• Corrosion Science and Technology
• /
• v.23 no.1
• /
• pp.54-63
• /
• 2024

This work investigated the influence of concentration and applied potential on the characteristics of zinc powder (purity, apparent density, morphology, particle size distribution, and particle zeta potential) produced by the electrochemical process from waste brass. High-purity zinc powder is obtained using selective leaching of industrial brass waste in acidic, neutral, and alkaline solutions. The free immersion method with and without voltage using linear polarization technique is used. In the electrochemical process, hydrochloric acid HCl in three different concentrations (0.1, 0.2, and 0.3) M is used. The time and the distance between the electrodes are set to be 30 min and 3 cm, respectively. It has been found that the percentage purity is 98%, 96%, and 94% for the acidic, neutral, and alkaline solutions, respectively. In addition, the morphology of zinc powder analyzed by SEM was dendritic and mossy. It has been recorded that the purity of zinc increases with the increase of the concentration and applied potential. The highest value of purity for zinc powder was %98.58 in 1000 mV and 0.3M concentration for graphite cathode.

• Structural Engineering and Mechanics
• /
• v.91 no.3
• /
• pp.279-289
• /
• 2024

The purpose of this study is to represent a useful alternative for the preliminary seismic vulnerability assessment of existing reinforced concrete buildings by introducing a statistical approach employing the binary logistic regression technique. Two different predictive statistical models, namely full and reduced models, were generated utilizing building characteristics obtained from the damage database compiled after 1999 Düzce earthquake. Among the inspected building parameters, number of stories, overhang ratio, priority index, soft story index, normalized redundancy ratio and normalized lateral stiffness index were specifically selected as the predictor variables for vulnerability classification. As a result, normalized redundancy ratio and soft story index were identified as the most significant predictors affecting seismic vulnerability in terms of life safety performance level. In conclusion, it is revealed that both models are capable of classifying the set of buildings being severely damaged or collapsed with a balanced accuracy of 73%, hence, both are able to filter out high-priority buildings for life safety performance assessment. Thus, in this study, having the same high accuracy as the full model, the reduced model using fewer predictors is proposed as a simple and viable classifier for determining life safety levels of reinforced concrete buildings in the preliminary seismic risk assessment.

• Journal of Bio-Environment Control
• /
• v.19 no.3
• /
• pp.147-152
• /
• 2010

Poor fruit set during winter period is one of the biggest problem in plastic tunnel watermelon cultivation. Hand pollination is inevitable to maximize fruit set of the winter watermelon. Productivity and viability of pollen grain and organic solvents for pollen storage were investigated. All cultivars produced more than 10 mg/flower except for 'Kumchun' cultivar. Pollen amount per flower were 13.8 mg in 'Bok' and 12.1 mg in 'Speedkul'. Germination rate of pollen grains incubated at $30^{\circ}C$ right after soaking in pentane solvent were 76% in 'Kumchun' as the lowest and 92% in 'Apollokul' as the highest. The pollen of 'Bok' showed the highest germination rate by 75% after a 15-day storage in pentane. All cultivars showed their pollen germination rate below 25% after a 24-day storage. Among the cuitivars, speed of pollen tube growth in vitro were relatively lower in 'Kumchun' and 'Sambokkul' by below $50\;{\mu}m/hr$. Pollen tube of these cultivars tended to burst during its elongation on the medium. Pollen stored 24 hrs in organic solvents showed 45, 39, 34, 23, and 19% of germination in pentane, ethyl ether, n-hexane, ethyl acetate, and acetone, respectively. Compared with light condition, pollen viability was higher in darkness during pollen storage in organic solvents. Pollen grain was susceptible to the organic solvent. The viability of pollen grains seems to be influenced greatly by duration of soaking pollen in organic solvent and the polarity of solvents. Organic solvent damages surface of pollen grain and extent of damage was varied by the solvents.

• The Journal of Korean Academy of Prosthodontics
• /
• v.36 no.3
• /
• pp.468-482
• /
• 1998

