• Title/Summary/Keyword: Silk-I

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Studies on Silk Fibroin Membranes(II) -Adsorption of Acid Dyes in Silk Fibroin Memberane- (Silk Fibroin 막에 관한 연구 (II) -Silk Fibroin 막에 대한 산성염료의 흡착-)

  • 최해욱;박수민;김경환
    • Textile Coloration and Finishing
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    • v.6 no.3
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    • pp.60-66
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    • 1994
  • With the view of studying on the dual adsorption mechanism of acid dyes in connection with the structural difference of silk fibroin, silk fiber and silk fibroin memberane were used for equilibrium dyeing at $60^{\circ}C$, $70^{\circ}C$, $80^{\circ}C$ and pH 3.2, pH 5.0. The dyes used were C.I.Acid Orange 7 and C.I.Acid Red 88 introduced aromatic hydrocabon into Acid Orange 7. From the adsorption isotherm experiment, the total uptake of dyes can be described by Langmuir sorption and Nernst partition. Nernst partition. Nernst partition coefficient $K_1$ decrease of crystalline regions and orientation. The saturation value S of Acid Red 88 were large than total amino group contents and it was attributed it hydrophobic bond. On the other hand, the standard afficity and enthalpy were increased with the in crease of hydrophobic part of dyes. Both $k_1$ and $K_2$ were decreased with the increase of pH, but $k_2$ were more effected than $K_1$.

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Comparison of the Electronic Methods of Raw Silk Testing and Grading with Those of the Current Methods I. Defference in Inspection Results and Grading to the Electronic Methods (생사검사에 있어서 현행방법과 전자식 방법에 대한 비교분석 I. 전자식 검사방법에 의한 검사성적과 등급비교)

  • 최병희;김한수
    • Journal of Sericultural and Entomological Science
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    • v.34 no.1
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    • pp.57-71
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    • 1992
  • These studies were carried out to establish Korean opinion about "The electronic method of raw silk testing and grading" which was taken shape along with the report by Silk Standard Committee(S.S.C.) at the meeting of International Silk Association(I.S.A) Directing Board session held in Zurich Swiss. This establishment was througly examine whether or not the above are the essential factors to be fulfilled in force as a international standard method of raw silk testing and grading.d grading.

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The Effect of Organic Solvent in the Dyeing of Silk Fiber (견섬유의 염색에 있어서 첨가용제의 영향( I ))

  • 황성민;윤남식;임용진;이동수;이인전
    • Textile Coloration and Finishing
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    • v.1 no.1
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    • pp.47-53
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    • 1989
  • The effect of organic solvent in the dyeing of silk fiber by acid dye was investigated. Acetophenone and benzyl alcohol were shown to be the most effective for the rate of dyeing of silk fiber by Milling Cyanine 5R (C.I. Acid Blue 113), a milling type acid dye, but, with benzyl alcohol, the equilibrium dye uptake was much lower than that in the absence of it. In the presence of solvent, maximum dye uptake shifted to lower temperature than 6$0^{\circ}C$, while without solvent, it was shown at about $60^\circ{C}$. When dyed by Orange II (C.I. acid Orange 7) under same condition equilibrium dye uptake of silk fiber was lower than that for milling type acid dye, and in the presence of benzyl alcohol, still much lower uptake resulted. All these fact reveals that organic solvents in the solvent-assisted dyeing of silk fiber broaden micelle spacings too much, resulting in increased rate of dyeing, and decreased equilibrium dye uptake, contrary to wool.

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Influence of Temperature on Microsporidian Multiplication and Spore Production in Various Tissues of Silkworm (Bombyx mori L.) During Larval Development

  • Mohanan N. Madana;Krishnan N.;Mitra P.;Das K.K.;Saratchandra B.;Haldar D.P.
    • International Journal of Industrial Entomology and Biomaterials
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    • v.12 no.2
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    • pp.87-93
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    • 2006
  • Multiplication and spore production of three microsporidia viz., Nosema bombycis, Nosema sp. 1 and Nosema sp. 2 in fifth instar larval tissues of silkworm, Bombyx mori L. in two seasons with distinct temperature regimes were studied. Nosema sp. 2 produced significantly (P < 0.01) higher number of spores in various tissues. Among the tissues, spore production was highest in silk gland, followed by fat body and gut. Spore production was significantly (P < 0.01) higher in season-II (Average temperature $29.4{\pm}1.1^{\circ}C$). Maximum spore production was observed 25 days post inoculation (p. i.) in season-I (Average temperature $18.9{\pm}1.1^{\circ}C$), whereas in season-II, it was 14 days p. i. In season-I, spore production was low up to 21 days p. i., then increased sharply. In season-II, there was a steady increase in spore production. The results indicate that the microsporidian multiplication is tissue specific and extremely sensitive to temperature at which the host is reared. It also reveals that, silk gland, fat body and gut are the most appropriate tissues for microscopic identification of microsporidia in the larval stage.

