• Proceedings of the Korean Institute of Building Construction Conference
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• 2015.05a
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• pp.15-16
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• 2015

In this research, the application of repair methods of water leakage cracks using self-healing technologies for subway tunnels is presented. In order to apply crack self-healing water stop agents and quick setting agents in subway tunnels, laboratory and field tests were performed based on various previous researches. Especially, this study focused on development of crack repair materials and their new repair methods. Therefore, various repair materials were examined for new repair materials with self-healing capability applied to crack sealing method and to patching repair method.

• Corrosion Science and Technology
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• v.8 no.6
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• pp.223-226
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• 2009

Polymer coatings are commonly applied to metal substrates to prevent corrosion in aggressive environments such as high humidity and under salt water. Once the polymer coating has been breached, for example due to cracking or scratches, it loses its effectiveness, and corrosion can rapidly propagate across the substrate. The self-healing system we will describe prevents corrosion by healing the damage through a healing reaction triggered by the actual damage event. This self-healing coating solution can be easily applied to most substrate materials, and our dual-capsule healing system provides a general approach to be compatible with most common polymer matrices. Specifically, we expect an excellent anti-corrosion property of the self-healing coatings in damaged parts coated on galvanized metal substrates.

• Journal of the Korean Recycled Construction Resources Institute
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• v.7 no.1
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• pp.29-36
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• 2019

This study investigated the self-healing properties of blast furnace slag cement paste sample with $Na_2SO_4$ as a blast furnace slag activator after conducting the permeability test. Self-healing properties were examined by crack filling ratio and quantification of self-healing products. The degree of self-healing was evaluated by the crack filling ratio, and the crack filling ratio was analyzed by panoramic analysis using BSE-DIP for objectivity. The average crack filling ratio showed a tendency of decreasing from the upper part of the specimen to the lower part as the average of the top part was 18%, the middle part was 7% and the bottom part was 5% on average. The maximum crack filling ratio was 44% and the minimum crack filling ratio was 3%. The residual self-healing product after the permeability test contained a large amount of Ca element and Al element derived from the blast furnace slag, and the Si element was mainly present near the crack surface. The most abundant minerals in self-healing products were about 68% C-A-H. $CaCO_3$ was about 13% and C-A-S-H was about 8%. Three minerals accounted for 90% of self-healing products. C-A-H was mainly present at a part slightly distant from the crack surface and showed an angular or acicular shape. The C-A-S-H was generated on the surface naturally connected to the existing specimen, and the $CaCO_3$ was generally observed on the surface of the specimen or the inside of the crack.

• Journal of the Korean Recycled Construction Resources Institute
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• v.6 no.4
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• pp.283-288
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• 2018

Since the crack self-healing materials are activated according to the exposure environmental conditions from the time of crack occurrence, it is very important to clarify the relationship between the healing performance and the exposure environmental conditions of the crack surface. In this paper, the influence of the exposure environmental conditions on the crack healing performance of self-healing repair mortar was investigated through the water permeability test. The influence of temperature and humidity on the crack width of cracked specimens was evaluated. As a result of measuring the change of the crack width, the effect of curing temperature was negligible but it was confirmed that crack-closing occurred due to the change of dry-wet condition. The healing materials produced on the crack surface of the specimens was identified as calcite minerals. Since the minerals with high density are precipitated under the influence of gravity, the healing performance is somewhat different according to the direction of the crack surface, and the healing performance was significantly improved in the wet exposure condition than the air exposure condition.

• Journal of the Korea institute for structural maintenance and inspection
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• v.25 no.2
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• pp.16-22
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• 2021

In this paper, a solid capsule was prepared using a crystal growth type inorganic material capable of hydration reaction. The solid capsules were mixed at 3, 5, and 10% according to the composition ratio of 8:2, 7:3, 6:4 based on the cement mass, and the self-healing mortar was mixed, Durable healing properties were evaluated through the water permeability test. As a result of the water level permeability test, the effect of optimally improving the natural healing performance was shown by mixing the solid capsules prepared in a composition ratio of 7:3 of the solid capsules. In the case of a crack width of 0.3mm or less, it is estimated that more than 90% of the self-healing performance can be secured. As a result, it was judged that the self-healing performance of the solid capsule had an effect on the durable healing properties through the water permeability test, It is judged that there is a tendency to improve self-healing performance according to the mixing of solid capsules.

