• 한국복합재료학회:학술대회논문집
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• 한국복합재료학회 2000년도 춘계학술발표대회 논문집
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• pp.139-142
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• 2000

The SiCp/AC8A composites were fabricated by the pressureless metal infiltration process successfully. The effect of additional Mg, which were mixed with SiC particles to promote interfacial wetting between the reinforcement and matrix alloy, and particle size on the mechanical properties was investigated. By increasing the additional Mg content the hardness of SiCp/AC8A composites was increased due to the hard reaction products, but the bending strength was decreased by the excess reaction of Mg and high porosity level when the additional Mg content is over 7%. The Hardness and bending strength was increased by decreasing the size of SiC particle.

• 대한기계학회논문집
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• 제16권10호
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• pp.1869-1876
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• 1992

본 연구에서는 고온에서 높은 강도특성을 유지하면서 동시에 내마모성이 뛰어 나 가스터어빈의 부재로서의 사용이 기대되는 탄화규소(SiC) 세라믹에 대하여, 고체입 자의 충격에 의해 생기는 손상에 미치는 입자의 재질 및 크기의 영향을 조사하였다. 또 각 형태의 손상발생 임계치와 강도저하에 미치는 입자크기의 영향에 관해서도 검토 하였다.

• 한국분말재료학회지
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• 제13권6호
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• pp.421-426
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• 2006

The microstructural and mechanical properties of Al-Si alloyed powder, prepared by gas atomization fallowed by hot extrusion, were studied by optical and scanning electron microscopies, hardness and wear testing. The gas atomized Al-Si alloy powder exhibited uniformly dispersed Si particles with particle size ranging from 5 to $8{\mu}m$. The hot extruded Al-Si alloy shows the average Si particle size of less than $1{\mu}m$. After heat-treatment, the average particle size was increased from 2 to $5{\mu}m$. Also, mechanical properties of extruded Al-Si alloy powder were analyzed before and after heat-treatment. As expected from the microstructural analysis, the heat-treated samples resulted in a decrease in the hardness and wear resistance due to Si particle growth. The friction coefficient of heat-treated Al-Si alloyed powder showed higher value tough all sliding speed. This behavior would be due to abrasive wear mechanism. As sliding speed increases, friction coefficient and depth and width of wear track increase. No significant changes occurred in the wear track shape with increased sliding speed.

• The Korean Journal of Ceramics
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• 제3권3호
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• pp.199-207
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• 1997

$Al_2O_3$/SiC particulate composites were fabircated by pressureless sintering. The dispersed phase was SiC of which the content was varied from 1.0 to 10 vol%. Three SiC powders having different median diameters from 0.28 $\mu\textrm{m}$ to 1.9 $\mu\textrm{m}$ were used. The microstructure became finer and more uniform as the SiC content increased except the 10 vol% specimens, which were sintered at a higher temperature. Under the same sintering condition, densification as well as grain growth was retarded more severly when the SiC content was higher or the SiC particle size was smaller. The highest flexural strength obtained at 5.0 vol% SiC regardless of the SiC particle size seemed to be owing to the finer and more uniform microstructures of the specimens. Annealing of the specimens at $1300^{\circ}C$ improved the strength in general and this annealing effect was good for the specimens containing as low as 1.0 vol% of SiC. Fracture toughness did not change appreciably with the SiC content but, for the composites containing 10 vol% SiC, a significantly higher toughness was obtained with the specimen containing 1.9$\mu\textrm{m}$ SiC particles.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2001년도 추계학술대회 논문집 Vol.14 No.1
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• pp.121-125
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• 2001

We study the feasibility of synthesizing Si particles using PLA method. In the previous studies, it was possible to control the size of Si nanoparticles by the He gas pressure. In this study, we fabricated sub-micron size Si particles with various shapes such as conical, hexagonal, and ring by controlling not only the ambient gas pressure but also the laser energy density. Furthermore, we found that the conical Si particles were uniform-sized and had step shape when observed from FE-SEM and AFM. The conical Si particle has the same crystal structure as the bulk single crystalline Si by the analysis of the Raman scattering. It is shown that the relationship between the laser energy density and the He gas pressure inside the chamber affects the shape of the Si particle.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2001년도 추계학술대회 논문집
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• pp.121-125
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• 2001