Characteristics of the Excavated Fabrics form ewongun's Tomb (의원군묘 출토직물에 관한 연구)

  • 조효숙;안지원
    • Journal of the Korean Society of Clothing and Textiles
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    • v.26 no.10
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    • pp.1390-1400
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    • 2002
  • The purpose of this study is to categorize the type of fabrics and to analyze weaving method on the silk fabrics from ewongun's Tomb. The conclusions of this research are as follow. 1) Among the 26pieces of excavated clothes,98% of them were made of silk fabric and among them 84% used high-quality non-patterned silk I would assume, therefore, that the tomb was owned by a person who had a dignified yet humble tagte of higher society. 2) The weaving methods of textiles are plain weave, twil1 weave, satin weave. Plain weave includes spun silk tabby, fine filament silk tabby, raw silk tabby, thine silk tabby, damask on tabby, twill weave includes twill damask with different directions, satin weave includes non-patterned satin damask,5-end satin damask(4/1 warp faces ground, l/4 wok faced pattern). As the result of literature survey, I settled the names of textiles as follows; tabby was called Myunju, Saeju, Saengcho, and Sookcho according to the kind and density of silk threads used; Damask on tabby was ca]led Hwamunju) Twill damask was called Hwmunnung Satin damask was ca]led Hwamundan if they bear patterns by themselves or Mumundan if they don't have any patterns on them.

The Effect of Benzyl Alcohol on Dyeing Properties of Silk fiber (I) - The Rate of Dyeing by Milling Acid Dye - (Benzyl Alcohol이 견섬유의 염색성에 미치는 영향(I) - Milling계 산성염료에 의한 염색속도 -)

  • 탁태문;김종호;배도규
    • Textile Coloration and Finishing
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    • v.4 no.2
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    • pp.55-63
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    • 1992
  • The effects of benzyl alcohol on the properties of dyeing kinetic of silk fibroin were studied. The acid dye used was C.I. Acid Red 114. The half dyeing time is shorten by addition of benzyl alcohol. The diffusion activation energy is higher with the increase of the solvent. The rate of dyeing at benzyl alcohol addition to the purified silk fibroin is faster than that of the unpurified one.

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Studies on the Sorption and Permeating of Acid dyes through silk fibroin Membrane(I) (견 피브로인 막을 통한 산성염료의 흡착과 투과에 관한 연구(I))

  • 배도규;탁태문
    • Journal of Sericultural and Entomological Science
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    • v.30 no.2
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    • pp.105-111
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    • 1988
  • 견 피브로인과 그 응용에 관한 기초적인 자료를 얻기 위하여, 본 연구에서는, 견섬유와 피브로인막의 구조에 대해서 IR, DSC, X-ray diffraction, SEM, 아미노산분석 등의 조사를 통하여 구조변화를 비교하였다. IR과 DSC를 통하여 얻은 결과, 피브로인 막의 구조는 대부분 random coil과 Silk I type으로 구성되어 있지만, Silk II type의 존재도 인정되었다. 피브로인 막을 전자현미경으로 관찰한 결과, 표면은 구상체로 치밀하게 형성되어 있었고, 단면구조는 거의 대칭적인 것임을 알았다. 견섬유와 피브로인 막의 아미노산 분석결과, 전체에 대한 염기성 아미노산의 함량은 피브로인 막보다 견섬유가 더 많은 것을 알 수 있다.

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Embroideries in Shoso-in of Japan and their Maker (일본 정창원의 경수와 그 제작국)

  • 이춘계
    • Journal of the Korean Society of Costume
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    • v.25
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    • pp.145-155
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    • 1995
  • After I stated the kinds of ancient embro-ideries of Shoso-in and the other places in Japan, including Silk embroidered design of a bird, Silk embroidery on a silk ground, and Buddha preaching. I searched for the possible countries they could have been made in. I found that Japan merely imported the dyes and paints from Korea, On the other hand, Korea unlike Japan, was capable of manufac-turing the embroderies from early times. The embroideries in Shoso-in and the other place, have respectivly on them the old Korean types of patterns such as flowers, lotuses, flying clouds, phoenixes, intertwined lions, houses, ghost masks, fairies and turtles, seen often on the titles of Silla.

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Effects of Methacrylamide Treatment on Silk Fibers I. Effects of Reaction Conditions on Weight Increase of Silk Fibers (견섬유에 대한 메타크릴아미드의 처리효과 I. 반응조건에 따른 견섬유의 무게 증가)

  • 신태섭;남중희
    • Journal of Sericultural and Entomological Science
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    • v.33 no.2
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    • pp.82-86
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    • 1991
  • The treatments of methacrylamide on silk fibers were studied in aqueous solution using potassium persulfate as an initiator, and suitable conditions of reaction were determined for weighing of silk fibers. The results obtained were summarized as follows ; The weight of MAA-treated silk fibers increased with monomer concentration. The adequate concentration of potassium persulfate was found to be 1.7%. Maximum weight increase was shown at initial pH 3.8 of reaction liquor controlled by buffer solution.

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Effect of Surfactant on Homogeneity of Partially Degummed Silk Fiber

  • Chung, Da Eun;Um, In Chul
    • International Journal of Industrial Entomology and Biomaterials
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    • v.28 no.1
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    • pp.19-24
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    • 2014
  • Silk has always been one of the most favored textile materials. Fully degummed silk fiber (i.e., silk fibers without sericin) shows better luster than raw silk fiber (with sericin); it is also softer. On the other hand, raw silk fiber feels cooler because of the presence of sericin, making it useful as a textile for the summer season. Recently, partially degummed silk has attracted researchers' attention because it provides better luster, feel, and dyeing properties. However, the partial degumming of silk is very difficult because it results in inhomogeneously degummed fiber. In the present study, silk yarns were degummed with surfactant aqueous solutions and the effects of each surfactant on the degumming ratio, crystallinity, and homogeneity of the degummed silk yarn were examined. The degumming ratio and crystallinity index of silk yarn varied depending on the type of surfactant. On the whole, anionic surfactants resulted in higher degumming ratios and better homogeneity than nonionic surfactants.