• 제목/요약/키워드: SiC coating

검색결과 562건 처리시간 0.024초

폴리카보실란을 이용하여 탄소단열재에 코팅한 실리콘카바이드 코팅막의 내산화 특성 (Preperation of Silicon Carbide Oxidation Protection Film on Carbon Thermal Insulator Using Polycarbosilane and Its Characterization)

  • 안수빈;이윤주;방정원;신동근;권우택
    • 한국재료학회지
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    • 제27권9호
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    • pp.471-476
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    • 2017
  • In order to improve the high temperature oxidation resistance and lifespan of mat type porous carbon insulation, SiC was coated on carbon insulation by solution coating using polycarbosilane solution, curing in an oxidizing atmosphere at $200^{\circ}C$, and pyrolysis at temperatures up to $1200^{\circ}C$. The SiOC phase formed during the pyrolysis process was converted into SiC crystals as the heat treatment temperature increased, and a SiC coating with a thickness of 10-15 nm was formed at $1600^{\circ}C$. The SiC coated specimen showed a weight reduction of 8.6 % when it was kept in an atmospheric environment of $700^{\circ}C$ for 1 hour. On the other hand, the thermal conductivity was 0.17 W/mK, and no difference between states before and after coating was observed at all.

Processing and Microstructure of Alumina Coated with $Al_2O_3$/SiC Nanocomposite

  • Ha, Jung-Soo;Kim, C-S.;D-S. Cheong
    • 한국결정성장학회:학술대회논문집
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    • 한국결정성장학회 1997년도 Proceedings of the 12th KACG Technical Meeting and the 4th Korea-Japan EMGS (Electronic Materials Growth Symposium)
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    • pp.19-22
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    • 1997
  • The surface modificaion of alumina by $Al_2$O$_3$/SiC nanocomposite coating was studied in terms of processing and microstructure. A powder slurry of 5 vol% SiC composition was dipcoated onto presintered alumina bodies and pressurelessly sintered at 1$700^{\circ}C$ for 2 h in $N_2$. The used of organic binder and plasticizer in the slurry preparation, and the control of the density of presintered alumina body were found to be necessary to avoid cracking and warping during processing. The nanocomposite coating well bonded to the alumina body with thickness about 110 ${\mu}{\textrm}{m}$. The average grain size of coating (2 ${\mu}{\textrm}{m}$) was much finer than that of alumina body (13 ${\mu}{\textrm}{m}$). Fracture surface observations revealed mostly transgranular fracture for the coating, whereas intergranular fracture for the alumina body. Some pores (about 6%) were observed in the coating layer, although the alumina body showed fully dense microstructure.

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Squeeze Casting법에 의해 제조된 A356/coated SiC복합재료의 미세조직과 기계적 특성에 관한 연구 (A Study on Microstructures and Mechanical Properties of A356/coated SiC Composites Fabricated by Squeeze Casting)

  • 이경구;이도재
    • 한국주조공학회지
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    • 제14권5호
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    • pp.429-437
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    • 1994
  • Influence of interfacial structure between matrix and particle in A356/coated SiC composite fabricated by squeeze casting method was studied. Experimental variables are types of coated metallic film on SiC particles such as Cu, Ni-P, and applied pressure for squeeze casting. It was found that coating treatment on SiC particles improves the wetting of liquid A356 alloy on SiC particles. SiC particle distribution is very homogeneous in A356 matrix alloy which is fabricated by squeeze casting. Analysing the surface morphology of fractured A356/coated SiC, it was concluded that metallic thin film by coating treatment on SiC particle improves the interfacial bonding between particle and matrix, and so does on mechanical properties such as tensile strength. However, there was on significant difference in hardness between those composite made of as-received SiC particle and coated SiC particle.

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용융 Si 침윤법에 의해 제조된 반응소결 탄소 섬유강화 탄화규소 복합체 제조; I. 탄소 섬유 코팅 방법에 따른 영향 (Fabrication of Carbon Fiber Reinforced Reaction Bonded SiC Composite Fabricated by a Molten Si Infiltration Method; I. The Effect of Carbon Fiber Coating Process)

  • 윤성호;;조경선;정훈;김영도;박상환
    • 한국세라믹학회지
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    • 제45권9호
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    • pp.531-536
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    • 2008
  • Reaction bonded silicon carbide (RBSC) composite for heat-exchanger was fabricated by molten Si infiltration method. For enforcing fracture toughness to reaction bonded silicon carbide composite, the surface of carbon fiber has coating layer by SiC or pyro-carbon. For SiC layer coating, CVD method was used. And for carbon layer coating, the phenol resin was used. In the case of carbon layer coating, fracture toughness and fracture strength were enhancing to 4.4 $MPa{\cdot}m^{1/2}$ and 279 MPa.

