• 산업기술연구
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• 제26권B호
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• pp.173-181
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• 2006

We analyzed systematically particle growth in the pulsed $SiH_4$ plasmas by a numerical method and investigated the effects of pulse modulations (pulse frequencies, duty ratios) on the particle growth. We considered effects of particle charging on the particle growth by coagulation during plasma-on. During plasma-on ($t_{on}$), the particle size distribution in plasma reactor becomes bimodal (small sized and large sized particles groups). During plasma-off ($t_{off}$), there is a single mode of large sized particles which is widely dispersed in the particle size distribution. During plasma on, the large sized particles grows more quickly by fast coagulation between small and large sized particles than during plasma-off. As the pulse frequency decreases, or as the duty ratio increases, $t_{on}$ increases and the large sized particles grow faster. On the basis of these results, the pulsed plasma process can be a good method to suppress efficiently the generation and growth of particles in $SiH_4$ PCVD process. This systematical analysis can be applied to design a pulsed plasma process for the preparation of high quality thin films.

• 한국입자에어로졸학회지
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• 제7권4호
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• pp.123-130
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• 2011

Previous designs of conventional aerodynamic lenses have a limitation of narrow range of focusable particle size, e.g. 30 to 300nm or 3 to 30nm. To enlarge the focusable size range to 30-3000nm, it is necessary to avoid a significant loss of particles larger than 300nm inside the lenses. From numerical simulations on size-resolved particle trajectories, we confirmed that the traveling losses of such large particles could be avoided only when the radial position of particles approaching the orifice lens was near the lens axis. Hence, we designed the lens system consisting of a converging-diverging nozzle and 7 orifices to fulfill the requirement. In particular, the orifices were aligned in a way that their diameters were descending and ascending to the downstream. As a result, 30-2800nm particles can be focused to the particle beam of 0.2mm or less in radius with above 85% transmission efficiency. Even $10{\mu}m$ particles can be focused with 74% of transmission efficiency.

• 대한기계학회논문집
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• 제16권11호
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• pp.2159-2168
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• 1992

본 연구에서는 CWS 액적의 가열 및 연소에 관한 현상규명에 있어서 액적크기, CWS 석탄함량 및 연소분위기 가스온도, CWS 액적중의 미분된 석탄입자의 크기와 특히 분위기중의 산소농도의 변화에 의한 영향을 파악하고자 한다.

• 한국자동차공학회논문집
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• 제17권4호
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• pp.55-62
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• 2009

As an experiment investigation, the effects of ethanol blended gasoline fuel with different injection method on nano-sized particle emission characteristics were examined in a 0.5L spark-ignited single-cylinder engine with a compression ratio of 10. Because this engine nano-particles are currently attracting interest due to its adverse health effects and their impact on the environments. So a pure gasoline and an ethanol blended gasoline fuels, namely E85 fuel, used for this study. And, as a particle measuring instrument, a fast-response particle spectrometer (DMS 500) with heated sample line was used for continuous measurement of the particle size and number distribution in the size range of 5 to 1000nm (aerodynamic diameter). As this research results, we found that the effect of ethanol blending gasoline caused drastic decrease of nano-particle emissions when port fuel injection was used for making better air-fuel mixture than direct fuel injection. Also injection timing, specially direct fuel injection, could be a dominant factor in controlling the exhaust particle emissions.

• 한국분말재료학회지
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• 제31권2호
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• pp.132-136
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• 2024

This study investigated the effects of revolution speed and ball size in planetary milling on the microstructure and dehydrogenation behavior of TiH₂ powder. The particle size analysis showed that the large particles present in the raw powder were effectively refined as the revolution speed increased, and when milled at 500 rpm, the median particle size was 1.47 ㎛. Milling with a mixture of balls of two or three sizes was more effective in refining the raw powder than milling with balls of a single size. A mixture of 3 mm and 5 mm diameter balls was the optimal condition for particle refinement, and the measured median particle size was 0.71 ㎛. The dependence of particle size on revolution speed and ball size was explained by changes in input energy and the number of contact points of the balls. In the milled powder, the endothermic peak measured using differential thermal analysis was observed at a relatively low temperature. This finding was interpreted as the activation of a dehydrogenation reaction, mainly due to the increase in the specific surface area and the concentration of lattice defects.

