• Title/Summary/Keyword: Setting time

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Setting Time Evaluation on Cement Paste with Retarder Using Non-Destructive Measurements (비파괴 측정법을 이용한 지연제 첨가 시멘트 페이스트의 응결 평가)

  • Ahn, Yu-Rhee;Jun, Yu-Bin;Yim, Hong Jae
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.26 no.4
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    • pp.48-56
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    • 2022
  • Controlling the setting time of cementitious materials is one of the most important factors in securing early-age performance of concrete structures. Recently, the use of retarding admixtures, which enable the inhibition of some hydration products to control the securing time due to average temperature rise is suggested. Although various non-destructive evaluation methods have been proposed to evaluate cement hydration and hardening of cement-based materials to overcome the limitations of Vicat needle test, experimental research is still required to use the non-destructive evaluation method with added retarding admixtures. In this study, measurements of electrical resistivity and ultrasonic wave velocity in early-aged cement pastes were performed according to the addition of retarding admixture(tartaric acid). The setting time of the cement pastes was evaluated by obtained rising time of the both non-destructive measurements. As a result, the possibility of evaluating the setting delay in cement pastes was confirmed through comparative analysis with the initial and final setting times by Vicat test. In addition, X-ray diffraction results at the rising time of electrical resistivity showed a key hydration product affecting the setting delay.

Influence of Cement Factor on the Strength Development of Concrete at the Early Age (콘크리트의 초기강도 발현에 미치는 시멘트 요인의 영향)

  • 김광화;김은호;임주혁;김규동;한천구
    • Proceedings of the Korea Concrete Institute Conference
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    • 2003.05a
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    • pp.737-740
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    • 2003
  • In this study, the influence of cement factor on the early strength gain and the other properties of concrete is discussed. According to the result, the setting time is faster in order of alumina cement(AC), high-early-strength cement(HSC) and ordinary Portland cement(OPC), and when OPC are replaced with HSC and AC, the final setting time is faster than when only OPC is used. At 10% replacement of AC, the instant setting happens. As the particle of cement is minute, setting time is shortened. As the properties of hardened concrete, the time when compressive strength of 5㎫, which the form can be removed, is gained is about 18 and 16 hours in the case of OPC and HSC respectively, and in the case of AC, it is about 5 hours. It also shows 16 hours at the replacing ratio of HSC of 50%, and 26 and 72 hours at the replacing ratio of AC of 5 and 10% respectively. And it shows 21, 16 and 12 hours with variation of fineness of cement, so early strength gain is fast with an increase of fineness. The coefficient of correlation between compressive strength and the rebound value is over 0.97, is very favorable. Therefore, if the rebound value of P type Schmidt hammer is more than 25, it is thought that the side forms can be removed.

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An Investigation of How the Accelerator Effects the Setting Time and The Headness of Plaster Products (석고제품(石膏製品)에 촉진제(促進劑) 사용시(使用時) 경화시간(硬化時間) 및 경도(硬度)에 미치는 영향(影響)에 관(關)한 실험적(實驗的) 연구(硏究))

  • Hwang, Seung-Sig
    • Journal of Technologic Dentistry
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    • v.19 no.1
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    • pp.43-54
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    • 1997
  • This investigation is carried out of inqurie into the effects of the accelerator on the setting time and haedness when it is used with plaster products. Plaster($\beta$), dental hard stone($\alpha$), and limproved dental hard stone($M{\alpha}$) are selected as the objects of the investigation, since they are most common materials for dental plaster products. Setting time is gauged by means of Vicket Needle and Gilmore Needle, and hardness is gauged by means of Brinell and Vicket Hardness machines. Samples of each material are made in the standerd water powder ratio and with the accelerator repectively, Every material is tested five times each. The results of the tests are as fallow : 1) In each case the setting time is shortened when the accelerator is used. 2) Of the three materials the hardness of the plaster was lowest A($\beta$) < B($\alpha$) < C($M{\alpha}$)} 3) In each case the hardness of the samples made in the standard water powder ratio were higher than that of the sample made with the accelerator. A1 > A2 ; B1>B2 ; C1>C2 4) Final Conclusion : Higher quality cast is expected when it is made in the standard water powder ratio.

