• 제목/요약/키워드: SEP

검색결과 1,146건 처리시간 0.025초

비파괴 분석 방법인 푸리에 변환 근적외선 분광 분석을 이용한 한지 기록물의 산성도 및 함수율 정량 분석 연구 (The study of quantitative analytical method for pH and moisture of Hanji record paper using non-destructive FT-NIR spectroscopy)

  • 신용민;박성배;이창영;김찬봉;이성욱;조원보;김효진
    • 분석과학
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    • 제25권2호
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    • pp.121-126
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    • 2012
  • 한지기록물의 상태를 평가하는 데 있어 기록물의 훼손을 방지하는 것은 필수적인 요소이다. 사용된 공시재료는 1900년대 생산된 한지기록물을 사용하였다. 이 종이 기록물의 상태를 평가하기 위하여 비파괴적 분석기인 12,500~4,000 $cm^{-1}$ 파장영역을 가진 푸리에변환(FT) 근적외선 분광 분석기를 이용하였다. 푸리에변환 방식의 간섭계는 뛰어난 정밀도와 정확도를 가지며, 신호-대-잡음비가 가장 우수 하여 정량 분석에서 가장 많이 사용되고 있다. 한지기록물의 산성도와 함수율을 적분구(integrating sphere)의 확산반사로 사용하여 측정하였다. 산성도(pH)의 경우에 전처리를 하지 않았을 때의 상관계수($R^2$)는 0.92, 표준예측오차(SEP)는 0.317이었고, 전처리를 하였을 때의 $R^2$는 0.98, SEP는 0.208 이었다. 그리고 함수율의 경우 산성도와 달리 전처리를 하지 않았을 경우에도 $R^2$와 SEP는 각각 0.99와 0.458로 확인 되었다. 전처리 중 다산란 보정방법(MSC)의 경우에는 $R^2$가 0.97, SEP가 0.558로 증가하는 것을 확인 할 수 있어 함수율은 전처리를 하지 않았을 때가 좋은 결과가 나오는 것으로 확인 되었다. 이러한 결과를 통해 비파괴적인 분석방법으로 한지기록물을 적분구와 FT 근적외선 분광 분석기를 이용하여 한지의 상태를 정확히 평가할 수 있을 것으로 판단되었다.

Development of robust Calibration for Determination Sweetness of Fuji Apple fruit using Near Infrared Reflectance Spectroscopy

  • Sohn, Mi-Ryeong;Kwon, Young-Kill;Cho, Rae-Kwang
    • Near Infrared Analysis
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    • 제2권1호
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    • pp.55-58
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    • 2001
  • The object of this work was to investigate the influence of growing district and harvest year on calibration for sweetness (Brix) determination of Fuji apple fruit using near infrared (NIR) reflectance spectroscopy, and to develop the robust calibration across these variation. The calibration models was based on wavelength range of 1100∼2500 nm using a stepwise multiple linear regression. A calibration model by sample set of one growing district was not transferable to other growing districts. The combined calibration (data of three growing districts) predicted reasonable well against a population set drawn from all growing districts (SEP=0.69, Bias=0.075). A calibration model by sample set of one harvest year was not also transferable to other harvest years. The combined calibration (data of three harvest years) predicted well against a population set drawn from all harvest years (SEP=0.53, Bias=0.004).

경량전철사업을 위한 실용적 SEMP 개발에 관한 연구 (A study on the practical Systems Engineering Management Plan for the LRT Project)

  • 최요철;한석윤;차기호;정수영;배준호
    • 한국철도학회:학술대회논문집
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    • 한국철도학회 2011년도 춘계학술대회 논문집
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    • pp.247-254
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    • 2011
  • This paper is a study on the practical Systems Engineering Management Plan(SEMP) for the LRT Project. A SEMP shall be developed and applied to define and manage the systems engineering activities during the beginning of LRT Project. This paper is addressed contents and description of the practical systems engineering management plan based on the existing practices about system engineering management plan in LRT Project domain as well as the systems engineering standard as MI-STD 499A, IEEE 1220 etc. In the early stage of a LRT Project, An acquirer should provide a Systems Engineering Plan(SEP), and a contractor should summit a Systems Engineering Management Plan as the SEP in proposal. This addressed the SEMP as an aspect of the system and sub-systems supplier to systematically and effectively accomplish the systems engineering activities in LRT Project generally.

