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A Study on the Nano Alloy Powders Synthesized by Simultaneous Pulsed Wire Evaporation (S-PWE) method II - Synthesis of Ee-Al Nano Alloy Powders

동시 전기 폭발법에 의한 나노 합금 분말 제조에 관한 연구 II - Fe-Al alloy 분말 제조

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  • O. M. ;
  • Yu. A. Kotov ;
  • 이근희 (한국원자력연구소 원자력재료기술개발부) ;
  • 이창규 (한국원자력연구소 원자력재료기술개발) ;
  • 김흥회 (한국원자력연구소 원자력재료기술개발) ;
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  • 권영순 (울산대학교 기계부품 및 소재 특성평가연구센터, 첨단소재공학부)
  • Published : 2004.04.01

Abstract

In this study the possibility to obtain a homogeneous mixture and to produce solid solutions and intermetallic compounds of Fe and Al nano particles by simultaneous pulsed wire evaporation (S-PWE) have been investigated. The Fe and Al wires with 0.45 mm in diameter and 35 mm in length were continuously co-fed by a special mechanism to the explosion chamber and simultaneously exploded. The characteristics, e.g., phase composition, particle shape, and specific surface area of Fe-Al nano powders have been analyzed. The synthesized powders, beside for Al and $\alpha$-Fe, contain significant amount of a high-temperature phase of $\gamma$-Fe, Fe Al and traces of other intermetallics. The phase composition of powders could be changed over broad limits by varying initial explosion conditions, e.g. wire distance, input energy, for parallel wires of different metals. The yield of the nano powder is as large as 40 wt % and the powder may include up to 46 wt % FeAl as an intermetallic compound.

Keywords

References

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