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Analysis of fruit growth and post-harvest characteristics of hydroponically grown 'K3' melons (Cucumis melo L.) harvested at different days after fruit setting and stored at low temperature

  • Jung-Soo Lee;Ju Youl Oh
    • Korean Journal of Agricultural Science
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    • v.49 no.2
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    • pp.341-355
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    • 2022
  • This research was to examine the differences in post-harvest quality of melons depending on the harvest time after fruit setting. Musk melon cultivar 'K3' plants were grown in glass house conditions with a hydroponic system, and the fruits were harvested at 50, 60, and 70 days after fruit setting. The post-harvest characteristics of melons stored at 7℃ were measured over 32 days. The harvested fruits at 50, 60, 70 days after fruit setting did not differ significantly in weight, height, or size. Solid sugar content was highest in the fruits harvested at 70 days after fruit setting, but firmness, L* value, and respiration rate were highest in the fruits harvested at 50 days after fruit setting. When the harvested melons were stored at 7℃, 'K3' melons responded differently according to the harvest days after fruit setting. The major changes during storage of 'K3' melons can be summarized as follows: Firmness, respiration, moisture content, and general appearance index during storage were highest in the melons harvested at 50 days after fruit setting, but soluble solid content, fresh weight loss, and sensory evaluation were high in the melons harvested at 60 and 70 days after one. During storage at 7℃, there were no significant differences in the appearance of 'K3' melons harvested at different periods after fruit setting, but difference in soluble solid content and taste were noted. It is recommended that the fruit of 'K3' melon plants be harvested about 60 days after fruiting to provide consumers with the highest quality for taste and for storage.

Fluidity and Setting Properties of Cement Paste by Adding of Fluoro Anhydrite and Fly Ash (불산 무수석고와 플라이 애쉬를 첨가한 시멘트 페이스트의 유동성 및 응결특성)

  • 노재성;김도수;홍성수;임계규;임헌성
    • Journal of the Korean Ceramic Society
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    • v.34 no.12
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    • pp.1261-1267
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    • 1997
  • Four kids of powder admixtures(A, B, C, D) based on anhydrite were manufactured by mixing at a fixed rate of II-anhydrite, fly ash and active silica as an industrial by-product. Fluidity properties of cement paste such as mini-slump, apparent viscosity with elapsed time, as well as setting time of cement pastes of these admixtures substituted up to 11wt% of cement were compared to those of cement paste(SS) substisuted by marketed high-strength powder admixture(S). Among these powder admixtures, the fluidity of cement pastes(PA, PC) substituted by A and C powder admixtures manufactured from II-anhydrite and fly ash had an excellent property than that of cement paste substituted by marketed powder admixture and also a good fluidity-retention effect with elapsed time by adding of superplasticizer. The setting time of cement paste substituted by powder admixtures based on anhydrite slightly retarded than that of cement paste substituted by marketed powder admixture.

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A Method on the Control of Hydration Heat of Mass Concrete Considering the Difference of Setting Time (응결시간차를 활용한 매스콘크리트의 수화열 조정공법)

  • 심보길;윤치환;한민철;김기철;오선교;한천구
    • Proceedings of the Korea Concrete Institute Conference
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    • 2001.11a
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    • pp.379-384
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    • 2001
  • This Paper Presents field application test results of mass concrete using super retarding agent. The field test was carried out at mat foundation(thickness 1m) of newly constructed information center of Chongju university. Placing lift composed of 2 layers, and each layer is 50cm. Fly ash and flowing method is also applied. Difference of setting time of concrete between with super retarding agent and without super retarding agent is considered. Concrete without super retarding agent is placed at upper layer and with super retarding agent at lower layer According to test results, the reducing method of hydration heat considering difference of setting time with super retarding agent can reduce the highest temperature about 3~4$^{\circ}C$, and delay the peak time about 3~4days. Compressive strength using super retarding agent is somewhat higher than that of normal concrete. Accordingly, super retarding agent does not affect the strength development.

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LS code pair setting and sequential allocation methods

  • Wook, Roh-Dong
    • Proceedings of the IEEK Conference
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    • 2001.06a
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    • pp.221-224
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    • 2001
  • A new code: LS code was proposed for IMT-2000 CDMA system. The code has special properties during a certain time of interval: 1) perfect autocorrelation 2) perfect crosscorrelation. The perfect autocorrelation means that the autocorrelation has nMaximum for zero time-offset and zero for other times during a certain time. Moreover the perfect crosscorrelation means that the crosscorrelation has zero during a time of interest. In the LAS-DMA system, the LS code is only used in the spreading of data bits in contrast to the conventional CDMA system. Therefore the LS code pair setting and allocation order should be dealt with carefully considering the special properties of LS code. This paper is intended as an investigation of the setting LS code pair and the sequential allocation method. Firstly, the optimum LS code pair set is proposed in order to minimize PAPR. Secondly, the sequential allocation method is studied to either minimize PAPR or expand IFW.