• 한국인쇄학회지
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• 제20권1호
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• pp.65-78
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• 2002

The suspension polymerization of styrene was carried out to obtain the narrow-size distribution of particle by using poly(vinyl alcohol) (PVA) as suspension stabilizer according to the degree of hydrolysis and the molecular weight. The stabilizing properties of suspension are also dependent on the interfacial tension of aqueous solution when PVA is added. When the polymerization process was carried out with low hydrolyzed PVA, it gave single, well-defined particles, while high hydrolyzed PVA gave clusters. The size of particle produced in this study ranged between 5${\mu}{\textrm}{m}$ and 10${\mu}{\textrm}{m}$. The suspending agent, PVA, influences on the drop size and drop stability, When the molecular weight of PVA is increased, the drop size decreases and the drops become more stable toward coalescence. An increase in the PVA concentration decreases the mean drop size and narrows the drop size distribution.

• 한국분무공학회지
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• 제6권1호
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• pp.35-43
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• 2001

Previous studies on image processing techniques for panicle size measurement usually have focused on a single panicle or weakly overlapped particles. In the present work, the image processing algorithm for particle size measurement has been improved to process heavily-overlapped spherical-particle images. The algorithm consists of two steps; detection of boundaries which separate the images of the overlapped panicles from the background and the panicle identification process. For the first step, Sobel operator (using gray-level gradient) and the thinning process was adopted, and compared with the gray-level thresholding method that has been widely adopted. In the second, Hough transform was used. Hough transform is the detection algorithm of parametric curves such as straight lines or circles which can be described by several parameters. To reduce the measurement error, the process of finding the true center was added. The improved algorithm was tested by processing an image frame which contains heavily overlapped spherical panicles. The results showed that both the performances of detecting the overlapped images and separating the panicle from them were improved.

• 한국의류학회지
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• 제28권6호
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• pp.854-861
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• 2004

To estimate dispersion stability of particles in anionic and nonionic surfactant mixed solution, suspending power was examined as functions of duration time of suspension, ionic and nonionic surfactant mixed ratio, surfactant concentration, kinds of electrolyte, ionic strength and mole numbers of oxyethylene additions to nonionic surfactant using $\alpha$-Fe$_2$O$_3$ particle as the model of particulate soil. The suspending power of anionic and nonionic surfactant mixed solution was relatively higher than that of anionic and nonionic surfactant single solution regardless of solution concentration. The suspending power was gradually decreased with increasing duration time of suspension. In the absence of electrolyte, the effect of surfactant concentration on suspending power was small but in solution with electrolyte, suspending power was lowest at 1 ％ surfactant concentration. With 1${\times}$10$^{-3}$ ionic strength and polyanionic electrolyte in solution, the suspending power was high but effects of oxyethylene mole number to nonionic surfactant on suspending power was small. Generally the suspending power was gradually increased with decreasing the particle size. Hence the suspending power was inversely related to the particle size.

• 한국재료학회지
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• 제23권10호
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• pp.543-549
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• 2013

The purpose of this paper was to investigate the effect of a high-energy milling (HEM) process on the particle morphology and the correlation between a thermal treatment and tetragonal/monoclinic nanostructured zirconia powders obtained by a precipitation process. To eliminate chloride residue ions from hydrous zirconia, a modified washing method was used. It was found that the used washing method was effective in removing the chloride from the precipitated gel. In order to investigate the effect of a pre-milling process on the particle morphology of the precipitate, dried $Zr(OH)_4$ was milled using a HEM machine with distilled water. The particle size of the $Zr(OH)_4$ powder exposed to HEM reduced to 100~150 nm, whereas that of fresh $Zr(OH)_4$ powder without a pre-milling process had a large and irregular size of 100 nm~1.5 ${\mu}m$. Additionally, modified heat treatment process was proposed to achieve nano-sized zirconia having a pure monoclinic phase. It was evident that two-step calcining process was effective in perfectly eliminating the tetragonal phase, having a small average particle of ~100 nm with good uniformity compared to the sample calcined by a single-step process, showing a large average particle size of ~300 nm with an irregular particle shape and a broad particle size distribution. The modified method is considered to be a promising process for nano-sized zirconia having a fully monoclinic phase.

• 한국전산유체공학회지
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• 제18권2호
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• pp.93-98
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• 2013

In this paper, we reported the verification of numerical simulation approach for sedimentation of the multi-size particles in a container. The comparison between experimentally measured values and numerically evaluated values on settle down process of fully mixed mixture is carried out. In an attempt to represent the natural particle size distribution, various diameters of single particles are simulated and the results are compared with the outcome of the multi-size computation. When the empirical formula for mean particle size estimation is adopted to define the sediment diameter, computation and comparison are conducted.