• 한국정보전자통신기술학회논문지
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• 제12권2호
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• pp.142-149
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• 2019

전기자동차를 무선으로 충전하기 위하여서는 전기에너지를 전송하기 위한 코일이 꼭 필요하다. 코일의 형태는 기본적인 원형 코일에서부터 두 코일 간의 커플링 효과를 높이기 위한 DD 형상의 코일 등 여러 종류가 있다. 하지만 코일 간 커플링이 좋은 DD 형상의 코일은 송수신 측 전력변환장치의 구조가 복잡해지는 단점이 있어 사용에 제한이 있다. 본 논문에서는 자유공간에서 2개의 코일을 이용하여 무선으로 전력을 전송할 때 제작이 편리한 스파이럴 인덕터의 인덕턴스 값을 계산하고 적절한 크기의 인턱터를 설계하는 방법을 제시하였다. 공진기에서 XLm 값이 부하저항 값과 비슷하여질 때 bifurcation 현상이 나타나므로, 이 현상이 덜 일어나도록 XLm 값을 최소부하저항 값과 같도록 선택하여 공진기에 필요한 인덕턴스 값을 계산하였다. 계산된 인덕턴스 값을 스파이럴 인덕터로 구현하기 위하여 스파이럴 인덕터에서 인덕턴스 값과 인턱터의 크기, 턴 수, 총 코일 길이와의 관계를 알아보았다. 또한, 두 개의 코일의 수평 이격에 따른 결합계수 k 값의 변화를 알아본 후 적절한 인덕터를 선정하였다.

• 한국동물위생학회지
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• 제43권4호
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• pp.261-265
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• 2020

Each commercial cyromazine insecticide has different HPLC conditions. The aim of this study was to establish a standardized chromatographic method for the determination of cyromazine in commercial insecticides. The separation was achieved on two C18 columns - Waters® Bondapak C (4×300 nm i.d., 10 ㎛) and X bridge (4.6×250 nm i.d., 5 ㎛) using a mobile phase composed of water/methanol/ethanolamine (76:24:0.1, v/v), with UV detection at wavelengths 230 nm and 254 nm. A total of six commercial cyromazine insecticides were analyzed. In this study, the optimal high-performance liquid chromatography conditions for the analysis of cyromazine were as follows: a mobile phase of water/methanol/ethanolamine (76:24:0.1, v/v) at a flow rate of 1.0 mL/min and a detection wavelength of 230 nm using a X bridge C18 column (4.6×250 nm i.d., 5 ㎛) at a column temperature of 25℃. The calibration curve was linear in the concentration range of 5~50 ㎍/mL, with a correlation coefficient of 0.99995. The cyromazine detection limit was 0.2 ㎍/mL, and the limit of quantification was 0.59 ㎍/mL. The percentage recovery ranged from 99.8% to 101.0% for cyromazine, and the relative standard deviation was not over 2.0%. The cyromazine concentration ranged from 92.7% to 109.4% and was within the acceptable range (90~120%) for the percent of the labeled amount. This method was found to be suitable for determining cyromazine in commercial insecticides.

• 한국해안·해양공학회논문집
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• 제32권6호
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• pp.420-433
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• 2020

기존 케이슨방파제의 안정성을 높이기 위해 케이슨 전면 또는 후면에 추가로 신규 케이슨을 설치하여 보강하는 경우 박리에 의한 에너지 손실효과와 케이슨과 케이슨 사이의 공극률 변화에 따른 개별 원형케이슨에 작용하는 파력 및 파처오름 특성 평가는 중요하다. 본 연구에서는 고유함수전개법에 투과성판에서의 속도는 판 전후의 압력차에 선형적으로 비례한다는 Darcy의 법칙을 이용하여 원형케이슨들간의 공극률 계수 변화에 따른 2열 배치된 원형방파제에 작용하는 파랑 특성을 분석하였다. 수치해석의 신뢰성을 확보하기 위해 Sankarbabu et al.(2008)의 수치 해석결과와 비교를 수행하였으며, 다양한 변수에 따른 개별 이중 원형케이슨에 작용하는 파력 및 파처오름 특성을 나타내었다.

