• Title/Summary/Keyword: Separate of particles

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Antioxidation Behavior of Submicron-sized Cu Particles with Ag Coating (서브 마이크론급 구리 입자의 은도금 공정에 따른 내산화성 강화 연구)

  • Choi, Eun Byeol;Lee, Jong-Hyun
    • Journal of the Microelectronics and Packaging Society
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    • v.23 no.3
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    • pp.51-56
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    • 2016
  • To fabricate a copper (Cu)-based fine conductive filler having antioxidation property, submicron silver (Ag)-coated Cu particles were fabricated and their antioxidation property was evaluated. After synthesizing the Cu particles of $0.705{\mu}m$ in average diameter by a wet-reduction process, Ag-coated Cu particles were fabricated by successive Ag plating using ethylene grycol solvent. Main process parameters in the Ag plating were the concentration of reductant (ascorbic acid), the injection rate of Ag precursor solution, and the stirring rate in mixed solution. Thus, Ag plating characteristics and the formation of separate fine pure Ag phase were observed with different combinations of process parameters. As a result, formation of the separate pure Ag phase and aggregation between Ag-coated Cu particles could be suppressed by optimization of the process parameters. The Ag-coated Cu particles which were fabricated using optimal conditions showed slight aggregation, but excellent antioxidation property. For example, the particles indicated the weight gain not exceeding 0.1% until $225^{\circ}C$ when they were heated in air at the rate of $10^{\circ}C/min$ and no weight gain until 75 min when they were heated in air at $150^{\circ}C$.

Study on the Effect of Design Parameters of the Vane Type Inertial Separator Using Commercial CFD Code (상용 CFD 프로그램을 사용한 베인형 관성분리기의 설계인자 영향 검토)

  • Lee, Dap-Yeon;Lew, Jae-Moon
    • Journal of the Society of Naval Architects of Korea
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    • v.54 no.6
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    • pp.470-475
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    • 2017
  • Since the intake air of gas turbine engine of marine purpose contains water particles, inertial separator for separating the air and water particles are provided. Saw type and wave type separator are now used to separate inflow water particle from the gas. In this paper, the design parameters of saw type separator are studied by numerical simulations. Using the commercial CFD program, Star-CCM+, Lagrangian-Eulerian method was used to perform the analysis of two phase flow of the mist in the air. This method solves Reynolds-Averaged Navier-Stokes equations in Eulerian framework for the continuous phase, while solves equation of motion for individual particles in Lagrangian framework. Lagrangian multiphase method was applied to monitor the particles of different sizes and shapes and to verify collision between particles by chasing particles. Water particles were injected through injectors located at the inlet of the separator and escape mode was used which assumes that the particles attached on the surface of inertial separator were removed from the simulation, effectively escaping the solution domain. Through the numerical computations with the inlet condition of constant water particle size in the wetness fraction of 85%, efficiency of eliminating the water particle and the pressure drop between the inlet and outlet were examined.

Dissolved Organic Matter (DOM) Leaching from Microplastics under UV-Irradiation and Its Fluorescence P roperties: Comparison with Natural P articles (UV 광풍화에 의한 미세플라스틱 기원 유기물 용출과 형광 특성: 자연유래 유기성 입자와의 비교)

  • Choi, Na Eun;Lee, Yun Kyung;Hur, Jin
    • Journal of Korean Society on Water Environment
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    • v.38 no.2
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    • pp.72-81
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    • 2022
  • Numerous studies have investigated the occurrence and fate of microplastics in the environment; however, only limited effort has been devoted to exploring the characteristics of dissolved organic matter (DOM) leached from microplastics. In microplastic (MP)-contaminated environment, MPs are typically mixed with naturally-occurring particles, which interferes with their detection in the environment. Thus, it is necessary to distinguish between the DOM leached from MPs and those leached from natural particles and also to characterize their properties. This study investigated DOM leaching behavior from MPs (polystyrene: PS, polyvinylchloride: PVC) and natural particulates (forest soil: FS, litter leaves: LL) under light, which is considered one of the main weathering processes that affect MPs in the environment. The leached DOM concentrations and fluorescence characteristics were compared under dark versus light conditions. Regardless of the origins, UV light promoted DOM release from all the particulates. More DOM was released from natural particles than from MPs under both conditions. However, the effect of promoting DOM release by UV was more pronounced for MPs than for natural particles. It was observed from fluorescence spectra that the intensity of the humic-like region was substantially reduced when MP-derived DOM was exposed to UV light, whereas the change of intensity was very little for natural particles. Under light conditions, the ratio of protein-like to humic-like fluorescence of MP-derived DOM was higher than that of DOM from natural particles. This study implies that a substantial amount of DOM could be leached from MPs even in MP-polluted environment under UV irradiation. Protein/humic fluorescence ratio could be utilized as a fast probing indicator to separate the two sources of particles under light.

