• 센서학회지
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• 제5권3호
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• pp.101-108
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• 1996

Au 또는 Pt를 확산시켜 실리콘 $p^{+}-n$ 접합 다이오드를 제작하였다. Au 또는 Pt의 확산을 $800{\sim}1010^{\circ}C$, 산소 및 질소분위기에서 실시하여 다이오드의 전기적 특성을 분석하였으며, Au 또는 Pt가 확산된 시편을 산소분위기의 $800{\sim}1010^{\circ}C$에서 2차 열처리를 실시한후 이 처리가 소자의 전기적 특성에 미치는 효과에 대해 고찰하였다. $1010^{\circ}C$의 온도에서 1차 확산결과 Pt가 확산된 다이오드의 누설전류는 Au가 확산된 다이오드 누설전류의 75배 였다. $1010^{\circ}C$, 질소분위기에서 1시간동안 Pt가 확산된 시편을 산소분위기에서 $800^{\circ}C$, 1시간동안 2차 열처리하였을 경우에 1차 열처리한 것보다 누설전류가 1/1100로 감소되었다. 초고속 실리콘 $p^{+}-n$ 접합 스위칭 다이오드의 특성을 만족하기 위해서는, Pt를 $1010^{\circ}C$, 질소분위기에선 1시간 확산시킨후 2차 열처리를 $800^{\circ}C$, 산소분위기에서 1시간동안 열처리하는 것이 최적 조건임을 알 수 있었다. 이때 다이오드의 제특성은 역회복시간 4ns, 항복전압 138V, 누설전류1.7nA 그리고 순방향 전압이 1V였다.

• 한국세라믹학회지
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• 제41권6호
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• pp.456-463
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• 2004

음극지지형 SOFC의 성능을 향상시키기 위해 단전지 제조공정을 개선하고 그 출력특성을 평가하였다. 액상응결 공정(Liquid Condensation Process : LCP)과 일축가압성형공정을 통하여 NiO/YSZ 복합체 음극기판을 제조하고 위에 YSZ 전해질을 스크린 인쇄한 후 140$0^{\circ}C$에서 3시간동안 동시소결하여 음극/전해질 기판을 제조하였다. 또한 LSM/YSZ 양극층은 임피던스 분석을 통해 분극저항이 최소가 되는 조성 및 열처리 조건을 선택하여 스크린 인쇄법을 이용해 구성하였고 이러한 적층공정을 거쳐 최종적으로 5${\times}$5와 l0${\times}$10 $\textrm{cm}^2$ 크기의 단전지를 제조하였다. 제조된 단전지의 출력특성을 측정한 결과 5${\times}$5와 10${\times}$10 단전지는 80$0^{\circ}C$에서 약 0.45W/$\textrm{cm}^2$ 와 0.22 W/$\textrm{cm}^2$의 최대출력밀도를 각각 나타내어 선행연구에서 기존공정으로 제조된 단전지에 비해 2배 이상 향상된 좋은 성능을 나타내었다.

• 한국농촌건축학회논문집
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• 제4권1호
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• pp.37-44
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• 2002

There are some studies about user's participation to reflect their desire and value on the planning of house by this time. These were constitution of unit space focused on the apartments, which is mostly theoretical. However, till completion of a construction work, it goes through various processes of some steps such as, buying building site, site planning, architectural planning and construction. In architectural planning process, it takes time for continuous discussion and revision between architects and users. Also changes of plan must of necessity be so because of in or outside conditions. So, right user's participation has its meaning that they take part in each step and portion of process faithfully on whole architectural processes. In this case, tenants of single house were decided and they already buy building site and lay out rules jointly. With this circumstance I've researched a kind of test the reflection on various desires and its acceptance in each steps through completion of a construction work, which is based on their participation.