• Natural Product Sciences
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• 제27권1호
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• pp.54-59
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• 2021

Bergenia ciliata (Family: Saxifragaceae) is a folklore remedy for the treatment of various ailments in Asian countries. Bergenin (1) has been isolated as an active constituent in many studies, however, the amount of bergenin has not been determined in all parts of the plant. A simple RP-HPLC method was developed to determine the amount of bergenin in methanol extracts of leaves, rhizomes and roots of the plant. Separation was achieved on an Agilent Eclipse XDB-C18 column maintained at 25 ℃ using isocratic solvent system (water: methanol: acetic acid; 62.5:37:0.5 v/v/v) adjusted at pH 2 0 at a flow rate of 1.0 mL/min. and detected at 275 nm. Correlation coefficient (0.9952) showed linearity of concentration (5-200 ㎍/mL) and response. The values of LOD (0.00947 ㎍/mL) and LOQ (0.02869 ㎍/mL) indicated that method was sensitive. The recovery of bergenin was 99.99-100% indicating accuracy of method. The methanol extract of rhizomes contained higher amount of bergenin (19.4%) than roots (9.2%) and leaves (6.9%). It is concluded that methanol extract of rhizomes is a better source of bergenin than other parts of the plant. The findings are useful for standardization of bergenin containing extracts and herbal preparations.

• 한국지반환경공학회 논문집
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• 제23권5호
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• pp.15-24
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• 2022

준설 매립지반의 경우 공학적, 물리적 조건이 열악하여 매립현장에서 이를 개량하기 위한 시간과 비용이 많이 든다. 또한 국내 실정에 적합한 관중혼합 이송처리 공법의 적용사례가 없고 공법 적용성 및 효과에 관하여 불확실할 뿐 아니라 실제 현장과 실내실험 간의 차이가 발생할 수 있다. 이러한 문제점을 해결하기 위해 개질재(표준사+입도조절재)가 혼합된 준설토를 대상으로 실내 특성실험을 통해 개질재의 적정한 입도분포 및 함수비 범위를 결정하였다. 그 결과 단계투기 시 침강압밀계수가 증가하고 분리침강에 대한 개선효과가 있는 것으로 확인되었다. 실험결과 회귀분석을 통해 개질 처리토의 함수비에 따른 비배수전단강도를 도출하고, 이를 활용하여 배합비를 결정할 수 있는 상관식을 제시하였다.

• Journal of Astronomy and Space Sciences
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• 제39권2호
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• pp.43-50
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• 2022

The unified scheme of Seyfert galaxies hypothesizes that the observed differences between the two categories of Seyfert galaxies, type 1 (Sy1) and type 2 (Sy2) are merely due to the difference in the orientation of the toroidal shape of the obscuring material in the active galactic nuclei. We used in this paper, a sample consisting of 120 Seyfert galaxies at 1.40 × 10⁹ Hz in radio, 2.52 × 10¹⁷ Hz in X-ray and 2.52 × 10²³ Hz in γ-ray luminosities observed by the Fermi Large Area Telescope (Fermi-LAT) in order to test the unified scheme of radio-quiet Seyfert galaxies. Our main results are as follows: (i) We found that the distributions of multiwave luminosities (L_radio, L_X-ray, and L_γ-ray) of Sy1 and Sy2 are completely overlapped with up to a factor of 4. The principal component analysis result reveals that Sy1 and Sy2 also occupy the same parameter spaces, which agrees with the notion that Sy1 and Sy2 are the same class objects. A Kolmogorov-Smirnov test performed on the sub-samples indicates that the null hypothesis (both are from the same population) cannot be rejected with chance probability p ~ 0 and separation distance K = 0.013. This result supports the fact that there is no statistical difference between the properties of Sy1 and Sy2 (ii) We found that the coefficient of the best-fit linear regression equation between the common properties of Sy1 and Sy2 is significant (r > 0.50) which plausibly implies that Sy1 and Sy2 are the same type of objects observed at different viewing angle.

• 한국결정성장학회지
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• 제31권6호
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• pp.233-239
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• 2021

본 연구에서는 산화갈륨의 방열 특성 향상을 위해 산화갈륨/다이아몬드 이종 박막 성장을 진행하였다. 먼저, 핫필라멘트 화학기상증착법을 이용하여 다결정 다이아몬드를 증착시킨 후, 미스트 화학기상증착법을 통해 450~600℃ 사이의 온도구간에서 산화갈륨 박막을 성장시켰다. 열처리 전후 비교를 통해 500℃에서 산화갈륨/다이아몬드 계면 분리 현상이 발생함을 확인하였다. 이는 비정질과 결정질이 혼재된 산화갈륨 박막이 성장된 후, 냉각 과정에서 열팽창계수의 차이로 인해 계면이 분리된 것으로 판단하였다. 따라서, 본 연구를 통한 산화갈륨/다이아몬드 계면의 물리적 안정성을 통해 산화갈륨의 열물성 보완및 고전력 반도체로의 활용이 기대된다.

