• Title/Summary/Keyword: SEM morphology

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A study on the growth morphology of AlN crystals grown by a sublimation process (승화법으로 성장된 AlN 결정의 성장 양상에 관한 연구)

  • Kang, Seung-Min
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.19 no.5
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    • pp.242-245
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    • 2009
  • AlN crystals were grown by a sublimation process without seed crystals and the growth morphology of them was characterized. The grown AlN crystals were a polycrystalline phase, which had a diameter of $60\sim200\;{\mu}m$ and were grown with a growth rate of $0.2\sim0.5\;{\mu}n/hr$. It was observed that the as-grown crystals had a hexagonal crystal structure and revealed that these crystals were grown with a morphology of columnar morphology in the initial stage of the growth before they were enlarged in a way of a lateral growth behavior in the final stage. On the surface, a lot of pinholes were observed on the surface of crystals grown. The evolution of a growth morphology was characterized by optical and scanning electron microscopic observation.

A Contribution to the Pollen Morphology of Salix viminalis L. (Salix viminalis의 화분형태(花粉形態)에 관(關)한 연구(硏究))

  • Kim, Kae Hwan
    • Journal of Korean Society of Forest Science
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    • v.66 no.1
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    • pp.64-67
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    • 1984
  • The genus Salix is nowadays becoming increasingly important for both biomass energy production and the expanding paper industry. The enlarging plantations will however create some potential as well as problem. The great potential of genetical improvement as well as the prevention of pollen allergies requires knowledge about e.g, the pollen morphology of the most used Salix species. This study investigated the pollen morphology of Salix viminalis L. both on light microscope (LM) and scanning electron microscope (SEM).

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Dyeing Study on DMF-Modified Polyesters for Morphology Characterization

  • Park, Myung-Ja
    • The International Journal of Costume Culture
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    • v.5 no.2
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    • pp.53-65
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    • 2002
  • Morphology of polyester fiber was physically modified by solvent treatment. PET fiber was treated with N,N-dimethylformamide (DMF) at 100, 120, $140^{circ}C$ for 10 minutes without tension. The structural changes in the morphology of DMF-induced modified PET fiber were FTIR and SEM analysis. Also dyeing behavior of DMF-treated polyester fibers with various disperse dyes was studied to detect changes of amorphous area in fine structure. DMF treatment resulted in increases in total void content, degree of crystallinity, trans isomer content, chain folding, segmental mobility and molecular packing, but it resulted in decreases in amorphous orientation, intermolecular forces and individual void size through longitudinal shrinkage, lateral welling and removal of oligomers. Void-size distribution could be estimated from the dye uptake with various sizes of disperse dyes. In contrast to the large increases in dye uptake with small dye molecules, there is no and little dye uptake with the bulkiest dye, which means that void size is bigger or smaller than the volume of each dye. Diffusion rates of dye molecules showed increases. This dyeing study revealed that the disperse dyeing is very effective method for characterizing the internal morphology of polyester fiber.

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Magnesium Thin Films Possessing New Corrosion Resistance by RF Magnetron Sputtering Method

  • Lee, M.H.;Yun, Y.S.;Kim, K.J.;Moon, K.M.;Bae, I.Y.
    • Corrosion Science and Technology
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    • v.3 no.4
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    • pp.148-153
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    • 2004
  • Magnesium thin flims were prepared on cold-rolled steel substrates by RF magnetron sputtering technique. The influence of argon gas pressure and substrate bias voltage on their crystal orientation and morphology of the coated films were investigated by scanning electron microscopy (SEM) and X-ray diffraction, respectively. And the effect of crystal orientation and morphology of magnesium films on corrosion behaviors was estimated by measuring anodic polarization curves in deaerated 3%NaCl solution. From the experimental results, all the sputtered magnesium films showed obviously good corrosion resistance to compare with 99.99% magnesium target of the sputter-evaporation metal. Finally it was shown that the Corrosion-resistance of magnesium films can be improved greatly by controlling the crystal orientation and morphology with effective use of the plasma sputtering technique.

