• 제목/요약/키워드: Si distribution

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급속응고 Al-Si계 합금의 단조공정에 대한 유한요소 해석 (Finite Element Analysis for Forging Processes of Rapidly Solidified Al-Si Alloys)

  • 손현택
    • 한국분말재료학회지
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    • 제5권1호
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    • pp.57-63
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    • 1998
  • The densification behaviors of rapidly solidified Al-Si alloys under high temperature processing were investigated. In general, it was difficult to establish optimum process variables for forging condition through experimentation, because this was costly and time consuming. In this paper, to overcome these problems, we compared the experimental result to the finite element analysis for forging processes of rapidly solidified Al-Si alloys. The results of these simulations helped understand the distribution of relative density during various forging processes. This information is expected to assist in improving rapidly solidified Al-Si alloys forging operations.

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CaO${\cdot}2SiO_2$ 또는 $SiO_2$을 적하한 8 mol% 이트리아 안정화 지르코니아에서의 계면상 분포 : 임피던스 측정에 의한 평가 (Intergranular-phase Distribution in $CaO{\cdot}2SiO_2-$ or $SiO_2-dropped$ 8 mol%-Yttria-Stabilized Zirconia : Impedance Spectroscopic Estimation)

  • 정영수;최정혜;이종흔;이제훈;김도연
    • 한국세라믹학회:학술대회논문집
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    • 한국세라믹학회 2003년도 추계총회 및 연구발표회 초록집
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    • pp.42.2-42
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    • 2003
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2단 튜브형 가열로 반응기에 의한 초미세 SiO2 입자의 제조 및 증착 연구 (A Study on Ultrafine SiO2 Particles Generation and Deposition by 2-Stage Tube Furnace Reactor)

  • 유수종;김교선
    • 산업기술연구
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    • 제17권
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    • pp.233-239
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    • 1997
  • The effects of preheating the gas stream on deposition characteristics of ultrafine $SiO_2$ particles were investigated theoretically. The model equations such as mass and energy balance equations and aerosol dynamic equations were solved to predict the particle growth and deposition. The gas temperatures, $SiCl_4$ concentrations, $SiO_2$ particle volumes, $SiO_2$ particle sizes and deposition efficiencies of $SiO_2$ particles were calculated for various preheating temperatures. As the preheater setting temperature increases, the $SiO_2$ particle size distribution becomes more uniform, because the effect of $SiCl_4$ diffusion decreases.

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Rheo-Compocasting에 의한 $SiC_p$/6063 Al합금의 복합조직 (Composite Structures of $SiC_p$/6063 Aluminum Alloy by Rheo-Compocasting.)

  • 최정철
    • 한국주조공학회지
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    • 제10권4호
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    • pp.309-315
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    • 1990
  • Aluminum alloy matrix composites reinforced by SiC particles were prepared by rheocompocasting, a process which consists of the incoporation and distribution of reinforcement by stirring within a semi-solid alloy. When the volume fraction of SiCp and stirring speed were fixed, the dispersion of SiCp in Al-matrix alloy depended on stirring time and solid volume fraction in slurry. The results were as follows : 1) As a dispersed SiCp during stirring at $647^{\circ}C$ in 6063-Al alloy, SiC was better dispersed than that other temperature, where solid volume fraction was 43% in slurry. 2) When increased solid fraction in slurry, rate of dispersing SiC increased during stirring and porosities decreased in matrix alloy after casting. 3) Inspite of stirring with 800rpm, since solid particles of matrix alloy in slurry joined each other and occured joining growth, so that SiC was not dispersed into solid particle.

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아공정 Al-Si합금 조직에 미치는 Sc의 효과 (The Effects of Sc on the Microstructure of Hypoeutectic Al-Si Alloys)

  • 김명한;이종태
    • 한국주조공학회지
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    • 제24권3호
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    • pp.145-152
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    • 2004
  • The eutectic Si in Al-8.5wt.%Si alloy was changed from large flake to fine lemellar(or fibrous) shape when the Sc amount in the Al-Si alloy reaches 0.2wt.%. The optimum amount of Sc for the best modification effect was 0.8wt.% and slight decrease of modification effect occurred over this value. The study on the distribution of the modifiers(Sr, Na, and Sc) and the measurement of the surface tension of the Al-8.5wt.%Si alloy melt added with Sr, Na, and Sc modifier, respectively, reveals that Sc modifies the eutectic Si by the decrease of surface tension, while Sr and Na modify the eutectic Si mainly by impurity induced twinning mechanism.

과공정 Al-18% Si 합금의 레올로지 성형시 기계적 교반을 이용한 입자 미세화 연구 (Studies on Grain Size Refinement for Rheocasting of Hypereutectic Al-18% Si by Using Sieve Type Mechanical Stirrer)

  • 강용기;박진욱;강성수;강충길;문영훈
    • 소성∙가공
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    • 제9권4호
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    • pp.389-394
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    • 2000
  • The studies on gram size refinement for rheocast processing of hypereutectic Al-18%Si alloys have been investigated in the present study. To increase the efficiency of mechanical stirring, sieve type stirrer are newly designed and implemented for rheocasting of hypereutectic Al-18%Si alloy. Mechanical stirring of semi-solid slurry by using sieve type mechanical stirrer results in morphological changes of the primary Si particles, from angular rod shape to near spherical shape and uniform distribution of proeutectic Si. The remarkable spheroidization of Primary Si Particles and distributional uniformity of proeutectic Si show well the efficiency of sieve type mechanical stirring method which can accelerate the coalescence-fracture-wear of the individual particles by strong turbulent flow between lattices during rotation of sieve type stirrer.

