• Title/Summary/Keyword: Separation condition

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Separation Device Development and Flight Test for Marine Recovery of Scientific Balloon (과학기구 기낭의 해상 회수를 위한 분리장치 개발 및 비행시험)

  • Shim, Gyujin;Kang, Jungpyo;Kim, Hweeho;Yee, Kwanjung
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.47 no.1
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    • pp.49-58
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    • 2019
  • The Scientific balloon is a flight system that could recover an entire platform at the end of the mission. The recovery takes place mainly in low-density populated areas, taking into account for the possible damage to the human life and public safety. In Republic of Korea, on the other hand, marine recovery should be considered due to the dense mountainous terrain and restrictions of the peninsula. In this operating environment, the envelope must be recovered because of severe marine pollution that may occur after the splashdown. Therefore, in this study, the separation device that consists of a location tracker and the waterproof system were developed. The device includes data transmission/reception, separation, and waterproof systems which are manufactured considering the environmental condition of the Korea. The performance of the device and the trajectory of the envelope were verified by conducting a separation test of a 20km platform at a target altitude and the recovery of the zero-pressure balloon.

A Study of Cadmium Recovery from LCC Crucible Using Solid-liquid Separation Method (고-액 분리법을 이용한 LCC 도가니에서의 카드뮴 회수에 관한 연구)

  • Park, Dae-Yeob;Kim, Tack-Jin;Kim, Jiyong;Kim, Kyung-Ryang;Kim, Si-Hyung;Shim, Joon-Bo;Peak, Seungwoo;Ahn, Do-Hee
    • Journal of Advanced Engineering and Technology
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    • v.4 no.4
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    • pp.431-436
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    • 2011
  • This study was carried out to reduce the problem during distillation process, which separate U, TRU (TRans Uranium) metal electro deposit, Cd and LiCl-KCl eutectic salt generating from LCC (Liquid Cadmium Cathode) electro winning process. The cadmium recovering apparatus was manufactured to separate for each metal using solid-liquid separation method. The apparatus consists of the first sieve for the separation of U and TRU metal electrodeposit, the second sieve for the separation of LiCl-KCl eutectic salt, cadmium collection basket, and a heating furnace. In addition, the size of each sieve is 2 mm to 3 mm. In this experiment, a metal wire was employed to replace TRU metal electrodeposit and U, which exist actually in a LCC crucible. In the solid state, The LiCl-KCl is separated at 340℃ at which the solid and the liquid of the remaining cadmium and LiCl-KCl eutectic salt coexists in each, after the metal wire separated at 500℃. As a result, it seems that it would be beneficial to set the processing condition in the distillation process with the additional treatment process of cadmium and LiCl-KCl eutectic salt.

Effect of acid or base additive in the mobile phase on enantiomer separation of amino alcohols using polysaccharide derived chiral columns (다당유도체를 기초로 한 키랄 컬럼에서 이동상에서의 산 또는 염기 첨가제가 아미노 알코올의 광학분리에 미치는 영향)

  • Huang, Hu;Jin, Jing Yu;Lee, Wonjae
    • Analytical Science and Technology
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    • v.22 no.4
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    • pp.313-318
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    • 2009
  • Liquid chromatographic enantiomer separation of amino alcohols was performed on several chiral columns based on polysaccharide derivatives under the mobile phase conditions containing acid or base additive. The chromatographic parameters were greatly influenced by the nature of the mobile phase containing acid or base additive as well as the used chiral columns. Compared to chromatographic results obtained in the mobile phase containing base additive (0.1% triethylamine), especially, Chiralcel OD showed dramatically enhanced separation factors and resolution factors with reduced capacity factors under the mobile phase condition containing acidic additive (0.1% trifluoroacetic acid). When the mobile phase containing 0.05% trifluoroacetic acid and 0.05% triethylamine was used on Chiralcel OD, the greatest separation factors and resolution factors among all other mobile phase conditions in this study were observed.