Suggestion of separation and recollection method of nano particles from suspension by using ultrasonic atomization (초음파 무화효과를 이용한 현탁액으로부터 나노입자의 분리포집법 제안)

  • Kim, Jihyang;Kim, Jungsoon;Yeom, Jiyeong;Ha, Kanglyeol;Kim, Moojoon
    • The Journal of the Acoustical Society of Korea
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    • v.35 no.6
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    • pp.445-451
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    • 2016
  • It is very important to obtain non-agglomerated nano particle state for practical application of nano technology. In order to improve the functionality of products using nano particles, more precise control of particle size distribution is required in their synthesis process. However, synthesized nano particles are agglomerated easily due to physical and chemical reasons, and it then veils unique properties of the nano particles and causes some troubles in their practical application. In this study, a separation method for nano particles from suspension by using the droplets as the separation space was proposed. Using the suspension of 0.002 wt. % with $TiO_2$ powder, the particle size distribution of nano particles in the recollected suspension was measured. From the results, it was confirmed that it is possible to separate and to recollect the nano particles monodispersed by using the suggested method.

Characterization of Wear Resistance of Particle Reinforced Al Matrix Composite Manufactured by Centrifugal Spray Casting (분사주조한 Al기지 입자강화 복합재료의 마모특성)

  • Bae, Cha-Hurn;Choi, Hak-Kyu;Bang, Kuk-Soo
    • Journal of Korea Foundry Society
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    • v.24 no.2
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    • pp.108-114
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    • 2004
  • $Al_2O_3$, SiC reinforced Al matrix composites were fabricated by centrifugal spray casting method and their wear resistance characteristics have been studied. Particles are generally uniformly distributed in the microstructure of as-cast specimens. In order to investigate the effect of secondary deformation, hot rolling was performed for each specimen of pure Al matrix composites with a reduction of 10, 20, 30, 40 and 50% at $400{\sim}500^{\circ}C$, respectively. Microstructure of specimen showed that particle distribution density and hardness increased because of increasing of reduction ratio. Wear test with a various sliding velocity of 1.98, 2.38, 2.88 and 3.53m/sec showed that the wear resistance characterization of composite improved remarkably compared to the normal alloy and performs without reinforced particles. Microstructural observation for the worn surface of pure Al specimens without particles showed that a change in wear mechanism seemed to separate layer by surface fatigue. In other case of Al composite reinforced with $Al_2O_3$ and SiC, the grinder type of wear mechanism was shown.

Design and Performance Evaluation of a Faraday Cage and an Aerosol Charger (패러데이 케이지와 에어로졸 하전기의 설계 및 성능평가)

  • Ji, Jun-Ho;Bae, Kwi-Nam;Hwang, Jung-Ho
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.28 no.3
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    • pp.315-323
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    • 2004
  • An electrical cascade impactor is a multi-stage impaction device to separate airborne particles into aerodynamic size classes using particle charging and electrical detection techniques. A Faraday cage and an aerosol charger, which are basic components of the electrical cascade impactor, were designed and evaluated in this study. The low-level current response of the Faraday cage was investigated with changing particle size and air flow rate by using sodium chloride (NaCl) particles. The response of the prototype Faraday cage was very similar to that of a commercial aerosol electrometer (TSI model 3068) within ${\pm}$5% for singly-charged particles. The response linearity of the prototype Faraday cage could be extended up to flow rate of 30 L/min. For the performance evaluation of the aerosol charger the monodisperse liquid dioctyl sebacate (DOS) particles, with diameters of 0.1∼0.8$\mu\textrm{m}$, were generated using spraying from an atomizer followed by evaporation-condensation process. Typical performance parameters of the aerosol charger such as P$.$n, wall loss, and elementary charges per particle were evaluated. The performance of the prototype aerosol charger was found to be close to that of the aerosol charger used in an electrical low pressure impactor (ELPI, Dekati).

