• Title/Summary/Keyword: Separation condition

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Simulation of SMB [Simulated Moving Bed] Chromatography for Separation of L-ribose and L-arabinose by ASPEN chromatography (L-ribose와 L-arabinose 분리를 위한 Aspen chromatography를 이용한 SMB [Simulated moving bed] 전산모사)

  • Lee, Seon-Hee;Lee, Eun;Kim, In-Ho
    • KSBB Journal
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    • v.23 no.2
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    • pp.135-141
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    • 2008
  • SMB (simulated moving bed) chromatography is a very useful utility for the separation of binary system. We simulated the separation of L-arabinose and L-ribose from the mixture by using lab-scale 4(1-1-1-1)-zone SMB chromatography. Preliminary experiments of PIM (pulse input method) were performed to measure adsorption isotherms of L-ribose and L-arabinose in $NH_2$ HPLC column, and experimental and simulated results from ASPEN chromatography were compared. To find the most suitable separation condition in SMB, we carried out a simulation in $m_2-m_3$ plane base on the triangle theory and calculated operating parameters (flow rate of four zone, switching time and feed concentration and so on) using ASPEN chromatography under the conditions of linear isotherms obtained from PIM.

Modeling of Foam Separator for Sea Water Treatment (해수 포말분리공정의 해석 및 모델)

  • HUR Hyun-Chul;SEO Jae-Koan;PARK Eun-ju;KIM Sung-Koo
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.32 no.2
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    • pp.165-169
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    • 1999
  • Experiments were conducted to evaluate a experimental model developed for the protein removal by foam separation. The foam separator was operated in well-mixed tank which would be considered as a completely mixed condition. The feasibility of foam separation to remove protein from sea water was investigated. Protein removal characteristics of the foam separator were obtained by batch experiments. To find the effect of the operating parameter to protein removal rate, the foam separation was carried with variation of initial protein concentration and superficial air velocity. The result indicated that the protein removal efficiency was increased with increasing protein concentration and superficial air velocity. The relationship between operation parameters and protein removal rate were evaluated by non-linear regression as the form of exponential function, Using both relationships, the simplified model was determined. The simplified foam separator operation model was verified by the batch operation. The simulation results showed a good relationship with the experimental data.

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Research on the Actual Condition with Regard to the Separation of Dental Technicians (치과 기공사의 이직에 관한 실태조사)

  • Min, Byoung-Kuk
    • Journal of Technologic Dentistry
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    • v.12 no.1
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    • pp.15-21
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    • 1990
  • This research was to investigate and study on 92 Dental Technicians who had had some experience of working or being employed at dental craft-shops or craft-rooms in Seoul area and had transferred to other types of occupation, with regard to their reasons for changing their profession. For an approach to the study, some questionnaires and interview including 3 aspects of in quiriesmental, economic and social backgrounds-were administered, and major findings are as follows ; 1. The ages in which transferring to other kinds of job happened occurred mostly from 20 to 30(78.26%) an a group of subjects whose ages ranged from 20 to 30 years old. And, with regard to their experience of working or being employed at dental craft-shops or craftrooms, the transfer of their profession to the other kinds mosty happened in a group of subjects(94.56%) whose experience of working in the dental field is less than 4 years. 2. The reason of transfer with reference to the mental background was mostly mattered in a group that expressed "Excessive Work Duties"(34.78%), and most lowly mattered in a group of subjets who had "Certain Relations with Dentists"(8.70%). Thus, it appeared that the biggest reason of transfer by the mental background was, due to the excessive duty work, not to have Sufficient time to be usualized by dental technicians for their own purpose. 3. With reference to the economical background, a group that declared there was "No Wage Standards in Ratio to Their Labor" was the most in the separation rate as shown 45.56%. And, a group suspecting "No Guarantee for Their Living after Retirement" Showed a separation rate, 9.78%. In other words, the reason for transfer was that they did not receive due wage according to their amount of labor. 4. With reference to the social background, a group making a subject for no good working environments or conditions had a separation rate, 41.30%, which was the most among others, and a group with a subject of "The Rarity of Employment because of Excessive Supply of Dental Technicians" had the rate, 10.87%, which was the lowest. This meant that the major cause of transfer by the social background was a phenomenon for dental technicans to escape from unclean working places.

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Solvent Extraction Separation of Nd and Pr from Chloride Solution using PC88A and D2EHPA (염산용액(鹽酸溶液)에서 PC88A와 D2EHPA에 의한 Nd와 Pr의 분리추출(分離抽出))

  • Park, Joo-Ho;Jeon, Ho-Seok;Lee, Man-Seung
    • Resources Recycling
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    • v.22 no.5
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    • pp.35-42
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    • 2013
  • Solvent extraction experiments have been performed to investigate an optimum condition to separate Nd and Pr from chloride solutions using PC88A and D2EHPA. In our experimental ranges, the distribution coefficients of Nd were higher than those of Pr. In both of PC88A and D2EHPA extractant system, our results indicated that the increase in concentration ratio of extractant to metal had a great effect on the extraction and separation of the two metals. In extraction with saponified D2EHPA, the initial pH of the aqueous solution and saponification degree had some effect on the extraction of the two metals but little effect on the separation factor.