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Hydration Products, Morphology and Microstructure of Activated Slag Cement

  • Murmu, Meena;Singh, Suresh Prasad
    • International Journal of Concrete Structures and Materials
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    • v.8 no.1
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    • pp.61-68
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    • 2014
  • This paper reports the physical properties and hydration products of slag cement that was prepared by activating ground granulated blast furnace slag with commercial lime and plaster of Paris (POP) as activators. The consistency, setting times and soundness of various mixes of slag-lime-POP is reported. The hydration products and formation of bonds in the paste during setting were studied with the help of SEM, FTIR and XRD tests and the same are correlated to the hydration process. The setting times of the mixes are found to be lower than that of the value prescribed for ordinary Portland cement (OPC). Borax is used as a setting retarder and a borax content of 0.4 % by mass gives setting times that are normally prescribed for OPC. In the early stages of setting C-A-S-H gels are found in this cementing material instead of C-S-H gel, as generally observed in the OPC.

A COMPARISON OF THE SETTING CHARACTERISTICS BETWEEN RESIN-MODIFIED GLASS-IONOMERS AND COMPOMERS (Resin-Modified Glass-Ionomer와 Compomer의 경화 반응 특성의 비교에 관한 연구)

  • Ko, Yong-Joon;Yoo, Hyeon-Mee;Um, Chung-Moon
    • Restorative Dentistry and Endodontics
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    • v.25 no.1
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    • pp.123-132
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    • 2000
  • To overcome problems of conventional glass ionomers, resin components have been added to glass ionomers. On a continuum between glass ionomers and composites are a variety of blends, employing different proportions of acid-base and free radical reactions to bring about cure. Popular groups defined between the ends are resin-modified glass-ionomers(RMGIs), polyacid-modified composite resins(Compomers) and ionomer modified resins. These groups show different clinical properties, and in selecting these materials for a restoration, one should sufficiently understand these different setting properties. In this study, some difference in the setting characteristics of different groups of hybrid ionomers were examined. Two RMGIs (Fuji2 LC,GC / Vitremer, 3M), three Compomers (Dyract AP, Dentsply / F2000, 3M / Elan, Kerr) were involved in this study. The identification of the setting characteristics of different groups was achieved by a two-stage study. First, thermal analysis was performed by a differential scanning calorimeter, and then the hardness of each group at different depth and time were measured by a micro-hardness tester. Thermal analysis was performed to identify the inorganic filler content and to record the heat change during setting process. The setting process was progressed for each material by chemical set mode and light-cured mode. In the hardness test, samples of materials were prepared with a 6mm-diameter metal ring, and the hardness was measured at the top, and 1mm, 2.5mm, 4mm below at just after a 40 second-cure, and after 10 minutes, 24 hours, and 7 days. Statistical analysis was performed by Mann-Whitney rank sum test to assess significant differences between set modes and types of materials, and by ANOVA and T-test to evaluate the statistical meanings of data at different times and depths of each materials. Followings are findings and conclusions derived from this study. Thermal analysis; 1. Compomers show no evidence of chemical setting while RMGIs exhibit heat output during the process of chemical setting. 2. Heat of cure of RMGIs exceed Compomers. 3. The net heat output of RMGIs through light-cured mode is higher than through chemically set mode. Hardness test; 1. Initial hardness of RMGIs immediately after light cure is relatively low, but the hardness increases as time goes by. On the contrary, Comomers do not show evident increase of the hardness following time. 2. Compomers show a marked decrease of setting degree as the depth of the material increases. In RMGIs, the setting degree at different depths does not significantly differ.

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Setting Time and Compressive Strength Gains of Glycocalix Coating Materials with Silica-based Accelerating Agents (실리케이트계 급결제를 혼입한 글라이코 캘릭스 코팅재의 응결시간 및 압축강도 발현 특성)

  • Jeong, Yun-Ji;Yoon, Hyun-Sub;Yang, Keun-Hyeok
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.8 no.1
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    • pp.105-111
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    • 2020
  • The present study examined the effect of the silica-based accelerating agents on the setting time and compressive strength gain of biomimetic glycocalix coating materials that has been developed for protecting the substrate of concrete exposed to chemical and microbiological attacks. The accelerating agent contents varied from 10mL/L to 40mL/L in the mixtures of glycocalix coating materials determined for shotcrete and lining techniques. Test results showed that the setting time of coating materials containing accelerating agents was affected by the contents of the bacteria carrier. When the accelerating agent content was 40mL/L, the final setting time was 80 minutes for shotcrete mixtures and 318 minutes for lining mixtures. Meanwhile, the compressive strength gain of coating materials with accelerating agents tended to be lower than that of counterpart materials without accelerating agents.