• Title/Summary/Keyword: Segregation effect

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Effect of the Alloying Elements in Ag-Cu-Zr-X Brazing Alloy on the Microstructure and the Bond Strength of $Al_2O_3$/Ni-Cr Steel Brazed Joint (알루미나/니켈크롬강 접합체의 미세조직 및 접합강도에 미치는 Ag-Cu-Zr-X 브레이징 합금성분의 영향)

  • Kim, Jong-Heon;Yoo, Yeon-Chul
    • Transactions of Materials Processing
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    • v.7 no.5
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    • pp.465-473
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    • 1998
  • The effect of alloying elements of Ag-Cu-Zr-X brazing alloy on the microstructure and the bond strength of $Al_2O_3/Ni-Cr$ brazed steel joint was investigated. The reaction layer, $ZrO_2$ (a=5.146 ${\AA}$ , b=5.213 ${\AA}$ , c=5.311 ${\AA}$ )was formed at the interface of $Al_2O_3/Ni-Cr$ steel joint by the redox reaction between alumina and Zr. The addition of An and Al to the Ag-Cu-Zr brazing alloy gave rise to changes in the thickness of the reaction product layer and the morphology of the brazement. Sn caused the segregation of Zr was decreased b Al the $ZrO_2$ layer formed at the Ag-Cu-Zr-Al alloy was thinner than that of $ZrO_2$ formed at the Ag-Cu-Zr-An alloy. The fracture shear strength was strongly dependent on the microstructure of the brazement. Brazing with Ag-Cu-Zr-Sn alloy resulted in a better bond strength than with Ag-Cu-Zr or Ag-Cu-Zr-Al alloy.

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Preparation of Bismuth Thin Films by RF Magnetron Sputtering and Study on Their Electrical Transport Properties (RF 마그네트론 스퍼터링을 이용한 Bismuth 박막의 제조와 그 전기적 특성 연구)

  • Kim Dong-Ho;Lee Gun-Hwan
    • Journal of the Korean institute of surface engineering
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    • v.38 no.1
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    • pp.7-13
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    • 2005
  • Bismuth thin films were prepared on glass substrate with RF magnetron sputtering and effects of substrate temperature on surface morphology and their electrical transport properties were investigated. Grain growth of bismuth after nucleation and the onset of coalescense of grains at 393 K were observed with field emission secondary electron microscopy. Continuous thin films could not be obtained above 473 K because of grain segregation and island formation. Hall effect measurements showed that substrate heating yields the decrease of carrier density and the increase of mobility. Resistivity of bismuth film has its minimum (about 0.7 x 10/sup -3/ Ωcm) in range of 403~433 K. Annealing of bismuth films deposited at room temperature was carried out in a radiation furnace with flowing hydrogen gas. The change of resistivity was not significant due to cancellation of the decrease of carrier density and the increase of mobility. The abrupt change of electrical properties of film annealed above 523 K was found to be caused by partial oxidation of bismuth layer in x-ray diffraction analysis.

Effect of Concrete Filling Conditions on Flexural Behavior of Beam Members (콘크리트 충전상태에 따른 보부재의 휨거동에 관한 연구)

  • 장일영;윤영수;노병철;박훈규
    • Journal of the Korea Concrete Institute
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    • v.12 no.2
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    • pp.3-11
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    • 2000
  • There is a possibility of poor-state concrete filling condition due to segregation and interlocking of aggregate and paste when a high performance concrete is used at reinforced concrete structure without compaction. This study was conducted to evaluate the flexural behavior of high performance concrete beams with design parameters such as c, t and different concrete filling conditions. Different concrete filling conditions were intentionally made such that the first type specimen was soundly cast to obtain the perfect concrete filling condition. Second type was cast in such a way that up to the longitudinal tensile reinforcement from the top, good concrete was filled while poor concrete was poured for the bottom part to simulate the poor strength, workability and unsatisfactory compaction. Third type was cast in such a was that up to the neutral axis of the beam section from the top, good concrete was filled while so did for the bottom part as the second type. The test results were analyzed in terms of load-displacement response, failure pattern, crack width and crack spacing. The test results indicate that have no effect of concrete filling conditions on the yielding strength of structures. But, have a grate influence on the stiffness and ductility of structures.

