• Korean Journal of Metals and Materials
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• v.50 no.1
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• pp.13-22
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• 2012

Forged and flat-bar rolled STD11 tool steel shows anisotropic dimensional change during heat treatment. The dimensional change in the rolling direction is larger than that in the transverse direction. The cause of the anisotropic dimensional change is that the steel is anisotropic in composition, microstructure and other properties. The decrease of anisotropic distortion in tool steel is important for making better precision cold working dies. In this study, the effect of ingot weight and hot rolling reduction ratio on the anisotropic dimensional change of STD11 during heat treatment has been studied. Dimensional change was evaluated by simulating a real heat treatment process, including gas quenching and tempering. Experimental results showed that all the rolled flat-bar products had anisotropic distortion to some degree, but the anisotropic distortion was reduced as hot rolling ratio increased. Ingot weight had a little effect on anisotropic distortion. Microstructural observation showed that the anisotropic dimensional change of STD11 tool steel was closely related to the amount, shape and distribution of coarse carbides.

• Journal of the Korean Society for Heat Treatment
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• v.14 no.1
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• pp.27-34
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• 2001

The effects of pre-heat treatment(Q/T) on microstructure and hardness of STD11 and STD61 tool steel nitrided by micro-pulse plasma were investigated. The quenching temperature for obtaining matrix hardness of STD11 and STD61 steel on range of HRC 50 to HRC 60 desired for machine parts is about $1070^{\circ}C$ and $1020^{\circ}C$ respectively. The hardness of STD11 and STD61 quenched at the temperature was HRC 63 and HRC 56 respectively. The nitrided case depth of STD11 and STD61 nitrided at $550^{\circ}C$ for 5 hours was independent of pre-heat treatment condition and the depth was approximately $100{\mu}m$. However, hardness and compactness of nitrided layer on Q/T treated specimen were higher than the annealed specimen. The case depth increased linearly with the increase of nitriding temperature, however, the hardness of nitrided layer decreased with the increase of temperature. Phase mixture of ${\gamma}-Fe_4N$ and ${\varepsilon}-Fe_{2-3}N$ was detected by XRD analysis in the nitrided layer formed at the optimum nitriding condition. The optimum nitriding temperature was approximately $490^{\circ}C$ which was $10^{\circ}C$ lower than the tempering temperature for preventing softening behavior of STD11 and STD61 matrix during nitriding process and the surface hardness of nitrided layer obtained by optimum pre-heat treatment condition was about Hv1400.

• Journal of the Korean Society for Heat Treatment
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• v.10 no.1
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• pp.71-78
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• 1997

This work was to investigate suitable tool steels for hardening using laser beam, and was studied on carbon tool steels and alloyed tool steels such as STC3 steel, STS3 steel, STD11 steel and SKH51 steel. The surface hardness of HV700-1000 and the hardening depth of 2-2.5mm were obtained on STC3 steel and STS3 steel, and HV800-1000 was obtained on SKH51 steel, but STD11 steel was not enough. Except STD11 steel, all steels used in this study can be hardened by laser quenching or laser rapid melting.

• Journal of the Korean Society of Safety
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• v.11 no.3
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• pp.59-65
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• 1996

This study is to evaluate dynamic fracture characteristics of alloy tool steel, STD-11, according to various tempering conditions (heat treatment). The dynamic fracture initiation toughness and some of the dynamic fracturing characteristics were evaluated by using the instrumented Charpy impact testing procedures. The distributions of Victors hardness and dynamic fracture initiation toughness with respect to varying tempering temperatures are found to be symmetric type with the help of experimental results for the STD-11. It is also found that the dynamic fracture initiation toughness is a inverse proportion to Vickers hardness. In this experimental study, it is found that the best heat treatment condition is 55$0^{\circ}C$ tempering in alloy tool steel, STD-11, because the results show high values of Vickers hardness and dynamic fracture initiation toughness.

• Korean Journal of Metals and Materials
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• v.46 no.12
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• pp.800-808
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• 2008

Heat treatment is an important step for tool manufacture, but unavoidably generates dimensional distortion. This study investigated the continuous dimensional change and the anisotropic behavior of STD11 tool steel during austenitizing and tempering heat treatment especially using quenching dilatometer. Dilatometric results represented that the dimensional change along longitudinal direction was larger than that along transverse direction. Anisotropic phase transformation strain was produced in forged STD11 tool steel during heat treatment. Anisotropic dimensional change increased with increasing austenitizing temperature. After tempering, anisotropic distortion was partially reduced. FactSage thermodynamic equilibrium phase simulation and microstructural observation (FE-SEM, TEM) showed that large ($7{\sim}80{\mu}m$) elongated $M_7C_3$ carbides could be formed along rolling direction. The resolution of elongated carbides during austenitizing was found to be related with the change of martensite transformation temperature after heat treatment. Anisotropic size change of STD11 tool steel was mainly attributed to large elongated carbides produced during rolling process. Using dilatometric and metallographic examination, the possible mechanism of the anisotropic size change was also discussed.