• Journal of the Korean Recycled Construction Resources Institute
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• v.8 no.4
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• pp.475-482
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• 2020

In this study, three levels of solid capsules were prepared according to the composition ratio of core materials for the crystal growth type self-healing solid capsule, and a cement mortar was prepared with the crystal growth type self-healing solid capsule. The prepared solid capsule was mixed with 3% of the cement mass to evaluate the healing properties according to the crack induction age of the cement mortar. As a result of test, the crack healing properties according to the crack induction age of cement mortar mixed of solid capsules, it was confirmed that the self-healing performance of the cement mortar with the solid capsules was increased self-healing performance of 7 days than 28 days. This is because the unhydrated binder remains.

• Journal of the Korean Recycled Construction Resources Institute
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• v.6 no.4
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• pp.236-244
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• 2018

In this study, we tried to fabricate self - healing microcapsules using liquid inorganic materials which can be mixed directly with cement composites. The basic properties of the liquid inorganic material were evaluated and microencapsulation was performed. The focus of this paper is on the quality and manufacturing characteristics of cement composites rather than the healing effects of self - healing microcapsules according to mixed capsules. Test results, the self-healing microcapsules encapsulate liquid inorganic material which is stable at room temperature and has high crack followability, and the yield is over 90%. The size of self - healing microcapsule was able to change according to the synthetic agitation speed and it was able to secure more than 70% of target size. In addition, the loss of less than 10% was found to occur through the membrane strengthening of self - healing microcapsules, and it could be reduced by 50% compared with the case without membrane strengthening.

• Journal of Ceramic Processing Research
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• v.21 no.2
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• pp.200-207
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• 2020

The self-healing fiber-reinforced composite (abbreviation: shFRC) was made by adding SiC, a self-healing material, between an Al₂O₃ matrix and an Al₂O₃ continuous fiber. shFRC has the characteristic of healing the reduced strength by self-healing. The purpose of this study was to evaluate the damage and healing of new composite material, shFRC, and define new failure criteria. The test method used in this study was a high temperature creep test. The interface fracture behavior with time was investigated by analyzing the creep rate. The creep test conditions were 137 MPa and 150 MPa at 1,000 ℃, and 68.5 MPa, 100 MPa, and 137 MPa at 1,200 ℃, respectively. As a result, the crack propagation of 1,000 ℃ was stopped by healing, and the creep rate was zero. The crack healing part was higher than the strength before the crack formation. Due to the rapid hardening of the interface and the decrease in strength of the fiber, delayed fracture behavior was not observed at 1,200 ℃. If the crack is stopped by self-healing at a constant load, shFRC can use that load stress as the allowable stress. However, when the reaction rate of the interface is markedly rapid, crack propagation is difficult to control.

• Architectural research
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• v.25 no.3
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• pp.53-59
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• 2023

Concrete is widely used in the construction industry; however, it has the disadvantage of deteriorating durability due to cracks occurring because of climate change and shrinkage. In addition, when cement is used as a binder, CO₂ emitted during the manu-facturing process accounts for ~8% of global CO₂ emissions. In this study, ecofriendly cementitious materials such as blast furnace slag powder and fly ash (FA) were used as cement substitutes in the production of mortar containing a chitosan-based polymer (CP), and their fluidity, compressive strength, and self-healing performance were examined. The 28-day compressive strength of the control sample was ~32.4 MPa (the lowest for all tested samples), while that of the sample containing 5% CP and 20% FA was ~49.6 MPa (the highest for all tested samples) and ~53.1% higher than that of the control sample. Even at a healing age of 56 days, the control sample exhibited the lowest healing performance, whereas the samples containing CP (5%, 10%) and 20% FA demonstrated excellent healing performance. After 28 days, the decrease in crack size for the control sample was minimal; however, for the sample containing only cement and CP, a significant decrease in crack size was observed even after 28 days. This study confirmed that the appropriate use of CP and cementitious materials improves not only compressive strength but also the selfhealing performance of mortar.

• Journal of the Korean Recycled Construction Resources Institute
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• v.10 no.1
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• pp.92-100
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• 2022

In this paper, to evaluate the effect of SC on the crack self-healing performance and mechanical recovery performance of cement composites, encapsulated intumescent inorganic material-based solid healing materials were prepared. SC was mixed with cement composite materials to evaluate the basic properties, permeability test, and load reload test. SC slightly improved the flow of cement composites, and the compressive strength decreased by about 10 %. Also, the flexural strength decreased by about 30 %. It was found that when SC was mixed with the cement composite material by 5 %, the crack self-healing rate of Plain was improved by about 𝜟10 %. As a result of the load reload test, it was found that the mechanical recovery rate of Plain was improved by about 𝜟20 %. In addition, as a result of analyzing the correlation between the crack self-healing rate and the mechanical recovery rate by the load reload test, it is judged that the healing area of the Plain can be increased due to SC.