Structural Transcription of Organogels to Mesoporous Silicas: A Chain-length Dependent Morphology and Pore Texture

  • Huang, Yaqun
    • Bulletin of the Korean Chemical Society
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    • v.33 no.11
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    • pp.3711-3718
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    • 2012
  • Here, we report a chain-length dependent morphology and pore structure tailing of mesoporous silica templated from organogels, which is formed by primary alkylamine and ethylene glycol at room temperature. As the chain length of alkylamine changes from 12 to 18, the resulted materials exhibit a morphology change from layers to spheres and platelets, respectively. SEM and TEM observation revealed that these shapes appear to be inherited from their parent organogels. Further pore structure characterization by nitrogen sorption analysis demonstrates that all the resulted silicas exhibit typical IV isotherms indicative of uniform mesopores, and their pore sizes are dependent on the chain length of alkylamine used.

Morphological transformations during drying of surfactant-nanofluid droplets

  • Osman, Abdulkadir;Shahidzadeh, Noushine;Stitt, Hugh;Shokri, Nima
    • Journal of Industrial and Engineering Chemistry
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    • v.67
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    • pp.92-98
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    • 2018
  • The effect of surfactants with different chain length on the drying dynamics of nanosized dispersion droplets and on the final morphology of the grains formed after water evaporation is investigated experimentally. An acoustic levitator was used to examine the drying dynamics of single droplets and SEM imaging was used to characterise the morphology of the final dried grains. Results show that the drying of drops with high molecular weight surfactants leads to more irregular grains and that the grain morphology is related to surface tension driven instability of the evaporating droplets which may lead to formation of hollow dried grains.

Morphology of the Gastric Mill of Nyctiphanes australis(Euphausiacea, Crustacea)

  • SUH Hae-Lip
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.22 no.4
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    • pp.214-218
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    • 1989
  • SEM observation revealed that the gastric mill of Nyctiphanes australis consists of paired cluster spines and paired lateral teeth, while the filter-press is absent. The morphology of the gastric mill was extremely constant; the numbers of both setiform processes of cluster spines and serrated spines of lateral teeth increased with increasing body length. The cluster spines of N. australis consisted of a single row of stout setiform processes but the lateral teeth comprised a large projection with small serrated spines. The cluster spines are symmetrical in setiform process distribution, however, the lateral teeth are asymmetrical in number of serrated spines.

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Observation of the Adults and Eggs of Two Species of the Family Perlidae(Plecoptera) to Korea (강도래과(강도래목) 2 종에 대한 성충 및 란의 외부형태 관찰)

  • 나철호;백순기;조영관
    • Animal Systematics, Evolution and Diversity
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    • v.7 no.1
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    • pp.101-110
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    • 1991
  • Two species of Perlidae, Oyamia coreana and Kiotina decorata which were collected in mountain valley of the Chonnam, Chonguk and Kyongnam provinces, south Korea are reported for the first time from Korea, with description of the external morphology of their eggs by SEM.

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Relationship between the maxillofacial skeletal pattern and the morphology of the mandibular symphysis: Structural equation modeling

  • Ahn, Mi So;Shin, Sang Min;Yamaguchi, Tetsutaro;Maki, Koutaro;Wu, Te-Ju;Ko, Ching-Chang;Kim, Yong-Il
    • The korean journal of orthodontics
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    • v.49 no.3
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    • pp.170-180
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    • 2019
  • Objective: The purpose of this study was to investigate the relationship between the facial skeletal patterns and the shape of the mandibular symphysis in adults with malocclusion by using a structural equation model (SEM). Methods: Ninety adults who had malocclusion and had records of facial skeletal measurements performed using cone-beam computed tomography were selected for this study. The skeletal measurements were classified into three groups (vertical, anteroposterior, and transverse). Cross-sectional images of the mandibular symphysis were analyzed using generalized Procrustes and principal component (PC) analyses. A SEM was constructed after the factors were extracted via factor analysis. Results: Two factors were extracted from the transverse, vertical, and anteroposterior skeletal measurements. Latent variables were extracted for each factor. PC1, PC2, and PC3 were selected to analyze the variations of the mandibular symphyseal shape. The SEM was constructed using the skeletal variables, PCs, and latent variables. The SEM showed that the vertical latent variable exerted the most influence on the mandibular symphyseal shape. Conclusions: The relationship between the skeletal pattern and the mandibular symphysis was analyzed using a SEM, which showed that the vertical facial skeletal pattern had the highest effect on the shape of the mandibular symphysis.