• Journal of the Korean Society for Heat Treatment
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• v.27 no.5
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• pp.242-252
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• 2014

A comparative study was performed on the microstructures and the mechanical properties of STD11 and 8Cr steel. The specimens were quenched from $1030^{\circ}C$ and tempered at $240^{\circ}C$ and $520^{\circ}C$. Vickers hardness, impact toughness and tensile tests were conducted at various tempering temperatures. Microstructural characterization to measure grain size, volume fraction of retained austenite and distribution of carbides was carried out by using SEM, EBSD, TEM and X-ray diffraction techniques. Due to finer $M_7C_3$ carbides dispersed, 8Cr steel showed larger impact toughness and plasticity than STD11 irrespective of the tempering temperature. While 8Cr steel had lower hardness in as-quenched state and after tempering at $240^{\circ}C$ owing to smaller carbide content and more retained austenite, it was harder after tempering at $520^{\circ}C$ due to larger precipitation hardening from finer $M_{23}C_6$.

• Journal of the Korean Society for Precision Engineering
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• v.16 no.2 s.95
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• pp.82-86
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• 1999

An experimental study has been carried out to reduce bending load, surface roughness and springback in bending process of stainless steel sheets. A U-bending test has been performed to investigate appropriate process parameters for getting better surfaces and accurate dimensions of stainless steel products. In the test, selected process parameters are die material, lubricant, and die clearance. Die materials used in the test are STD11(HRC60), STD11(TiCN), and AMPCO. From the test results, we can suggest that AMPCO dies are most suitable for reducing bending load and surface roughness of stainless steel sheets. And STD11 dies are favorable for avoiding spring-back in the stainless steel sheet-bending.

• Journal of the Korean Society for Heat Treatment
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• v.16 no.3
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• pp.134-140
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• 2003

Effects of cryogenic treatment and tempering temperature on the amount of retained austenite, hardness and wear properties has been investigated using alloy tool steel, STD 11. Cryogenic treatments were performed at the temperatures of $-100^{\circ}C$, $-150^{\circ}C$ and $-196^{\circ}C$, and tempering were performed at $200^{\circ}C$ and $530^{\circ}C$. It was shown that lower hardness value was obtained on high temperature ($530^{\circ}C$) tempering even after cryogenic treatment. And retained austenite was not entirely transformed to martensite after cryogenic treatment even at $-196^{\circ}C$, which was not consistent with the belief that $-80^{\circ}C$ was sufficient to entirely transform any austenite retained in the quenched microstructure. Austenite retained in cryogenic treated condition was completely transformed to martensite only after tempering at $530^{\circ}C$. As far as wear test conditions in this investigation, it was found that cryogenic treatments improved the sliding wear resistance, but improvement of wear resistance was not directly related with retained austenite contents. And it was found that predominent wear mechanisms of STD 11 steel were oxidation wear and adhesive wear In sliding wear conditions.

• Journal of the Korean Society for Heat Treatment
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• v.24 no.5
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• pp.262-270
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• 2011

Carbide precipitation and dissolution behavior at various temperatures during heat treatment has been studied in STD11 cold working die steel through confocal scanning laser microscopy; dilatometry; and X-ray diffraction analysis. The equilibrium phase diagram and phase fractions with temperature were calculated using a FactSage program. Confocal laser microscopic observation revealed that ${\alpha}$ to ${\gamma}$ transformation temperature is near $800^{\circ}C$; M7C3 carbides melt at $1245^{\circ}C$; and the melting temperature of STD11 is near $1370^{\circ}C$. XRD results indicated that the M23C6 carbides dissolve in the matrix if austenitized at over $1030^{\circ}C$; while the M7C3 carbides remain up to $1200^{\circ}C$ although their amount decreases. The calculated equilibrium phase diagram showed good agreement with experimental results on carbide dissolution and phase transformation temperatures.

• Korean Journal of Materials Research
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• v.32 no.3
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• pp.139-145
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• 2022

Reheat treatment process of mold is necessary when partial machining of the mold is required, such as shape correction for an existing mold. If defects such as cracks or significant deterioration of mechanical properties of the mold occur during reheat treatment, it is impossible to reuse the mold. In this study, reheat treatment was performed up to two times for STD11 tool steel, and microstructure and mechanical properties according to the reheat treatment were evaluated. Carbide fraction and grain size of prior austenite were almost unchanged after the reheat treatment. Hardness and impact toughness increased significantly after QT treatment, and these properties were maintained without significant change even after the reheat treatment. It is concluded that up to two iterations of reheat treatment does not cause deterioration of properties of STD11 tool steel. Based on these results, a mold for a face-lifted front bumper was manufactured through machining and reheat-treating of an existing mold.