• 한국정밀공학회지
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• 제33권3호
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• pp.199-205
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• 2016

A thin sheet of metal with corrugated structures has been utilized in various devices: heat exchangers, separators in fuel cells, and many others. However, it is not easy to fabricate thin corrugated structures using a single-step stamping process due to their geometrical complexity. To solve this problem, firstly, a plate type heat exchanger was redesigned to attain the optimal value of aspect ratio and the optimal shape of corrugated structures for the actual loading conditions. A forming analysis of the corrugated plate was then carried out to determine the process parameters. From this work, the optimal value of aspect ratio was found to be 4.6. In addition, the process parameters of heat exchanger forming were optimized using the optimal value of aspect ratio, and the analytical results were evaluated through experiments. The results obtained indicated good agreements between them.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 2001년도 춘계학술대회 논문집
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• pp.15-19
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• 2001

A dedicated reverse engineering(RE) system for rapid manufacturing of human head in a 3D bust has been developed. The first step in the process is to capture the surface details of a human head and shoulder by three scanners based upon the digital moire fringe technique. Then the multiple scans captured from different angles are aligned and merged into a single polygonal mesh, and the aligned data set is refined by smoothing, subdividing or hole filling process. Finally, the refined data set is sent to a 4-axis computer numerically control(NC) machine to manufacture a replica. In this paper, we mainly describe on the algorithms and software for aligning multiple data sets. The method is based on the recently popular Iterative Closest Point(ICP) algorithm that aligns different polygonal meshes into one common coordinate system. The ICP algorithm finds the nearest positions on one scan to a collection of points on the other scan by minimizing the collective distance between different scans. We also integrate some heuristics into the ICP to enhance the aligning process. A typical example is presented to validate the system and further research work is also discussed.

• 대한지구과학교육학회지
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• 제5권1호
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• pp.8-19
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• 2012

The purpose of this study is to: analyze the characteristics on ill-structured problem-solving process; examine the type of memories used in their monitoring. The data were primary collected from observation and secondary the semi-structured in-depth interviews based on analysis of observation results with two students who belong to science school and a guidance. The findings of this study revealed that the ill-structured problems possess multiple representations and the upper level's problem have several sub-problems. And multiple steps simultaneously exist in particular stage of problem-solving process that is not single sequential but complex flow and have high frequency of discussion step. Type of memories used in ill-structured problems include idiosyncratic memories which is related in personal histories such as school performance, problem-related memories, abstract rules and intuition.

• Journal of Information Science Theory and Practice
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• 제9권4호
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• pp.35-49
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• 2021

In a situation where there are multiple diverse datasets, it is essential to have an efficient method to provide users with the datasets they require. To address this suggestion, necessary datasets should be selected on the basis of the relationships between the datasets. In particular, in order to discover the necessary datasets for disaster resolution, we need to consider the disaster resolution stage. In this paper, in order to provide the necessary datasets for each stage of disaster resolution, we constructed a disaster type and disaster management process ontology and designed a method to determine the necessary datasets for each disaster type and disaster management process step. In addition, we introduce a method to determine relationships between datasets necessary for disaster response. We propose a method for discovering datasets based on minimal relationships such as "isA," "sameAs," and "subclassOf." To discover suitable datasets, we designed a knowledge exploration model and collected 651 disaster-related datasets for improving our method. These datasets were categorized by disaster type from the perspective of disaster management. Categorizing actual datasets into disaster types and disaster management types allows a single dataset to be classified as multiple types in both categories. We built a knowledge exploration model on the basis of disaster examples to ensure the configuration of our model.

• Restorative Dentistry and Endodontics
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• 제35권5호
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• pp.321-334
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• 2010

연구목적: 본 연구는 상아질 접착제의 잔류 용매가 접착 효율에 미치는 영향을 평가하고자 하였다. 연구 재료 및 방법: 본 연구에서는 5세대 2단계 산부식형 접착제와 7세대 단일과정 자가부식형 접착제를 사용하였다. 상아질 접착제의 증발률과 전환률, 적용 후 용매의 공기건조 방법에 따른 미세인장결합강도를 측정하였으며 접착 계면을 FE-SEM을 이용하여 관찰하였다. 결과: 1. 시간에 따라 접착제의 증발률은 증가하나 접착제의 종류에 따라 증가 양상이 서로 달랐다. 2. 대부분 전환률은 증발률에 비례하는 경향을 나타내었다. 3. 공기건조 방법에 따라 결합강도는 대부분 under군, control군, over군 순으로 증가하는 양상을 나타내었다. 4. FE-SEM에서 아세톤을 용매로 사용하는 접착제는 공기건조 방법에 따라 droplet이나 gap이 관찰되었다. 결론: 상아질 접착제의 잔류 용매는 접착 효율에 부정적인 영향을 미치기 때문에, 상아질 접착제의 선택과 사용 시 용매의 종류와 특징에 대한 적절한 이해가 필요할 것이다.