We study the feasibility of synthesizing Si particles using PLA method. In the previous studies, it was possible to control the size of Si nanoparticles bythe He gas pressure. In this study, we fabricated sub-micron size Si particles with various shapes such as conical, hexagonal, and ring by controlling not only the ambient as pressure but also the laser energy density. Furthermore, we found that the conical Si particles were uniform-sized and had step shape when observed from FE-SEM and AFM. The conical Si particle has the same crystal structure as the bulk single crystalline Si by the analysis of the Raman scattering. It is shown that the relationship between the laser energy density and the He gas pressure inside the chamber affects the shape of the Si particle.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2007년도 춘계학술대회A
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• pp.126-129
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• 2007

The particle formation using pyrolysis has many advantages over other particle manufacturing techniques. The particles by pyrolysis have relatively uniform size and chemical composition. Also, we can easily produce high purity particles. Thus, we studied the formation of silicon particles by pyrolysis of 50% $SiH_4$ gas diluted in Ar gas. A pyrolysis furnace was used for the thermal decomposition of $SiH_4$ gas at $800^{\circ}C$ and atmospheric pressure. The aerosol flow from furnace is separated into two ways. The one is to the Scanning Mobility Particle Sizer (SMPS) for particle size distribution measurement and the other is to the particle deposition system. The produced silicon particles are deposited on the wafer in the deposition chamber. SEM measurement was used to compare the particle size distribution results from the SMPS. Depending on the experimental conditions, particles of high concentration in the $30\sim80$ nm size range were generated.

• 한국산학기술학회논문지
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• 제16권7호
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• pp.4835-4841
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• 2015

n형 FeSi2의 열전물성에 미치는 입자크기 및 성형압력의 영향에 대해 조사하였다. 입자크기가 다른 출발 분말을 각각 가압성형(성형압력; $70{\sim}220kg/cm^2$) 하였고, 제작한 성형체를 Ar 분위기 1473 K에서 7시간 소결한 후, 반도체상인 ${\beta}$상을 얻기 위해 1103 K에서 100시간 소둔처리 하였다. XRD, SEM 및 EDS를 이용해서 시편들의 미세구조 및 상분석을 행하였다. 동일 시료를 가지고 Ar 분위기 상온~1023 K에서 도전율과 Seebeck 계수를 동시에 측정하였다. 입자크기가 작을수록 소결밀도와 잔존 ${\varepsilon}$-FeSi 금속전도상 증가에 의해 도전율이 상승하였으며, Seebeck 계수는 700~800 K에서 최고값을 나타내었고, 입자크기가 작을수록 잔존 ${\varepsilon}$-FeSi 금속전도상 증가에 의해 감소하였다. 반면에 성형압력의 변화는 도전율 및 Seebeck 계수에 그다지 큰 영향을 미치지 않았다. 결과적으로 power factor는 성형압력 보다 입자크기에 큰 영향을 받았다.

• 한국분말재료학회지
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• 제7권1호
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• pp.27-34
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• 2000

The fabrication process and mechanical properties of SiC particle prefrrms with high volume fraction ranged 50∼71% were investigated to make metal matrix composites for possible applications as heat sinks in electronic packares. The SiC particle preforms with 50∼71vol% of reinforcement were fabricated by a new modified process named ball milling and pressing method. The SiC particle performs were fabricated by ball milling of SiC particles with single sized of 48${\mu}$m in diameter or two different size of 8${\mu}$m and 48${\mu}$min diameter, with collodal SiO2 as inorgnic binder in distilled water, and the mixed slurries were cold pressed for consolidation into final prefom. The compressive strengths og calcined SiC particle prefoms increased from 20MPa to 155MPa with increasing the content of inorganis binder, temperature and time for calcination. The increase of compressive strength of SiC particle bridge the interfaces of two neighboring SiC particles.

• 한국분말재료학회지
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• 제21권5호
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• pp.331-337
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• 2014

The effects of particle size of Li-Si alloy and LiCl-KCl addition as a binder phase for raw material of anode were investigated on the formability of the thermal battery anode. The formability was evaluated with respect to filling density, tap density, compaction density, spring-back and compressive strength. With increasing particle size of Li-Si alloy powder, densities increased while spring-back and compressive strength decreased. Since the small spring-back is beneficial to avoiding breakage of pressed compacts, larger particles might be more suitable for anode forming. The increasing amount of LiCl-KCl binder phase contributed to reducing spring-back, improving the formability of anode powder too. The control of particle size also seems to be helpful to get double pressed pellets, which consisted of two layer of anode and electrolyte.