• Title/Summary/Keyword: SEM morphology

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A Study on Fractal Analysis and 3D Images of Surface on BST Thin Films. (BST 박막 표면의 프랙탈 분석 및 3D 이미지 특성)

  • Hong, Kyung-Jin;Min, Yong-Ki;Cho, Jae-Cheol
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.05b
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    • pp.103-106
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    • 2002
  • The applicability of models based on fractal morphology to characterize $(Ba\;Sr)TiO_{3}$ thin film surfaces was investigated. The fractal morphology of coated barium strontium titan oxide thin film surfaces was described using fractal dimension from scanning electro microscopy image. The $(Ba\;Sr)TiO_{3}$ coating were deposited on silicon wafers using $(Ba\;Sr)TiO_{3}$ solution and spin coater. BST solution was composited by mol ratio, and then spin-coated from 3 times to 5 times coating on $Pt/SiO_{2}/Si$ substrate. Qualitative thin film analysis was performed with scanning electro microscopy (SEM), and surfaces parameters such as average grain diameter, roughness exponent and fractal dimension were determined.

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Growth of ZnO Nanostructures on Various Substrates by Simple Aqueous Solution Method (습식화학방법에 의해 다양한 기판위에 ZnO 나노구조물의 성장)

  • Lee, Sam-Dong;Jin, Mi-Jin;Shin, Kyung-Sik;Jeong, Soon-Wook;Kim, Sang-Woo
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.21 no.7
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    • pp.599-602
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    • 2008
  • Growth of well-aligned ZnO nanostructures on various substrates such as GaN, ITO/glass, and sapphire was realized via a simple aqueous solution method at low temperature of $90^{\circ}C$. Morphology of ZnO nanostructures grown on various substrates as function of substrate was studied. It was found that ZnO nanostructures is a strong function of substrate. It was clearly observed that the morphology of ZnO nanostructures could be varied by change of substrate. Morphology, crystallinity, and crystal characteristics were carried out by FE-SEM, synchrotron x-ray scattering measurements, and high-resolution electron microscopy, respectively.

The Effect of Coagulant on the Post Drawing and Morphology of Wet Spun Regenerated SF/Nylon 6 Blend Filaments

  • Um, In-Chul
    • International Journal of Industrial Entomology and Biomaterials
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    • v.16 no.2
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    • pp.61-66
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    • 2008
  • In this paper, the regenerated silk fibroin (SF)/nylon 6 blend filaments were fabricated using wet spinning technique and the effect of coagulant on the post drawing and morphology of blend filaments was investigated. In the result of wet spinnability, methanol, acetone, DMF, and THF showed relatively good coagulation strength and fiber formation for the regenerated SF. On the contrary, they did not exhibit strong enough to produce a uniform nylon 6 filament due to the lack of coagulation strength. In the examination of post drawing performance, methanol showed the highest maximum draw ratio of the blend filament over all blend ratios. The maximum draw ratio of SF/nylon 6 blend filaments decreased with the reduction of SF content regardless of type of coagulant. SEM observation showed the consistent result with that of post-drawing performance. As SF content decreased, the uniform and regular structure was changed to irregular one. In particular, the severe macro-phase separation between SF and nylon 6 could be detected in the 50/50 SF/nylon 6 blend filaments coagulated in methanol and THF.

Investigation on HT-AlN Nucleation Layers and AlGaN Epifilms Inserting LT-AlN Nucleation Layer on C-Plane Sapphire Substrate

  • Wang, Dang-Hui;Xu, Tian-Han
    • Journal of the Optical Society of Korea
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    • v.20 no.1
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    • pp.125-129
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    • 2016
  • In this study, we have investigated a high-temperature AlN nucleation layer and AlGaN epilayers on c-plane sapphire substrate by low-pressure metal-organic chemical vapor deposition (LP-MOCVD). High resolution X-ray diffraction (HRXRD), atomic force microscopy (AFM), scanning electron microscope (SEM) and Raman scattering measurements have been exploited to study the crystal quality, surface morphology, and residual strain of the HT-AlN nucleation layer. These analyses reveal that the insertion of an LT-AlN nucleation layer can improve the crystal quality, smooth the surface morphology of the HT-AlN nucleation layer and further reduce the threading dislocation density of AlGaN epifilms. The mechanism of inserting an LT-AlN nucleation layer to enhance the optical properties of HT-AlN nucleation layer and AlGaN epifilm are discussed from the viewpoint of driving force of reaction in this paper.

A Study on the Mechanical Properties and Shrinkage of Thermoplastic Elastomer (열가소성 엘라스토머의 기계적 물성과 수축에 관한 연구)

  • Han, S.R.;Kim, J.H.;Jeon, S.G.;Jeong, Y.D.
    • Transactions of Materials Processing
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    • v.16 no.1 s.91
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    • pp.36-41
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    • 2007
  • Thermoplastic elastomer(TPE) can be recycled and molded such as commercial thermoplastic. Therefore TPE has being widely applied on automobile, household and etc. in these days. This study shows the variation of mechanical properties and shrinkage on TPE moldings for variation of injection molding conditions such as injection pressure, holding pressure, melt temperature, mold temperature and etc. Mechanical properties in relation to tensile strength, hardness and shrinkage in connection with precision dimension of part are investigated. The tensile strength and shrinkage of the experimental TPEs are mainly influenced by injection pressure and melt temperature. All injection molding conditions scarcely affect on hardness. To verify the variation of tensile strength and shrinkage, morphology of TPE molding was scanned by the SEM. The morphology showed that as the melt temperature increased, the rubber particles on the TPE became smaller and widely were dispersed. This behavior of rubber particles influenced on the increase of tensile strength.