• 한국동물위생학회지
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• 제45권3호
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• pp.243-248
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• 2022

The HPLC conditions for analysis of ivermectin in solutions dosage forms of commercial anthelmintics are different for each product. The purpose of this study was to establish a standardized chromatographic method for the quantification of ivermectin in solution. The separation was achieved on Waters Xbridge C18 column (4.6×150 nm, 5 ㎛) using different kinds of mobile phase composed of water/methanol/acetonitrile (15/34/51, v/v and 19.5/27.5/53, v/v), with UV detection at wavelengths 245 nm and 254 nm. A total of five commercial ivermectin in solution samples were analyzed. In this study, the optimal chromatographic conditions for analysis of ivermectin in solution were mobile phase of water/methanol/acetonitrile (15/34/51, v/v) at a flow rate of 1.0 mL/min and a detection wavelength of 245 nm using a Waters Xbridge C18 column (4.6×250 nm, 5 ㎛) at a column temperature of 25℃. The linearity was observed in the concentration range of 50~150 ㎍/mL, with a correlation coefficient, r²= 0.99999. The limit of detection and the limit of quantification were 0.88 and 2.68 ㎍/mL, respectively. The accuracy (% recovery) was found to be 98.9 to 100.3%. Intra-day and Intermediate precisions with relative standard deviations were less than 1.0%. The content of ivermectin for five market samples ranged 91.2~102.7%. The proposed method was also found to be robust, therefore, the method can be used for the routine analysis of ivermectin in solutions dosage forms.

• 한국해안·해양공학회논문집
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• 제34권1호
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• pp.11-18
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• 2022

본 연구는 대한해협 인근 입자추적 예측 기법의 정확도 개선을 위해서 해수유동 수치모델 결과를 이용하여 만든 입자추적 모델과 현장 관측 자료를 이용한 기계학습 기반 입자 추적 모델을 비교 및 분석하였다. 세부 연구 방법으로는 대한해협에서 관측된 표층 뜰개 이동 궤적 자료, 3개 관측소(가거도, 거제도, 교본초 관측소)의 조위 및 바람자료를 학습시켜 만든 기계 학습(선형 회귀, 의사결정나무) 기반 예측자료, 수치모델 예측자료(ROMS, MOHID)를 3가지 오차평가방법(CC, RMSE, NCLS)을 통해 비교하였다. 최종 결과로서 CC와 RMSE에서는 의사결정나무 모델의 예측 정확도가 가장 우수하였고 NCLS에서는 MOHID 모델의 예측 결과가 가장 우수하였다.

• Journal of Electrochemical Science and Technology
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• 제14권1호
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• pp.75-84
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• 2023

The accumulation of spent carbide (YG8), not only pollutes the environment but also causes waste of tungsten, cobalt and other rare metal resources. To better address this issue, we proposed a combined electrochemical separation process of low-temperature aqueous solution and high-temperature molten salt for tungsten and cobalt. H₂WO₄ was obtained from spent carbide in an aqueous solution, and we calcined it to obtain WO₃, which was used as a raw material to obtain tungsten by using molten salt electrodeposition. The influence of the current efficiency and the electrochemical behavior of the discharge precipitation of W(VI) were also studied. The calcination results showed that the morphology of WO₃ was regular and there were no other impurities. The maximum current efficiency of 82.91% was achieved in a series of electrodeposition experiments. According to XRD and SEM analysis, the recovered product was high purity tungsten, which belongs to the simple cubic crystal system. In the W(VI) reduction mechanism experiments, the electrochemical process of W(VI) in NaCl-Na₂WO₄-WO₃ molten salt was investigated using linear scanning voltammetry (LSV) and chronoamperometry in a three-electrode system. The LSV showed that W(VI) was reduced at the cathode in two steps and the electrode reaction was controlled by diffusion. The fitting results of chronoamperometry showed that the nucleation mechanism of W(VI) was an instantaneous nucleation mode, and the diffusion coefficient was 7.379×10^-10 cm²·s^-1.