and different modes of applying the pressure were changed in order to understand the behavior during sintering. All the samples retained their nanostructure with an increase of the grain size from about 46 up to 70-90 nm.

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Unified Molding and Simulation for Nano-structured Tungsten Carbide

  • Park, Seong-Jin;Johnson, John L.;German, Randall M.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.362-363
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    • 2006
  • Nano-structured tungsten carbide compacts with cobalt matrices (WC-Co) offer new opportunities for achieving superior hardness and toughness combinations. A unified modeling and simulation tool has been developed to produce maps of sintering pathways from nanocrystalline WC powder to sintered nano-structured WC-Co compacts. This tool includes (1) die compaction, (2) grain growth, (3) densification, (4) sensitivity analysis, and (5) optimization. All material parameters were obtained by curve fitting based on results with two WC-Co powders. Critical processing parameters are determined based on sensitivity analysis and are optimized to minimize grain size with high density.

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Fabrication of Textured $Al_2O_3-Mullite-SiC$ Nano-composite by Slip Casting in a High Magnetic Field and Reaction Sintering

  • Sakka, Yoshio;Saito, Sho;Honda, Atsushi;Suzuki, Tohru S.;Moriyoshi, Yusuke
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.327-328
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    • 2006
  • We have demonstrated that textured $Al_2O_3-mullite-SiC$ nanocomposites can be fabricated by slip casting followed by partial oxidation - reaction sintering of mixed suspensions of $Al_2O_3$ and SiC powders in a high magnetic field. The sintered density was changed by the degree of oxidation at 1200C and 1300C. The degree of orientation of alumina in the nanocomposite was examined on the basis of the X-ray diffraction patterns and scanning electron micrographs. It is confirmed that alumina-oriented nanocomposites were fabricated. The three-point bending strength at room temperature was observed for the nanocomposites.

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Three-dimensional Printing of Shape Memory Alloys

  • Carreno-Morelli, E.;Martinerie, S.;Bidaux, J.E.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.256-257
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    • 2006
  • 3D printing of NiTi alloys has been successfully achieved. A novel printing process has been developed and used, which consists in selective deposition of a solvent on a granule bed. The granules are composed of metal powders and thermoplastic binder, which are mixed and sieved by conventional methods. A sound green strength is obtained after solvent evaporation. Sintered parts exhibit good density, proper phase composition and shape memory behaviour.

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Densification Behavior of Fe-Ni Alloy Nanoparticles

  • Kim, Sang-Phil;Lee, Woo-Seok;Lee, Jae-Wook;Choi, Chul-Jin
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.531-532
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    • 2006
  • The effects of compaction pressure and sintering temperature on the densification of Fe-40wt%Ni alloy nanoparticles were analyzed. The Fe-Ni nanoparticles were fabricated by an arc-discharge method and then, compacted at three different pressures and sintered at 550 to $900\;^{\circ}C$. Densification was completed at temperature as low as $600\;^{\circ}C$ and high-pressure compaction was found to enhance densification. Densification behaviors and microstructure developments have been investigated through density measurements, electron microscopies, and hardness measurements.

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