• Title/Summary/Keyword: Simultaneous Pulsed Wire Evaporation

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A Study on the Nano Alloy Powders Synthesized by Simultaneous Pulsed Wire Evaporation (S-PWE) Method, Part I - Background (동시 전기 폭발법에 의한 나노 합금 분말 제조에 관한 연구 Part I - 동시 전기 폭발을 위한 이론적 배경)

  • ;;;O. M. Samatov;Yu. A. Kotov
    • Journal of Powder Materials
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    • v.11 no.1
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    • pp.60-68
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    • 2004
  • Pulsed wire evaporation (PWE) method is known as the promising production-technique for nanopowders. In this study, we developed and modified the previous single wire explosion equipment to the simultaneous two-wire explosion one for the fabrication of alloy or mixture of nano metallic powder. First of all, both the theoretical and empirical background of pulsed wire explosion of single wire were summarized, and compared with our experimental results for Cu and Al single wlre explosion. After then, the simultaneous wire evaporation equipment was designed, constructed, and tested. The current and voltage behavior were well matched between the calculated ones from the circuit equations, and the experimental results from simultaneous explosion of Cu and Al wire.

A Study on the Nano Alloy Powders Synthesized by Simultaneous Pulsed Wire Evaporation (S-PWE) method II - Synthesis of Ee-Al Nano Alloy Powders (동시 전기 폭발법에 의한 나노 합금 분말 제조에 관한 연구 II - Fe-Al alloy 분말 제조)

  • ;;;O. M.;Yu. A. Kotov
    • Journal of Powder Materials
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    • v.11 no.2
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    • pp.105-110
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    • 2004
  • In this study the possibility to obtain a homogeneous mixture and to produce solid solutions and intermetallic compounds of Fe and Al nano particles by simultaneous pulsed wire evaporation (S-PWE) have been investigated. The Fe and Al wires with 0.45 mm in diameter and 35 mm in length were continuously co-fed by a special mechanism to the explosion chamber and simultaneously exploded. The characteristics, e.g., phase composition, particle shape, and specific surface area of Fe-Al nano powders have been analyzed. The synthesized powders, beside for Al and $\alpha$-Fe, contain significant amount of a high-temperature phase of $\gamma$-Fe, Fe Al and traces of other intermetallics. The phase composition of powders could be changed over broad limits by varying initial explosion conditions, e.g. wire distance, input energy, for parallel wires of different metals. The yield of the nano powder is as large as 40 wt % and the powder may include up to 46 wt % FeAl as an intermetallic compound.