• 한국독성학회:학술대회논문집
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• 한국독성학회 2006년도 추계학술대회
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• pp.65-74
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• 2006

Modem drug discovery requires rapid pharmacokinetic evaluation of chemically diverse compounds for early candidate selection. This demands the development of analytical methods that offer high-throughput of samples. Naturally, liquid chromatography / tandem mass spectrometry (LC-MS/MS) is choice of the analytical method because of its superior sensitivity and selectivity. As a result of the short analysis time(typically 3-5min) by LC-MS/MS, sample preparation has become the rate- determining step in the whole analytical cycle. Consequently tremendous efforts are being made to speed up and automate this step. In a typical automated 96-well SPE(solid-phase extraction) procedure, plasma samples are transferred to the 96-well SPE plate, internal standard and aqueous buffer solutions are added and then vacuum is applied using the robotic liquid handling system. It takes only 20-90 min to process 96 samples by automated SPE and the analyst is physically occupied for only approximately 10 min. Recently, the ultra-high flow rate liquid chromatography (turbulent-flow chromatography)has sparked a huge interest for rapid and direct quantitation of drugs in plasma. There is no sample preparation except for sample aliquotting, internal standard addition and centrifugation. This type of analysis is achieved by using a small diameter column with a large particle size(30-5O ${\mu}$m) and a high flow rate, typically between 3-5 ml/min. Silica-based monolithic HPLC columns contain a novel chromatographic support in which the traditional particulate packing has been replaced with a single, continuous network (monolith) of pcrous silica. The main advantage of such a network is decreased backpressure due to macropores (2 ${\mu}$m) throughout the network. This allows high flow rates, and hence fast analyses that are unattainable with traditional particulate columns. The reduction of particle diameter in HPLC results in increased column efficiency. use of small particles (<2 urn), however, requires p.essu.es beyond the traditional 6,000 psi of conventional pumping devices. Instrumental development in recent years has resulted in pumping devices capable of handling the requirements of columns packed with small particles. The staggered parallel HPLC system consists of four fully independent binary HPLC pumps, a modified auto sampler, and a series of switching and selector valves all controlled by a single computer program. The system improves sample throughput without sacrificing chromatographic separation or data quality. Sample throughput can be increased nearly four-fold without requiring significant changes in current analytical procedures. The process of Bioanalytical Method Validation is required by the FDA to assess and verify the performance of a chronlatographic method prior to its application in sample analysis. The validation should address the selectivity, linearity, accuracy, precision and stability of the method. This presentation will provide all overview of the work required to accomplish a full validation and show how a chromatographic method is suitable for toxirokinetic sample analysis. A liquid chromatography/tandem mass spectrometry (LC-MS/MS) method developed to quantitate drug levels in dog plasma will be used as an example of tile process.

• 전기화학회지
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• 제10권3호
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• pp.159-168
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• 2007

An electrochemical study related to the redox characteristics of Ethyl-3-acetyl-6-methyl-1, 4-diphenyl-4, 3a-dihydro-1, 3, 4-triazolino[3, 4-a] pyrimidine-5-carboxylate ester and its derivatives (1a-f) and (2a-e) in nonaqueous solvents such as 1, 2-dichloroethane (DCE), dichloromethane (DCM), acetonitrile (AN), dimethylsulphoxide (DMSO) and tetrahydrofurane (THF) using $0.1\;mol\;dm^{-3}$ tetrabutylammonium perchlorate (TBAP) as a supporting electrolyte at platinum, glassy carbon and gold electrodes, has been performed using cyclic voltammetry (CV). Controlled potential electrolysis (CPE) is also carried out to elucidate the course of different electrochemical reactions through the separation and identification of the intermediates and final electrolysis products. The redox mechanism is suggested and proved. It was found that all the investigated compounds in all solvents are oxidized in a single irreversible one electron donating process following the well known pattern of the EC-mechanism to give a dimer. On the other hand, these compounds are reduced in a single irreversible one electron step to form the anion radical, which is basic enough to proton from the media forming the radical which undergoes tautomerization and then dimerization processes to give also another bis-compound through N-N linkage formation.