Since the concept of osseointegration was introduced by Branemark of Sweden, dental implants have been used for various dental prosthetic treatments. The survival rate of dental implant is likely to be closely related to the total biomechanical role of each component of implant system. The use of interchangeable component is very attractive for dental practitioners because such an approach would save treatment cost, flexibility of prosthetic treatment options as well as conveniences. Therefore, the use of interchangeable implant system has been increasing without scientific assessment of safety and efficacy of various interchangeable implant system. The purpose of this study, therefore, were to compare the geometric characteristic of four interchangeable dental implant screws and the loosening torque of these screws. Four types of dental implant screws tested in this study were Nobelpharma, 3i, Impla-med, Restore. Four screws each of the test specimens were subjected for scanning electron microscopic examinations under the same condition and a 35x magnified standard SEM picture was objected from each test specimen using JSM-5200 scanning microscope. From each of the SEM pictures, eight parameters. i.e., diameter of screw head. screw length, thread pitch, major diameter. neck diameter, neck length, crest width and root width were determined using a caliper. The measurement for each parameters were then corrected for their magnification factor. The loosening torque were also determined by using a torque gauge. All of the measurements were statistically analyzed by ANOVA test and multiple range test. Statistical significance was set in advance at the probability level of less than 0.05. All analyses were done with SPSS software for the personal computer. The conclusion obtained from this studies were summarized as the following; 1. No statistically significances were noted in the thread pitch. and crest width in the four screws, and in the case of major diameter, the Impla-med screw was significantly smaller than the other three screws (p<0.05). Therefore, four implant bolts could be physically inserted in a abutment nuts. 2. The diameter of screw head was decreased in the order of Restore, 3i, Nobelpharma, Impla-med screws and the length of screws were decreased in the order of 3i, Restore, Nobelpharma and Impla-med. The diameter of neck was decreased in the order of Impla-med, Restore. Nobelpharma, 3i screws. The differences of each of these parameters were statistically significant (p<0.05). The width of root of screws were decreased in the order of Nobelpharma, Impla-med, Restore and 3i. The differences among Nobelpharma and Impla-med. Restore and 3i were statistically significant (p<0.05). 3. When the screws were loosening 1, 3, 4 and 5 times, the loosening torque for Impla-med and 3i screws were significantly higher than that of Nobelpharma or Restore screws (p<0.05). However, when statistically smaller than that of 3i, Restore or Nobelpharma screws(p<0.05).

• Journal of Korean Society of Transportation
• /
• v.32 no.3
• /
• pp.207-217
• /
• 2014

Many a number of policies have been tried to reduce auto accidents so far, but it is obvious that further studies are still needed to find a more fundamental and multi-dimensional preventive measure with effect. The National Mental Health Statistics shows that the most profound forms of negative emotions, that is, depression and anxiety, have been increasing, but studies on such a topic are scarce to find. Therefore, we conducted a structural analysis between the negative emotions, including depression and anxiety, of drivers and their driving behaviors using a Structural Equation Modeling(SEM) technique. The review of past literature and studies indicated that not all of human emotions manifest themselves as the ultimate behaviors because they go through emotion regulation Strategies. For this reason, the purpose of this study was set to analyze the structural model developed in this study reflecting the emotion regulation strategies. The result of our analysis showed that the driver's negative emotion had a more significant influence on dangerous driving behaviors than safe ones, and especially, the expressive suppression strategy was found to be the highest factor. Also, the total effect analysis with the negative emotional factors showed that expressive suppression had more significant influence compared to that of cognitive reappraisal. The implication of this study might provide a better understanding on driving behaviors of the drivers and could be used as a fundamental study for future policy development to reduce traffic accidents.

• Proceedings of the Korean Institute of Surface Engineering Conference
• /
• 2003.10a
• /
• pp.134-135
• /
• 2003

The dental implant materials required good mechanical properties, such as fatigue strength, combined with a high resistance to corrosion. For increasing fatigue resistance and delaying onset of stress corrosion cracking, shot peening has been used for > 50 years to extend service life of metal components. However, there is no information on the electrochemical behavior of shot peened and hydroxyapatite(HA) coated Ti-6Al-4V alloys. To increase fatigue strength, good corrosion resistance, and biocompatibility, the electrochemical characteristics of Ti/TiN/HA coated and shot peened Ti-6Al-4V alloys by electron beam physical vapor deposition(EB-PVD) have been researched by various electrochemical method in 0.9%NaCl. Ti-6Al-4V alloys were prepared under the condition of hydrogen and vacuum arc furnace. The produced materials were quenched at 1000$^{\circ}C$ under high purity dried Ar atmosphere and were hold at 500$^{\circ}C$ for 2 hrs to achieve the fatigue strength(1140㎫) of materials. Ti-6Al-4V alloys were prepared under the condition of hydrogen and vacuum arc furnace. Shot peening(SP) and sand blasting treatment was carried out for 1, 5, and 10min. On the surface of Ti-6Al-4V alloys using the steel balls of 0.5mm and alumina sand of 40$\mu\textrm{m}$ size. Ti/TiN/HA multilayer coatings were carried out by using electron-beam deposition method(EB-PVD) as shown Fig. 1. Bulk Ti, powder TiN and hydroxyapatite were used as the source of the deposition materials. Electrons were accelerated by high voltage of 4.2kV with 80 - 120mA on the deposition materials at 350$^{\circ}C$ in 2.0 X 10-6 torr vacuum. Ti/TiN/HA multilayer coated surfaces and layers were investigated by SEM and XRD. A saturated calomel electrode as a reference electrode, and high density carbon electrode as a counter electrode, were set according to ASTM GS-87. The potentials were controlled at a scan rate of 100 mV/min. by a potentiostat (EG&G Co.273A) connected to a computer system. Electrochemical tests were used to investigate the electrochemical characteristics of Ti/TiN/HA coated and shot peened materials in 0.9% NaCl solution at 36.5$^{\circ}C$. After each electrochemical measurement, the corrosion surface of each sample was investigated by SEM.