Synthesis of SiC from the Wire Cutting Slurry of Silicon Wafer and Graphite Rod of Spent Zinc-Carbon Battery (폐 반도체 슬러리 및 폐 망간전지 흑연봉으로부터 탄화규소 합성)

  • Sohn Yong-Un;Chung In-Wha;Sohn Jeong-Soo;Kim Byoung-Gyu
    • Resources Recycling
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    • v.12 no.3
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    • pp.25-30
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    • 2003
  • The synthesis of SiC used for the parts of the gas turbine and the heat exchanger, was carried out. In this study, wire cutting slurry of silicon wafer and the graphite rod of spent zinc-carbon battery were applied to the starting materials for the synthesis. The powders of Si or Si+SiC were obtained from the waste material by filtration, gravity separation and magnetic separation. Graphite powder was produced by dismantling, grinding and gravity separation from spent zinc-carbon battery. The synthesis of SiC could be completed from the mixture powders of Si and C or Si+SiC and C at the condition of equivalent ratio of Si and C, atmosphere of Ar or vacuum, temperature of above 1$600^{\circ}C$ and 2 hours reactions. The purity of synthesized Si-C was above 99%.

Optimizing of Coagulation and Solid-Liquid Separation Conditions Using Aluminum Sulfate and Poly-Aluminum Chloride Coagulants from Brine Wastewater Discharged by the Epoxy-resin Process (에폭시수지 공정에서 발생되는 고염 폐수로부터 황산알루미늄과 PAC 응집제를 이용한 응집/고액분리 조건 최적화)

  • Lee, Chang-Han;Kim, Yu-Jin;Moon, Sung-Hyun;Kwon, Sung-Hun;Ahn, Kab-Hwan
    • Journal of Environmental Science International
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    • v.31 no.1
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    • pp.1-8
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    • 2022
  • In this study, solid-liquid separation conditions for coagulation and sedimentation experiments using inorganic coagulant (aluminum sulfate and Poly-Aluminum Chloride (PAC)) were optimized with brine wastewater discharged by the epoxy-resin process. When the turbidity and suspended solid (SS) concentration in raw wastewater were 74 NTU and 4.1 mg/L, respectively, their values decreased the lowest in a coagulant dosage of 135.0 - 270.0 mg Al3+/L. The epoxy resin was re-dispersed in the upper part of wastewater treated above 405.0 mg Al3+/L. The removal efficiencies of turbidity and SS via dosing with aluminum sulfate and PAC were evaluated at initial turbidity and SS of 74 - 630 NTU and 4.1 - 38.5 mg/L, respectively. They increased most in the range from 135.0 - 270.0 mg Al3+/L. The solid-liquid separation condition was quantitatively compared to the correlation of SS removal efficiency between the coagulant dosage and SS concentration based on the concentration of aluminum ions. The empirical formula, R = beaD, shows the relationship between SS removal efficiency (R) and coagulant dosage (D) at 38.5 mg/L; it produced high correlation coefficients (r2) of 0.9871 for aluminum sulfate and 0.9751 for PAC.

Acceleration data and shape change characteristics of a gravity quay wall according to inclination condition grades

  • Su-Kyeong Geum;Jong-Han Lee;Dohyoung Shin;Jiyoung Min
    • Structural Engineering and Mechanics
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    • v.90 no.6
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    • pp.591-600
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    • 2024
  • This study investigated the acceleration response and shape change characteristics of a gravity quay wall according to the magnitude of the applied acceleration. The quay wall was defined as a port facility damaged by the Kobe earthquake. Four experimental scenarios were established based on the inclination condition grades, considered to be a significant defect factor in the quay wall. Then, the shaking table test was conducted using scaled-down quay wall models constructed per each scenario. The ground acceleration was gradually increased from the peak ground acceleration (PGA) of 0.1 g to 0.7 g. After each ground acceleration test, acceleration installed on the wall and backfill ground and inclination on the top of the wall were measured to assess the amplification of peak response acceleration and maximum response amplitude and the change in the inclination of the quay wall. This study also analyzed the separation of the quay wall from the backfill and the crack pattern of the backfill ground according to PGA values and inclination condition grades. The result of this study shows that response acceleration could provide a reasonable prediction for the changes in the inclination of the quay wall and the crack generation and propagation on the backfill from a current inclination condition grade.