An OpenFlow User-Switch Remapping Approach for DDoS Defense

  • Wei, Qiang;Wu, Zehui;Ren, Kalei;Wang, Qingxian
    • KSII Transactions on Internet and Information Systems (TIIS)
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    • v.10 no.9
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    • pp.4529-4548
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    • 2016
  • DDoS attacks have had a devastating effect on the Internet, which can cause millions of dollars of damage within hours or even minutes. In this paper we propose a practical dynamic defense approach that overcomes the shortage of static defense mechanisms. Our approach employs a group of SDN-based proxy switches to relay data flow between users and servers. By substituting backup proxy switches for attacked ones and reassigning suspect users onto the new proxy switches, innocent users are isolated and saved from malicious attackers through a sequence of remapping process. In order to improve the speed of attacker segregation, we have designed and implemented an efficient greedy algorithm which has been demonstrated to have little influence on legitimate traffic. Simulations, which were then performed with the open source controller Ryu, show that our approach is effective in alleviating DDoS attacks and quarantining the attackers by numerable remapping process. The simulations also demonstrate that our dynamic defense imposes little effect on legitimate users, and the overhead introduced by remapping procedure is acceptable.

Analysis on the non-equilibrium dendritic solidification of a binary alloy with back diffusion (역확산을 고려한 이원합금의 비평형 수지상응고 해석)

  • Jeong, Jae-Dong;Yu, Ho-Seon;Lee, Jun-Sik
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.20 no.10
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    • pp.3361-3370
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    • 1996
  • Micro-Macro approach is conducted for the mixture solidification to handle the closely linked phenomena of microscopic solute redistribution and macroscopic solidification behavior. For this purpose, present work combines the efficiency of mixture theory for macro part and the capability of microscopic analysis of two-phase model for micro part. The micro part of present study is verified by comparison with experiment of Al-4.9 mass% Cu alloy. The effect of back diffusion on the macroscopic variables such as temperature and liquid concentration, is appreciable. The effect, however, is considerable on the mixture concentration and eutectic fraction which are indices of macro and micro segregation, respectively. According to the diffusion time, the behavior near the cooling wall where relatively rapid solidification permits short solutal diffusion time, approaches Scheil equation limit and inner part approaches lever rule limit.

Combined effect of mineral admixture and curing temperature on mechanical behavior and porosity of SCC

  • Djamila, Boukhelkhal;Othmane, Boukendakdji;Said, Kenai;El-Hadj, Kadri
    • Advances in concrete construction
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    • v.6 no.1
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    • pp.69-85
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    • 2018
  • In order to provide sufficient stability and resistance against bleeding and segregation during transportation and placing, mineral admixtures are often used in self-compacting concrete mixes (SCC). These fine materials also contribute to reducing the construction cost and the consumption of natural resources. Many studies have confirmed the benefits of these mineral admixtures on properties of SCC in standard curing conditions. However, there are few published reports regarding their effects at elevated curing temperatures. The main objective of this study is to investigate the effect of three different mineral admixtures namely limestone powder (LP), granulated blast furnace slag (GS) and natural pozzolana (PZ) on mechanical properties and porosity of SCC when exposed to different curing temperatures (20, 40, 60 and $80^{\circ}C$). The level of substitution of cement by mineral admixture was fixed at 15%. The results showed that increasing curing temperature causes an improvement in performance at an early age without penalizing its long-term properties. However the temperature of $40^{\circ}C$ is considered the optimal curing temperature to make economical and high performance SCC. On the other hand, GS is the most suitable mineral admixture for SCC under elevated curing temperature.

The Effects of Cold Rolling on the Graphitization in Boron Addition High Carbon Steel (B첨가 고탄소강의 흑연화에 미치는 냉간압연의 영향)