Enhanced Corrosion Resistance of WC-Co with an Ion Beam Mixed Silicon Carbide Coating

  • 여순목;박재원
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2011년도 제41회 하계 정기 학술대회 초록집
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    • pp.193-193
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    • 2011
  • Strong adhesion of a silicon carbide (SiC) coating to a WC-Co substrate was achieved through an ion beam mixing technique and the corrosion resistance of the SiC coated WC-Co was investigated by means of a potentiodynamic electrochemical test. In a 1 M NaOH solution, the corrosion current density of SiC-coated WC-Co after heat treatment at 500$^{\circ}C$ was about 50 times lower than that for the as-received WC-Co. In addition, the corrosion resistance systematically increases with increasing the SiC coating thickness. On the other hand, for a 0.5 M H2SO4 solution, the corrosion current density for SiC-coated WC-Co was about 3 times lower than that for the as-received WC-Co. We discuss the physical reasons for the changes in the corrosion current density with the different electrolytes.

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CrN/AlSiN multilayer coatings의 고온안정성 및 특성에 관한 연구

  • 김영수;김광석;김성민;허용강;이상율
    • 한국표면공학회:학술대회논문집
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    • 한국표면공학회 2008년도 추계학술대회 초록집
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    • pp.47-47
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    • 2008
  • Cr and AlSi (Si=20 and 66 at.%) target들을 이용하여 Closed-field unbalanced magnetron sputtering (CFUBMS)으로 증착된 주기($\Lambda$)가 2.3 nm에서 8.0nm인 CrN/AlSiN multilayer coatings의 crystal structure, 화학적 조성, 및 기계적 특성을 glow discharge optical emission spectroscopy (GDOES), X-ray diffractometry (XRD), X-ray photoelectron spectroscopy (XPS) and nano-indenter 등의 분석장비를 이용하여 분석하였다. 고온안정성을 시험하기 위하여 $800^{\circ}C$$1000^{\circ}C$ 공기중 에서 30분 열처리하였다. CrN/AlSiN multilayer coatings의 고온안정성은 Si조성이 증가함에 따라 향상되었다. Si이 18.2 at.%함유된 coating이 가장 우수한 고온안정성을 갖고 있다.

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흑연의 내산화성 증진을 위한 실험 계획법에 따른 탄화규소 코팅에 관한 연구 (A Study of the Pack Cemented SiC Coating on Graphite by Experimental Design)

  • 서임춘;리원준;예병한;박종욱
    • 한국세라믹학회지
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    • 제29권10호
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    • pp.785-790
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    • 1992
  • A study of the pack cemcented SiC coating on graphite was performed and the process conditions were evaluated by means of experimental design. The content of Si, P2O5, B and Al2O3 reaction temperature, reaction time and acid treatment wast tested as the experimental variables. The results were analyzed and compared by the characteristic value of 10% weight loss by oxidation. The acid treatment exhibited the most effective anti-oxidation property and the optimum conditions were the powder composition of 20% Si, 3% B and 77% SiC, the reaction temperature of 1550$^{\circ}C$ for 7 hours with phosphoric acid treatment. The pack coating performed under this condition improved the 10% weight loss oxidation temperature by 514$^{\circ}C$ compared to the bare graphite.

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알콕사이드로부터 $Al_2O_3-SiC$ 복합재료의 제조 및 특성 (Synthesis and Properties of $Al_2O_3-SiC$ Composites from Alkoxide)

  • 이형민;이홍림;조덕호
    • 한국세라믹학회지
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    • 제32권10호
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    • pp.1212-1218
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    • 1995
  • Al2O3-coated SiC composite powder and mechanically mixed Al2O3-SiC composite powder were synthesized using Al-isopropoxide and commercial SiC as the starting materials. Experiment results showed that the sinterability of Al2O3-coated SiC composite powder was more improved than the mechanically mixed Al2O3-SiC composite powder by the effect of homogeneous coating of alumina around SiC particles. Hence, the mechanical properties of the former was also much more improved than the latter.

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TiO2/SiOxCy 이중 박막을 이용한 투명 친수성/내마모성 반사방지 코팅 (Anti-Reflective Coating with Hydrophilic/Abraion-Resistant Properties using TiO2/SiOxCy Double-Layer Thin Film)

  • 이성준;이민교;박영춘
    • 한국표면공학회지
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    • 제50권5호
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    • pp.345-351
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    • 2017
  • A double-layered anti-reflective coating with hydrophilic/abrasion-resistant properties was studied using anatase titanium dioxide($TiO_2$) and silicon oxycarbide($SiO_xC_y$) thin film. $TiO_2$ and $SiO_xC_y$ thin films were sequentially deposited on a glass substrate by DC sputtering and PECVD, respectively. The optical properties were measured by UV-Vis-NIR spectrophotometer. The abrasion-resistance and the hydrophilicity were observed by a taber abrasion tester and a contact angle analyzer, respectively. The $TiO_2/SiO_xC_y$ double-layer thin film had an average transmittance of 91.3%, which was improved by 10% in the visible light region (400 to 800 nm) than that of the $TiO_2$ single-layer thin film. The contact angle of $TiO_2/SiO_xC_y$ film was $6.9^{\circ}$ right after UV exposure. After 9 days from the exposure, the contact angle was $10.2^{\circ}$, which was $33^{\circ}$ lower than that of the $TiO_2$ single-layer film. By the abrasion test, $SiO_xC_y$ film showed a superior abrasion-resistance to the $TiO_2$ film. Consequently, the $TiO_2/SiO_xC_y$ double-layer film has achieved superior anti-reflection, hydrophilicity, and abrasion resistance over the $TiO_2$ or $SiO_xC_y$ single-layer film.