Between-hemisphere Separation of Target and Distractor Reduces Response Interference (표적과 방해자극의 반구간 분리가 반응 간섭에 미치는 영향)

  • Kim Min-Shik;Sohn Young-Sook
    • Korean Journal of Cognitive Science
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    • v.17 no.1
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    • pp.29-52
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    • 2006
  • There has been a claim that Interaction between the cerebral hemispheres could reduce the effect interfering information (Weissman & Banich, 1999). We ran three experiments to show that between-hemisphere separation of target and distractor could be more effective for reducing interference than Interaction between the hemispheres. In experiment 1, a colored box and a rotor name were presented to a single or to separate hemispheres. In experiment 2 and 3, a colored circle (distractor) was presented along with a colored box and a color name which was always printed in black. In experiment 3, a peripheral cue was presented either to the target location(66.7%) or to the distractor location(33.3%) Immediately before the presentation of stimuli. In all experiments, the participants were asked to deride whether the moaning of the color matched the rotor of the box, Ignoring the printed rotor of the word(Exp. 1), or the color of the circle(Exp. 2 & 3). There were three renditions of distractor (congruent, incongruent, and neutral) and two conditions of matching (between- and within-hemisphere matching). If interhemispheric interaction were effective for interference reduction, there should be a decrease in the interference in the between-hemisphere compared to the within-hemisphere matching condition. The results showed that there was no difference in the interference between the two matching conditions in Exp 1. In Exp 2 and in the target-cue renditions of Exp. 3, the amount of interference in the between-hemisphere condition was greater than that in the within-hemisphere condition. These findings are consistent with what we have previously reported (Sohn et al., 1996, Sohn & Lee, 2003). However, when the distractor was precued in Exp. 3, the amount of interference did not differ between the two marching conditions. These results suggest that between-hemisphere separation of target and distractor can be more effective for reducing response interference than interhemispheric communication. It implies a possible role of an interhemispheric shielding mechanism (Merola & Liederman, 1985) to prevent the transfer of task-irrelevant, harmful information across the hemispheres.

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Studies of separation and quantitation for selenium species in food (식품중의 셀레늄 화학종의 분리 및 정량연구)

  • Jang, Hee-Young;Min, Hyungsik;Lee, Jonghae;Pak, Yong-Nam
    • Analytical Science and Technology
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    • v.26 no.3
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    • pp.182-189
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    • 2013
  • The purpose of this research is to separate and quantitate selenium species in some food samples with HPLC-ICP-MS. Cation exchange chromatography showed efficient separation only for inorganic Se species while reversed phase ion pair chromatography showed good separation for both inorganic and organic Se species. $C_8$ column ($Symmetryshield^{TM}\;RP_8$, 3.5 ${\mu}m$, $4.6{\times}150$ mm) was used with optimum condition of 5% methanol mobile phase, 0.05% of nonafluorovaleric acid ion pairing reagent. Five standard Se species of Se(IV), Se(VI), SeCys(selenocystein), SeMet(selenomethionine) and Se-M-C(seleno methyl cystein) were separated successfully under the optimum condition (mobile phase; 5% methanol, ion-pairing reagent; 0.05% nonafluorovaleric acid, flow rate; 0.9 mL $min^{-1}$). To extract Se species, microwave assisted and enzyme-assisted extraction methods were studied. In enzyme-assisted extraction method, protease I for garlic, protease I plus trypsin for pork and mackerel, and protease XIV for tuna showed the best extraction efficiency. With the optimum condition for each sample, it was found that mostly inorganic Se, SeCys and SeMet are present in the sample studied ranging from few ${\mu}g$ $g^{-1}$ to few tens of ${\mu}g$ $g^{-1}$.

Structural Static Test of Pylon for External Attachment Separation Load (외부장착물 분리하중에 대한 파일런 구조 정적시험)

  • Kim, Hyun-gi;Kim, Sungchan;Hong, Seung-ho;Choi, Hyun-kyung;Cho, Sang-hwan;Park, Hyung-bae
    • Journal of Aerospace System Engineering
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    • v.16 no.1
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    • pp.104-109
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    • 2022
  • The bomb rack unit (BRU) installed inside the pylon serves to fix external attachments such as external fuel tank or external weapon, and also serves to separate external attachments in case of emergency. In particular, the load generated when the external attachment is separated from the BRU is called the punching load. In this study, we present the results of a structural static test performed to verify the structural integrity of the pylon under the BRU punching condition acting on it. In the structural static test report, we present the implementation method for the separation load of the external attachment and the test profile for the BRU punching load condition, and compared the error between the load input signal and the feed-back signal to determine the appropriateness of load control in each test. Furthermore, we compared the strain results obtained in the numerical analysis and structural test at the main positions of the specimen. As a result, it was shown that the load of the actuators were properly controlled within the allowable error range in each test, and the numerical analysis effectively predicted the test result. Finally, through structural static tests conducted by design limit load and design ultimate load, we verified that the aircraft pylon dealt with in this study has sufficient structural strength for external attachment separation condition.