  • Woo, K.D.;Park, Y.K.;Ryu, J.H.;Lee, C.H.;Ra, J.P.
    • Journal of the Korean Society for Heat Treatment
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    • v.12 no.2
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    • pp.99-107
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    • 1999
  • The graphitization is affected by the addition of small amount of the elements(such as Si, Al, Ni, B, Cr and Mn etc.) and the pre-treatment(such as cold rolling). Boron is well known element to accelerate the graphitization of cementite in high carbon steels. Also, cold rolling is known to accelerate the graphitization. But the graphitization nucleation mechanism by cold rolling is few reported. Therefore the effect of cold rolling in Fe-0.5%C-1.0%Si-0.47%Mn-0.005%B steel on the graphitization is investigated quantitatively using hardness test, optical microscope and scanning electron microscope, neutron induced microscopic radiography. The nucleation of graphite in cold-rolled Fe-0.5%C-1.0%Si-0.47%Mn-0.005%B steel is formed at void which is formed at pearlite/pearlite boundary by cold rolling. But the effect of cold rolling on graphitization in boron addition steel is more effective than that of no boron addition steel due to segregation of BN at void in boron addition steel.

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The effect of $SrSO_{4}$ on Bi2212 HTS tube ($SrSO_{4}$의 첨가량이 Bi2212 고온초전도체 튜브에 미치는 영향)

  • Jung, Seng-Ho;Jang, Gun-Eik
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.05a
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    • pp.80-83
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    • 2003
  • $SrSO_4$ were systematically added on Bi2212 from 0 to 10wt% to study the effect of Bi2212 superconductor tube characteristics. After mixing, the melted solution of Bi2212 and $SrSO_4$ was initially poured into the cylinder type of steel mold preheated at $550^{\circ}C$ for 30min and rotated at 1000rpm. Following that, tube was annealed at $840^{\circ}C$ for 72hrs. The tube dimension was 60 in diameter, 60mm in length and 2mm in thickness. XRD data suggests that there was no typical segregation phase related with $SrSO_4$. Well textured grain with typical 2212 phase was observed and average size was $20{\mu}m$. The measured critical current and critical current density of Bi2212 tube added by 5% $SrSO_4$ at 77K were 495A and $202A/cm^2$ respectively.

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An extended analytical solution for the mixture solidification problem (혼합물의 응고문제에 대한 확장된 해석해)

  • Jeong, Jae-Dong;Yu, Ho-Seon;Lee, Jun-Sik
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.22 no.2
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    • pp.184-192
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    • 1998
  • This paper deals with an extended analytical solution for the mixture solidification problem, in which temperature is inherently coupled with the solute transport due to the presence of volume contraction induced flow. A new exact solution to the energy equation accounting for the convection effect in the melt is successfully derived, which allows the present analysis to cover a high initial superheating. Difference in properties between the solid and liquid phases is rigorously incorporated into the model equations in the solid fraction weighted form. Taking advantage of linearized correction factors, a systematic and easy-to-implement algorithm for determining the solidus and liquidus positions is introduced, which proves not only to converge stably but also to be very efficient. For a specific case, the present results show excellent agreements with the existing solution. The effect of convection in the melt becomes appreciable with increasing the initial superheating. It is revealed that variable properties in the mushy region significantly affect the solidification behaviors. The present study is also capable of resolving the interaction between microsegregation and macrosegregation.

Effect of Powder and Aggregates on Compactability of High Performance Concrete

  • Lee, Seung-Han;Han, Hyung-sub
    • KCI Concrete Journal
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    • v.11 no.3
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    • pp.19-28
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    • 1999
  • This study treated self-compacting high Performance concrete as two Phase materials of Paste and aggregates and examined the effect of powder and aggregates on self-compacting high performance, since fluidity and segregation resistance of fresh concrete are changed mainly by paste. To improve the fluidity and self-compactibility of concrete, optimum powder ratio of self-compacting high performance concrete using fly ash and blast-furnace slag as powders were calculated. This study was also designed to provide basic materials for suitable design of mix proportion by evaluating fluidity and compactibility by various volume ratios of fine aggregates, paste, and aggregates. As a result, the more fly ash was replaced, the more confined water ratio was reduced because of higher fluidity. The smallest confined water ratio was determined when 15% blast-furnace slag was replaced. The lowest confined water ratio was acquired when 20% fly ash and 15% blast-furnace slag were replaced together. The optimum fine aggregates ratio with the best compactibility was the fine aggregate ratio with the lowest percentage of void in mixing coarse aggregate and fine aggregate In mixing the high performance concrete. Self-compacting high performance concrete with desirable compactibility required more than minimum of unit volume weight. If the unit volume weight used was less than the minimum, concrete had seriously reduced compactibility.

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