A Study on the Separation of Electrolyte from Amino Acid Solution through Electrodialysis (전기투석법을 이용한 아미노산으로부터 전해질 분리정제에 관한 연구)

  • 김석곤;한정우;김한성;전경용;조영일
    • Membrane Journal
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    • v.4 no.3
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    • pp.163-170
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    • 1994
  • The separation of inorganic salt from amino acid solution using was performed electrodialysis. In order to review the availability of electrodialysis using isoelectric point of amino acid as a bio-separation technique, electrodialysis stacks were designed using ion exchange membrane. Separation of NaCl from amino acid solution was performed in the condition similar to amino acid fermentation process. To obtain otimum conditions of separation, leakage of amino acid depending of pH and limiting current density were measured. On the basis of optimum condition, removal of NaCl and leakage of amino acid were investigated quantitatively in batch and continuous process, and current efficiencies were also obtained. As a result of batch experiment for 11 hours each amino acid solution, removal efficiencies of NaCl were in the ranges of 96.1~96.2%. Amino acid leakage rate of glycine, methionine, alanine were 2.5, 1.7, 2.0% respectively. Current efficiencies were in the ranges of 44.5~44.6%. As a result of continuous experiment in various flow rate of each amino acid solution, it took 120 ~ 150 min to reach to steady state. Removal efficiency of NaCl was increased as the flow rate was decreased, but current efficiency was decreased. At the steady states, there were no leakage of amino acid.

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Elderly Women's Adaptation Process on Separation by Death in Rural Areas (농촌여성노인의 배우자 사별 적응과정)

  • Jang, hee Sun;Kim, Yun Jeong
    • 한국노년학
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    • v.31 no.4
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    • pp.939-967
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    • 2011
  • This study observed elderly women's adaptation process on separation by death in rural areas through grounded theory approach and developed its entity theory. Participants for this study were 14 elderly women who have lost their husbands in the last 12 months. The study was conducted for 8 months starting January 2010. Each interview per session took 40 to 90 minutes, study notes were taken on site, and recorded contents were transcribed by the researcher which was myself. The research data were collected by in-depth interview and with help of local community's nurses who were in charge of taking care of the participants. The collected data were analyzed by applying Strauss & Corbin's grounded theory (1998). As a result of study, 80 concepts, 28 subcategories, and 12 categories were deducted during open coding process. Adaptation process on separation by death was process of 'finding a way to live alone' which used strategy of 'attempting a make changes in life', and 'embracing the situation' which were influenced by conciliatory conditions of 'degree on economic condition', 'change in health', and 'supporting system' which focuses on phenomenon of 'bearing life alone' which is influenced by context condition of 'marital chemistry of couples during lifetime', and 'the couple's leadership during lifetime' together with casual conditions of 'the fall of wall'. The adaptation process accordance to time flow were divided into 4 steps which were step of 'shock and release of emotions', step of 'longing and resentment', step of 'resignation and acceptance', and step of 'life's restructure'. Above results suggest right directions for welfare for the aged and process of 'finding a way to live alone' for participants by controlling several factors and using intervention strategy, and provided basic data required for developing and applying practical welfare mediation.

Development of a Simulation Model for Separation Analysis and Design of Star Screen in Construction Wastes Recycling (건설폐기물 선별 해석을 위한 치차형 스크린 해석모델 개발)

  • Kim, Kwang-Hoon;Park, Jung-Hong;Moon, Byung-Young;Park, Yong-Ki
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.22 no.4
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    • pp.213-218
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    • 2010
  • In this study, a star screen model was constructed to predict the dynamic characteristics of interactive waste particles and to simulate separation capability of the particle using geared type screen(star screen). In order to approach this model, it is necessary to determine the design parameters of the screen such as driving torque, percentage of open space, and capability. Thus, a dynamic star screen model was developed with a total of 32 columns of geared assembly including screen part, wastes guide, and extra joints to rotate the screen using ADAMS. Each parameter was simulated to predict the screening capability for particle size, rotating speed, and particle condition. From the results, separation ability was predicted according to the affecting variables by using the dynamic star screen model.

A Method for the Separation of Mouse Pancreatic Islets Using Discontinuous Percoll Gradient Centrifugation

  • Cho, Yu-Ree;Kim, Sang-Duk;Chang, Hyo-Ihl;Sung, Ha-Chin;Lee, Cherl-Ho;Kim, Chan-Wha
    • Journal of Microbiology and Biotechnology
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    • v.9 no.4
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    • pp.522-524
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    • 1999
  • A discontinuous Percoll gradient was used to separate islets from the collagenase-treated mouse pancreas easily and rapidly. Since the osmolality of Percoll is very low, adjustment of its osmolality to 340 mOs/kg $H_2$O was essential for securing the optimal separation. A discontinuous gradient layering with Percoll solution of 1.09 g, 1.07g, and1.05g/m, respectively, when centrifuged at 800$\times$g for 10 min, resulted in an optimal condition for separation and yielded a banding pattern with an even distribution of islet cells. No significant difference was observed in the morphological features between the Percoll-isolated and the manually-isolated islets. In conclusion, the discontinuous Percoll gradient can be effectively used to isolate the pancreatic islets from mice with four-fold higher efficiency compared to the handpicking method.