The Reaction Efficiency and Surface Characteristics for Metallic Ions in Air Flotation Process (부상공정에서 금속이온의 기포 표면 전위 특성 및 반응효율)

  • Han, Moo-Young;Dockko, Seok;Kim, Young-Hwan
    • Journal of Korean Society of Water and Wastewater
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    • v.18 no.2
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    • pp.222-227
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    • 2004
  • Flotation processes involve the use of very small bubbles (micro-bubbles) to separate particles from water. The process has become a good alternative to sedimentation, especially where the particles are small or of low density. Although the flotation process commences with a collision between particles and bubbles, most research has been focused only on the characteristics of the particles. In this paper, recent theoretical and experimental research on the characteristics of bubbles is summarized. The effect on the collision efficiency of the size and charge of bubbles is calculated through trajectory analysis. The size and charge of bubbles are measured under different conditions and the ramifications of the results are discussed. The results may lead to a better understanding and optimization of the existing process. In particular, we discuss an idea that a new advanced flotation process might be possible by the modification of the characteristics of the bubble alone or of both bubble and particle.

Development of a Miniature Aerosol Separator for a Black Carbon Measuring Instrument (블랙카본 측정기용 초소형 사이클론 집진기 개발)

  • An, Ik-Hyun;Lim, Jun-Hyung;Lee, Hyo-Young;Yook, Se-Jin
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.19 no.12
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    • pp.42-48
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    • 2020
  • Given the increasing interest in air pollution, several technologies to measure black carbon (BC) aerosol particles have been developed. As most BC aerosol particles are smaller than 1 ㎛, it is necessary to pre-separate the particles by size before a BC measuring instrument samples the aerosol particles. In this study, a miniature cyclone separator for portable BC measuring instruments was developed. A numerical approach was used to design the miniature cyclone separator with operating flow rates of 50, 100, or 150 mLPM, and then a prototype cyclone separator was manufactured for experimental validation. The numerical results of the cut-off size and pressure drop of the miniature cyclone separator agreed well with the experimental data. The cut-off sizes of the miniature cyclone separator were determined to be 2.9, 0.94, and 0.63 ㎛ for operating flow rates of 50, 100, and 150 mLPM, respectively. Thus, the miniature cyclone separator is suitable for use as a sampling inlet for the portable black carbon measuring instrument to sample BC aerosol or PM2.5 aerosol.

Selective Separations Using Molecularly Imprinted Membranes (분자 각인 막의 선택적 분리)

  • Lee, Jeong-Woo;Park, Joong-Kon
    • KSBB Journal
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    • v.20 no.3
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    • pp.133-141
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    • 2005
  • This review presents the preparation, transport mechanism and application of molecularly imprinted membranes (MIM). Molecular imprinting has now been established as a technique which allows the creation of tailor-made binding sites for many classes of compounds. MIM have some advantages; a high capacity due to a large surface area, faster transport of substrate molecules and faster equilibrium of binding cavities compared to molecularly imprinted particles. MIM were prepared by covalent and non-covalent chemical bonding systems, by interactions between functional monomer and template. MIM can be prepared by in-situ polymerization, wet phase inversion, dry phase inversion, and surface imprinting method. MIM can continuously separate mixtures based on facilitated or retarded diffusion of the template. MIM can change their permeability in the presence of templates. MIM have a potential to be used to separate chiral compounds and materials with similar structures. However the application of MIM by the chemical industries is still in its infancy stages.

Flow Analysis of Cyclone-Cartridge Filter Gausing Collector (사이클론-카트리지필터 일체형 가우징 집진기의 유동해석)

  • Jang, Sung-Cheol;Jung, Dae-Young;Cho, Jung-Sick
    • Journal of the Korean Society of Industry Convergence
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    • v.21 no.3
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    • pp.133-139
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    • 2018
  • Precipitator is the most widespread device used to separate dust particles from the exhaust gas. In the shipyard, welding umbrellas, spark protection covers, and ventilators are not purchased and used for the work place to capture the flames and high temperature metal dust generated during the gardening process. In particular, a thorough analysis of design factors, such as capture rate, collection capacity calculation, filter speed, and materials selection, is required since spatial constraints are followed by structures, etc. In this study, conceived to address problems such as this cyclone and filtration filter system that combines all-in-one gausing collector prototype. Assessed through interpretation through the validity of the design and reliability.