• Journal of the Korean Ceramic Society
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• v.28 no.3
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• pp.234-242
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• 1991

Ti-B system ceramics were prepared by the self-propagating high-temperature synthesis method from the mixture of metal titanium and boron powders The major crystalline phase as a function of boron content was TiB for mixtures containing 0.5 or 1.0mol B, and TiB2 for these containing over 1.3mol B. The combustion mode observed by a high-speed camera was steady-state. The Combustion velocity increased with increasing the boron content. Sintered TiB2 specimen showed the density of 97% of theoretical valve, Vicker's hardness of 2250kg/㎟ for 0.2kg load and three-point-flexure strength of 500MPa.

• Korean Journal of Materials Research
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• v.10 no.5
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• pp.343-349
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• 2000

Fabrication of various carbide fibers from carbon fibers and elementary powders of Ti, Zr, Nb, Zi, W, B, and Mo by self-propagating high temperature synthesis was attempted. It was found the almost pure phase of TiC, ZrC, NbC, SiC, $B_4$C, and $Mo_2$C carbides were successfully produced. The three types of morphologies were ob-served, TiC, ZrC, NbC, and $B_4$C had a hollow-type fibrous shape. SiC had fiber shape consisting of smaller particles and fine whiskers. WC and $Mo_2$C had non-fibrous shapes. The reason for the different morphologies was explained. The formation mechanism of hollow fibers was suggested.

• Journal of the Korean Dietetic Association
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• v.25 no.1
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• pp.30-43
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• 2019

This study compared the predictive models for the growth kinetics of Staphylococcus aureus in ham rice balls. In addition, a semi-quantitative risk assessment of S. aureus on ham rice balls was conducted using FDA-iRISK 4.0. The rice was rounded with chopped ham, which was mixed with mayonnaise (SHM), soy sauce (SHS), or gochujang (SHG), and was contaminated artificially with approximately $2.5{\log}\;CFU{\cdot}g^{-1}$ of S. aureus. The inoculated rice balls were then stored at $7^{\circ}C$, $15^{\circ}C$, and $25^{\circ}C$, and the number of viable S. aureus was counted. The lag phases duration (LPD) and maximum specific growth rate (SGR) were calculated using a Baranyi model as a primary model. The growth parameters were analyzed using the polynomial equation as a function of temperature. The LPD values of S. aureus decreased with increasing temperature in SHS and SHG. On the other hand, those in SHM did not show any trend with increasing temperature. The SGR positively correlated with temperature. Equations for LPD and SGR were developed and validated using $R^2$ values, which ranged from 0.9929 to 0.9999. In addition, the total DALYs (disability adjusted life years) per year in the ham rice balls with soy sauce and gochujang was greater than mayonnaise. These results could be used to calculate the expected number of illnesses, and set the hazard management method taking the DALY value for public health into account.

• Journal of the Korean Society of Environmental Restoration Technology
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• v.2 no.1
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• pp.1-9
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• 1999

To find pertinent soil type and maintenance method for artificial planting ground, the effects of soil compositions{sandy loam(S), vermiculite(V), sandy loam+vermiculite+sand(SVS), sandy loam+ carbonized rice husk+sand(SCS), sandy loam+humus sawdust+sand(SHS)}, and fertilizers (organic, chemical) on plant(kentuckyblue grass) growth were measured and compared from the field experiment. The results are summarized as follows 1. the highest germination rate is found from "vermiculite(V)" and the lowest from "sandy loam(S)" among tested 5 soil compositions. 2. "sandy loam+vermiculite+sand(SVS)" composition shows the highest plant height growth effect (5cm growth during tested 3 months) comparing to other 4 compositions. 3. "sandy loam+vermiculite+sand(SYS)" composition shows the highest ground covering rate after first two months, but it concede its order to "sandy loam+humus sawdust+sand(SHS)" composition after next one month growing. 4. the effects of fertilizers are follows 1) Among the blocks where no fertilizer was tried, the predominant height growth was obvious in "sandy loam+carbonized rice husk+sand(SCS)" and "sandy loam+humus sawdust+sand(SHS)" composition. 2) Among the blocks where chemical fertilizer was tried, relatively positive results were found from "vermiculite(V)" and "sandy loam+vermiculite+sand(SYS)" blocks on germination and growth rate. But on the ground coverage ratio, the effect of "sandy loam+carbonized rice husk+sand(SCS)" composite precede that of those 2 composites. 3) Among the blocks where organic fertilizer was tried, "sandy loam+humus sawdust+sand(SHS)" and "vermiculite(V)" blocks show relatively high ground coverage rate, growth rate than others. 4) When compositional differences were not considered, the block where organic fertilizer was tried shows most positive effects on all 3 measurements-germination ratio, height growth and ground covering.