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XPS와 SIMS를 이용한 PSG/SiO2/Al-1%Si 적층 박막내의 Na 게터링 분석 (Analysis of the Na Gettering in PSG/SiO2/Al-1%Si Multilevel Thin Films using XPS and SIMS)

  • 김진영
    • 한국표면공학회지
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    • 제49권5호
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    • pp.467-471
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    • 2016
  • In order to investigate the Na gettering, PSG/$SiO_2$/Al-1%Si multilevel thin films were fabricated. DC magnetron sputter techniques and APCVD (atmosphere pressure chemical vapor deposition) were utilized for the deposition of Al-1%Si thin films and PSG/$SiO_2$ passivations, respectively. Heat treatment was carried out at $300^{\circ}C$ for 5 h in air. SIMS (secondary ion mass spectrometry) depth profiling and XPS (X-ray Photoelectron Spectroscopy) analysis were used to determine the distribution and binding energies of Na, Al, Si, O, P and other elements throughout the PSG/$SiO_2$/Al-1%Si multilevel thin films. Na peaks were mainly observed at the the PSG/$SiO_2$ interface and at the $SiO_2$/Al-1%Si interfaces. Na impurity gettering in PSG/$SiO_2$/Al-1%Si multilevel thin films is considered to be caused by a segregation type of gettering. The chemical state of Si and O elements in PSG passivation appears to be $SiO_2$.

원심분무에 의한 Uranlum filicide 분산핵연료의 제조와 특성 (Preparation and Characterization of Uranium Silicide Dispersion Nuclear Fuel by Centrifugal Atomization)

  • 김창규
    • 한국분말재료학회지
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    • 제1권1호
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    • pp.72-78
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    • 1994
  • Two kinds of $U_3Si$ powders and $U_3Si$ dispersed nuclear fuel meats have been prepared by conventional comminution process and a newly developed rotating disk atomization process. In contrast to angular shape and broad size distribution of the conventionally processed powder, the atomized powder was spherical and showed narrow size distribution. For the atomized powder, the heat treatment time for the formation of $U_3Si$ by a peritectoid reaction was reduced to about one tenth, thanks to microstructure refinement by rapid cooling of about 5$\times$104 K/s. The extruding pressure of atomized $U_3Si$ powder and Al powder mixture was lower than that of comminuted $U_3Si$ and Al powder mixture. The elongation of the atomization processed fuel meats was much higher than that of the comminution processed fuel meats and remained over 10% up to 80wt.% of $U_3Si$ powder fraction in the fuel meats. It appears therefore that the loading density of $U_3Si$ in fuel meat can be increased by using atomized $U_3Si$ powder. The atomized spherical particles were randomly distributed, while the comminuted particles with angular and longish shape were considerably aligned along the extrusion direction. Along the transverse direction of the extraction the electrical conductivity of the atomization processed fuel meats was appreciably higher than that of comminution processed fuel meats. This tendency became pronounced as $U_3Si$ content increased. Because the thermal conduction which is believed to be proportioned to the electrical conduction in the nuclear fuel meats occurs in radial direction, the atomization processed fuel can be better used in research reactors where high thermal conductivity is required.

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액상확산접합법을 이용한 Ti 금속기복합재료 제조에 관한 연구 (A Study on Fabrication of Ti Matrix Composites by Liquid Phase Diffusion Bonding)

  • 김경미;우인수;강정윤;이상래
    • 한국재료학회지
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    • 제6권2호
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    • pp.210-220
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    • 1996
  • The purpose of this study is to develop the processing techniques of Fiber Reinforced Metal by Liquid Phase Diffusion Bonding method with SiC fiber as a reinforcing material and CP Ti(Commercial Pure) as a matrix. The microstructure and the distribution of elements in reaction and CP Ti(Commercial Pure) as a matrix. The microstructure and the distribution of elements is reaction zone among CP Ti/Ti-15wt%Cu-20wt%Ni(TCN20)/SiC long fiber were investigated by Optical Microscope, SEM/EDX, EPMA, X-ray and AES. The results obtained in this study are as follows. 1) When Ti matrix composite materials are fabricated under the bonding condition of 1273Kx1200sec, the SiC long fiber was the most suitable reinforcing material for Ti matrix composite materials. 2) With SiC long fiber under same condition, a TiC layer(1.0-1.6$\mu\textrm{m}$) was observed on the surface of SiC long fiber. 3) Liquid Phase Diffusion Bonding has shown the feasibility of production of Ti matrix composite materials.

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$Si^3 N_4$ 구조용세라믹재의 연삭가공시 숫돌마멸에 따른 가공특성 (Machining Characteristics According to the Wheel Wear in Surface Grinding for Structural Ceramics of $Si^3 N_4$)

  • 왕덕현;김원일;신경오
    • 한국공작기계학회논문집
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    • 제12권4호
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    • pp.9-16
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    • 2003
  • In this study, the decision of dressing time for diamond wheel was analyzed by observing with acoustic emission signals and surface roughness, and also obtained the machining characteristics by weibull distribution plot for the values of bending strength. From the experimental study, it was possible to predict the time of re-dressing for the diamond grinding wheel with the analysis of acoustic emission signals and surface roughness values, and following conclusions were obtained. The root-mem-square values of acoustic emission signals were obtained low as the increased of table speed for different abrasive grain size. This is caused by the lack of grinding power which is not able to get rid of all real grinding mass of depth as the table speed is increased. The values of bending strength for ground $Si_3 N_4$ specimens were decreased for gain size of #400 than that of #60, but it was found that the surface roughness values for gain size of #60 were better than that of #400. As compared the shape parameter of weibull distribution plot for the values of bending strength, it was found that the reliability of bending strength for grain size of #60 increased than that of #400.