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식육중 Chlorfluazuron의 잔류분석법 및 잔류량에 관한 연구 (Studies on the Analytical Methods and Quantity of Residual Chlorfluazuron in Meat)

  • 박건상;홍무기;백선영;정병곤;박종세
    • 한국식품위생안전성학회지
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    • 제12권4호
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    • pp.288-293
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    • 1997
  • Analytical method using capillary GC/ECD was developed to determine trace residues of chlofluazuron, 1-[3, 5-dichloro-5-trifluoromethyl-2-pyridyloxy)phenyl]-3-(2, 6-difiuorobenzoyl), in meat, and applied to analyze the residues in domestic and imported meats. The analytical scheme developed does not require column chromatographic cleanup; chlorfiuazuron was extracted with diethyl ether and petroleum ether (50: 50), partitioned against acetonitrile, cleaned up with silica Sep-Pak cartridge, identified GC/ECD, and comfirmed by GC/MS. The mean recoveries of the pesticide in meat fortified with standard solution 0.1, 0.5, 0.1 mg/kg were ranged from 82 to 95%. The limit of detection and limit of quantitation were 0.001 and 0.005 mg/kg, respectively. Chlorfluazuron residues were not found in domestic samples, but found in imported Australian beef ranging from 0.02 to 0.17 mg/kg, detected by 18% among the samples.

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UWB를 이용한 실내측위의 베이스 스테이션 최적 배치 (Optimization of base stations' configuration in UWB-based indoor localization)

  • 장효욱;차맹규;김용일;유기윤
    • 한국측량학회:학술대회논문집
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    • 한국측량학회 2006년도 춘계학술발표회 논문집
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    • pp.3-7
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    • 2006
  • Indoor localization is getting more and more importance with the increasing demand for location based service. Location based service necessarily requires the information about customers' locations to provide them the right service according to their changing locations. To satisfy that requirement, GPS is used to achieve outdoor localization. However, there is no leading technology to achieve indoor localization. Indoor localization through UWB wave and TDOA algorithm is considered as the most accurate method until now. In implementing that method, configuration of base stations that serve as control points affects the localization accuracy. Thus, this paper discusses about optimal configuration of base stations. The variation in localization accuracy according to spatial relationship between an object and base stations Is mentioned through SEP also.

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총폐정맥 환류이상의 수술적 교정및 후발성 폐정맥 협착 (Total Anomalous Pulmonary Venous Connection; Surgical Correction and Late Pulmonary Venous Obstruction)

  • 서동만;송명근
    • Journal of Chest Surgery
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    • 제26권4호
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    • pp.260-265
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    • 1993
  • Twelve patients underwent surgical correction of total anomalous pulmonary venous connection[TAPVC] between Sep. 1989 and May 1993. There were 9 boys and 3 girls whose ages ranged from 10 days to 17 month [median 1.2 month]. Six patients were less than 1 month of age at operation. The anomalous drainage was supracardiac in 6, cardiac in 2, infracardiac in 2, and mixed in 2. There were 3 early death, and its mortality rate was 25%. There were no operative mortality after Sep. 1991. Age at operation, presence of preoperative pulmonary venous obstruction, preoperative assisted ventilation and type of anomaly did not affect early mortality. Late pulmonary venous obstruction was developed in 4 patients between 1 month to 4 month after operation. Among these patients, 2 were died and one was reoperated and well, and the other one was not operated because of patient`s refusal. We conclude that late pulmonary venous obstruction is fatal and its early detection and correction is important for improving late survival.

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Brain MRA상 stenosis정도와 중풍변증모형을 비교한 18례 (Relationship between the Severity of Stenosis and Stroke Pattern-identification in 18 Acute Stroke Patients)

  • 곽미애;정우상;박정미
    • 대한한의학회지
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    • 제21권3호
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    • pp.51-56
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    • 2000
  • To assess the relationship between the severity of stenosis in MCA territory and the differentiation of syndromes in oriental medical aspects, the general characteristics, the scores of stroke-pattern identification, and the findings of MRA were compared in 18 acute cerebral infarction patientshospitalized in Dept. of Internal Medicine, Pundang CHA Oriental Medicine Hospital from 1998 sep. 1 to 1999 sep. 31. We compared the scores of stroke-pattern identification with the severity of stenosis by Kruskall-Wallis test, and analyzed the relationship by Pearson correlation test. The P value under 0.05 was regarded as significant. The results are as follows: The incidence of stenosis(mild to complete occlusion) was 83.3%. There were significant difference of the mean scores according to the severity of stenosis in Yin deficiency pattern. We could also observe a strong relationship between the severity of stenosis and Yin deficiency pattern, whose Pearson correlation coefficient was 0.655 (P<0.05). These results showed that Yin deficiency pattern could be a major cause of cerebral infarction.

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