• Journal of the Korean Ceramic Society
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• v.32 no.3
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• pp.341-348
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• 1995

An analysis of the use of temperature profiles in the determination of the kinetic parameters of combustion synthesis of Ti5Si3 were investigated. From profile analysis, an apparent activation energy of 12KJ/mol was calculated. The Maximum heating rate achieved during 10wt% Ti5Si3 reaction by the product dilution method was approximately $1.5\times$104 K/s. Coupling this value with the measured wave velocity of 7.02 cm/s yields a maximum thermal gradient of 2.14$\times$103 K/cm. The value of tr (=t*) was calculated to be 1.2$\times$10-1 s and the value of td (=tx) was calculated to be 32.89 s. Using the definition of t* and the measured wave velocity, the effective thermal diffusivity, $\alpha$, was calculated to be 0.59$\times$10 $\textrm{cm}^2$/s. From these analysis, the power function, G, was also calculated.

• KIEAE Journal
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• v.4 no.3
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• pp.129-136
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• 2004

Recently, indoor air pollution has been seriously apprehended, and became a striking issue, due to the airtightness of buildings or the misuse of building materials. Especially, SHS(Sick House Syndrome) and MCS(Multi Chemical Sensitivity) which can have bad influences on the resident in an existing apartment house as well as newly constructed apartment house start to attract public attention. The emission rates of VOCs is sensitively affected by the indoor/outdoor condition, construction materials, construction method, and character of ventilation facilities. Therefore, in this study, by measuring the indoor air pollution substance of the existing apartment house, the problem over this tends to be grasped and it is going to secure an improvement methods.

• The Korean Journal of Ceramics
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• v.5 no.2
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• pp.148-154
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• 1999

A method to simultaneously synthesize and consolidate $Ti_5Si_4 \;and\; Ti_5Si_3$-20 vol%Nb composite from powders of Ti, Si and Nb was investigated. Combustion synthesis was carried out under the combined effect of an electric field and mechanical pressure. Highly dense $Ti_5Si_4 \;and\; Ti_5Si_3$-20 vol% Nb with relative densities up to 98% was produced from powders of Ti, Si and Nb under the application of 60 MPa pressure and 3000A current on the reactant.

• Journal of Powder Materials
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• v.8 no.4
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• pp.231-238
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• 2001

We combined Field-Activated Combustion Synthesis(FACS) with mechanical pressure to produce dense WC-20 vol.%Co composite in one step. The hardness, the fracture toughness and the relative density of the dense WC-20 vol.%Co were investigated. Under the application of 60 MPa pressure and 3000A current on the reactants, the relative density of WC-20 vol.%Co composite was 99.4%. The fracture toughness and hardness were $9.4 MPa.m^{1/2}$ and $1672kg\textrm{mm}^2$ respectively. The fracture toughness and hardness of WC-20 vol.%Co composite produced by FAPACS were lower than that of nanostructured composite, but similar to commercial ones. Therefore we concluded that the FAPACS method which can produce WC-20 vol.%Co within several minutes in one step is superior to conventional ones.

• Analytical Science and Technology
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• v.35 no.5
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• pp.189-196
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• 2022

When cationic basic compounds are chromatographed using hydro-organic mobile phase, the presence of anionic free silanols in the silica-based stationary phases results in broad and asymmetrical peaks. The addition of an ionic reagent to the mobile phase prevents analytes from accessing free silanols, improving peak shape. In this study, the chromatographic behavior of salbutamol sulfate as a basic compound was investigated under various conditions, including the use of different columns, mobile phases, and ion-pair reagents such as triethanolamine (TEA) and sodium heptane sulfonate (SHS). The retention and peak shape of chromatograms were both evaluated. The results show that pre-conditioning the column with TEA and including it in the mobile phase can prevent cationic analytes from accessing anionic silanols, resulting in improved peak shape. Furthermore, buffering the mobile phase is an important factor in keeping the pH constant throughout the process. The chosen method was validated in part. This study could be helpful for researchers and analyst to solve such problems with cationic basic components.

• Transactions of the Korean Society for Noise and Vibration Engineering
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• v.14 no.7
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• pp.551-560
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• 2004

A method how to determine the shock response spectrum from the FRF of the statistical energy analysis( SEA ) is presented here. The system of 3 different Plates connected by bolt joints is selected simulating missile structural sections Joined together. First, the SEA model was rendered by SEA parameters which were determined from experimental SEA method. Then, the mobility power was input to the SEA model and we can verify the validity of the model in the medium to high frequency range checking the reproduction of output average velocity. And, the shock induced shock response spectrum(SRS) was obtained using SEA FRF and arbitrarily chosen experimental FRF. We have compared the thus obtained SRS with actually measured SRS and they were relatively in good agreement. In this paper, we used the measured SEA FRF and therefore we have got the SRS well agreed with actually measured SHS even in the low frequency range. If the SEA FRF of well verified SEA model is used, the good result will come out in SEA effective frequency range which is more important at SRS.