• Journal of the Korean Society for Nondestructive Testing
• /
• v.36 no.1
• /
• pp.18-26
• /
• 2016

The semiconductor industry is one of the key industries of Korea, which has continued growing at a steady annual growth rate. Important technology for the semiconductor industry is high integration of devices. This is to increase the memory capacity for unit area, of which key is photolithography. The photolithography refers to a technique for printing the shadow of light lit on the mask surface on to wafer, which is the most important process in a semiconductor manufacturing process. In this study, the width and step-height of wafers patterned through this process were measured to ensure uniformity. The widths and inter-plate heights of the specimens patterned using photolithography were measured using transmissive digital holography. A transmissive digital holographic interferometer was configured, and nine arbitrary points were set on the specimens as measured points. The measurement of each point was compared with the measurements performed using a commercial device called scanning electron microscope (SEM) and Alpha Step. Transmission digital holography requires a short measurement time, which is an advantage compared to other techniques. Furthermore, it uses magnification lenses, allowing the flexibility of changing between high and low magnifications. The test results confirmed that transmissive digital holography is a useful technique for measuring patterns printed using photolithography.

• Journal of Korean Elementary Science Education
• /
• v.43 no.1
• /
• pp.95-107
• /
• 2024

In this study, we explored the mediating effect of grit in the relationship between elementary school science teachers' perceived personal pedagogical content knowledge (pPCK) and enacted pedagogical content knowledge (ePCK). Drawing on insights from a review of the literature, we developed a research hypothesis model that set pPCK, ePCK, and grit as latent variables. Pearson correlation was conducted to examine the interrelationships among the latent variables. Structural equation modeling (SEM) was then employed to analyze the model fit. Additionally, bootstrap analysis was performed to specifically investigate the mediating effect of grit in the relationship between pPCK and ePCK. The Pearson correlation analysis indicated statistically significant correlations among the measurement variables. Meanwhile, the SEM analysis revealed that the measurement model aligned with the research hypothesis model. Furthermore, the bootstrap analysis demonstrated that grit had a statistically significant mediating effect in the relationship between elementary school science teachers' perceived pPCK and ePCK. These findings quantitatively examine the importance and impact of grit in the teacher expertise domain, providing valuable insights for the development of teachers' expertise and teacher education research within elementary school science classes.

• Journal of the Microelectronics and Packaging Society
• /
• v.11 no.2 s.31
• /
• pp.23-28
• /
• 2004

We utilized Ag capping layer for fluxless bonding. To investigate the effect of Ag capping layer, two sets of sample were used. One set was bare In and Sn solders. The other set was In and Sn solders with Ag capping layer. In ($10{\mu}m$) and Sn ($10{\mu}m$) solders were deposited on Cu/Ti/Si substrate using thermal-evaporation, and Ag ($0.1{\mu}m$) capping layers were deposited on In and Sn solders. Solder joints were made by joining two In and Sn deposited specimens at $130^{\circ}C$ for 30 s under 0.8, 1.6, 3.2 MPa using thermal compression bonder. The contact resistance was measured using four-point probe method. The shear strength of the solder joints was measured by the shear test of cross-bar sample in the direction. The microstructure of the solder joints was characterized with SEM and EDS. In and Sn solders without Ag capping layers were only bonded at $130^{\circ}C$ under high bonding pressure. Also the shear strength of the In-Sn solder joints under was lower than that of the Ag/In-Ag/Sn solder joints. The resistance of the solder joints was $2-4\;m{\Omega}$ The solder joints consisted of In-rich phase and Sn-rich phase and the intermixed compounds were found at the interface. As bonding pressure increased, the intermixed compounds formed more.

• Design & Manufacturing
• /
• v.14 no.1
• /
• pp.49-55
• /
• 2020

In this study, the fatigue behavior and fatigue life characteristics of PA2200 specimens fabricated by SLS 3D printer were studied. Fatigue tests were performed according to the standard specification (ASTM E468) and fatigue life curves were obtained. In order to perform the fatigue test, mechanical properties were measured according to the test speed of the simple tensile test, and the self-heating temperature of the specimen according to the test speed was measured using an infrared temperature measuring camera in consideration of heat generation due to plastic deformation. There was no significant difference within the set test speed range and the average self-heating temperature was measured at 38.5 ℃. The mechanical strength at the measured temperature showed a relatively small difference from the mechanical strength at room temperature. Fatigue test conditions were established through the preceding experiments, and the loading conditions below the tensile strength at room temperature 23 ℃ were set as the cyclic load. The maximum number of replicates was less than 100,000 cycles, and the fracture behavior of the specimens with the repeated loads showed the characteristics of Racheting. It was confirmed that SLS 3D printing PA2200 material could be applied to the Basquin's S-N diagram for the fatigue life curve of metal materials. SEM images of the fracture surface was obtained to analyze the relationship between the characteristics of the fracture surface and the number of repetitions until failure. Brittle fracture, crazing fracture, grain melting, and porous fracture surface were observed. It was shown that the larger the area of crazing damage, the longer the number of repetitions until fracture.