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Effects of Column Length and Particle Diameter on Phospholipid Analysis by Nanoflow Liquid Chromatography-Electrospray Ionization-Mass Spectrometry

  • Lee, Ju-Yong;Lim, Sang-Soo;Moon, Myeong-Hee
    • Mass Spectrometry Letters
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    • v.2 no.3
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    • pp.65-68
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    • 2011
  • The effects of column length and particle size on the efficiency of separation and characterization of phospholipids (PLs) are investigated using nanoflow liquid chromatography-electrospray ionization-tandem mass spectrometry (nLC-ESI-MS-MS). Since PLs are associated with cell proliferation, apoptosis, and signal transduction, it is of increasing interests in lipidomics to establish reliable analytical methods for the qualitative and quantitative profiling of PLs related to biomarker development in adult diseases. Due to the complexity of PLs, the preliminary separation of PLs is necessary prior to MS analysis. In this study, length of capillary column and the particle size of reversed phase ($C_{18}$) packing materials are varied to find a reliable condition for the high speed and high resolution separation using 8 PL standard mixtures. From experiments, it was found that a capillary column of nLC-ESI-MS-MS analysis for PL mixtures can be minimized to a 5 cm long pulled tip column packed with 3 ${\mu}m$ $C_{18}$ particles without losing resolution.

Solvent Extraction Separation of Co, Mn and Zn from leaching solution from Ni-Cd battery by Na-PC88A

  • Ahn Jong-Gwan;Park Kyoung-Ho;Sohn Jeong-Soo;Kim Dong-Jin;Lee Jaereyeong;Jeong HunSaeong
    • 한국지구물리탐사학회:학술대회논문집
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    • 2003.11a
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    • pp.618-623
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    • 2003
  • Solvent extraction experiments for separation of impurities from Ni-rich solution were carried out for manufacturing of high purity Ni compounds from acid leaching solution of spent Ni-Cd secondary battery. Artificial and leaching solutions were used as aqueous phases and PC88A saponified by sodium in kerosene were used as organic phase. The extraction order is Zn>Mn>Co>Ni and extraction percentage of metal ions was increased with increase of the concentration of extractant, initial pH of aqueous phase and ratio of O/A. The separation of cobalt, zinc and manganese from nickel was effectively accomplished at the condition of extraction stage=l, O/A=1 and initial pH 5.0 with 1.0 $mol/dm^3$ PC88A saponified to $50\%$ with NaOH.

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Spatial flow structure around a smooth circular cylinder in the critical Reynolds number regime under cross-flow condition

  • Raeesi, Arash;Cheng, Shaohong;Ting, David S.K.
    • Wind and Structures
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    • v.11 no.3
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    • pp.221-240
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    • 2008
  • The spanwise flow structure around a rigid smooth circular cylinder model in cross-flow has been investigated based on the experimental data obtained from a series of wind tunnel tests. Surface pressures were collected at five spanwise locations along the cylinder over a Reynolds number range of $1.14{\times}15^5$ to $5.85{\times}10^5$, which covered sub-critical, single-bubble and two-bubble regimes in the critical range. Separation angles were deduced from curve fitted to the surface pressure data. In addition, spanwise correlations and power spectra analyses were employed to study the spatial structure of flow. Results at different spanwise locations show that the transition into single-bubble and two-bubble regimes could occur at marginally different Reynolds numbers which expresses the presence of overlap regions in between the single-bubble regime and its former and later regimes. This indicates the existence of three-dimensional flow around the circular cylinder in cross-flow, which is also supported by the observed cell-like surface pressure patterns. Relatively strong spanwise correlation of the flow characteristics is observed before each transition within the critical regime, or formation of first and second separation-bubbles. It is also noted that these organized flow structures might lead to greater overall aerodynamic forces on a circular cylinder in cross-flow within the critical Reynolds number regime.