Preparation of Al-Sn Coating Bearings by RF Sputtering Method and Evaluation of Their Properties (RF 스퍼터링법에 의한 Al-Sn계 코팅베어링의 제작과 특성 평가)

  • 이찬식;이명훈
    • Journal of Advanced Marine Engineering and Technology
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    • v.24 no.6
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    • pp.139-146
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    • 2000
  • The development of high performance materials is very important subject in order to enhance the properties of bearings whose role is to transfer energy harmoniously by reducing the problem of friction and wear down, etc. between the interacting solid surfaces in relative motion under high loads in comply with mechanical operating mechanism of engines. In this study, several (100-x)Al-xSn coating films (where x=85, 75, 65 atomic % at Al) on substrates which are abt. 2mm thickenss of Kelmet layer sintered back steel were prepared by using RF sputtering system. These coating films were observed the morphology by SEM(Scanning Electron Microscope) and investigated the crystal structure by XRD(X-ray Diffractor) for their properties. And friction coefficient of these films was measured by ball-on-disc tester for their tribological properties. From the experimental results, it was shown that high performance properties of bearing can be improved greatly by controlling the composition and morphology of material surface with effective use of the plasma-assisted sputtering process.

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Surface morphology of Al cathode for OLED with Kr gas (Kr가스에 의한 OLED용 Al 음전극의 표면 형상)

  • Kim, Hyun-Woong;Keum, Min-Jong;Kim, Kyung-Hwan
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2005.11a
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    • pp.283-284
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    • 2005
  • Al electrode for OLED was deposited by Facing Targets Sputtering(FTS) system which can reduce the damage of organic layer. The Al thin films were deposited on the slide glass as a function of working gas such as Ar, Kr or mixed gas. The film surface image was observed by AFM and SEM. In the results, when Al thin film were deposited using mixed gas, the surface morphology was improved in some region.

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Effect of Co-solvent Ratios and Solution Concentrations on Morphologies of Electrospun Zein Nanomaterials

  • Rabbani, Mohammad Mahbub;Kim, Young Hun;Yeum, Jeong Hyun
    • Current Research on Agriculture and Life Sciences
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    • v.31 no.1
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    • pp.11-17
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    • 2013
  • To investigate the effects of co-solvents on the morphology of nano-scale zein materials, zein solutions were electrospun with different co-solvent ratios of EtOH/$H_2O$. Different zein solution concentrations were used to study the effects of the zein content on the electrospun materials. The resulting electrospun materials were all characterized using field-emission scanning electron microscopy (FE-SEM) and transmission electron microscopy (TEM). The diameters of the electrospun nanoparticles and nanofibers were found to increase when increasing the EtOH ratio at certain zein concentrations. Furthermore, increasing the zein content changed the morphology of the electrospun materials from nanoparticles to nanofibers.

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Spermatogenesis and Spermatozoan Ultrastructure of Pacific Oyster (Crassostrea gigas) (참굴 (Crassostrea gigas)의 정자형성과정과 정자미세구조)

  • KIM Jin Hee;CHANG Myo In;YOO Myong-Suk
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.36 no.6
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    • pp.641-645
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    • 2003
  • Spermatogenesis, ultrastructure, and sperm morphology of the Pacific oyster (Crassostrea gigas) were investigated with TEM and SEM. C. gigas sperm were primitive consisting of a head midpiece and tail. Sperm size (head and midpiece) was about 1.78 ${\mu}m$. Sperm morphology was similar to a sharp of a small water jar with a rough surface. Sperm had both anterior nuclear fossa (anf) and posterior nuclear fossa (pnf). Acrosome forms had a hat-like shape. The axial rod was projected in front of the acrosome. C. gigas sperm had four large mitochondria in the midpiece.

Investigation of Relationship between Etch Current and Morphology and Porosity of Porous Silicon

  • Jang, Seunghyun
    • Journal of Integrative Natural Science
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    • v.3 no.4
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    • pp.210-214
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    • 2010
  • Relationship between etch current and morphology and porosity of porous silicon (PS) has been investigated. The gravimetric method is applied to measured the porosity of PS. As the current density increase, the silicon dissolution rate increases, resulting in a higher porosity and etching rate. The result shows that linear dependence of PS porosity and etching rate as a function of current density. The morphology of porous silicon was investigated by using cold field emission scanning electron micrograph (FE-SEM). The size of pores formed during anodization is predominantly controlled by the current density, with an increase in the pore size corresponding to an increase in the current density.