• Title/Summary/Keyword: SEM Test

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Mechanical and wear properties evaluation of Al/Al2O3 composites fabricated by combined compo-casting and WARB process

  • Vini, Mohamad Heydari;Daneshmand, Saeed
    • Advances in Computational Design
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    • v.7 no.2
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    • pp.129-137
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    • 2022
  • Compo-casting method is one of the popular technique to produce metal based matrix composites. But, one of the main challenges in this process is un-uniform spreading of reinforced subdivisions (particles) inside the metallic matrix and the lack of desirable mechanical properties of the final produced composites due to the low bonding strength among the metal matrix and reinforcement particles. To remove these difficulties and to promote the mechanical properties of these kind of composites, the WARM ARB technique was utilized as supplementary technique to heighten the mechanical and microstructural evolution of the casted Al/Al2O3 composite strips. The microstructure evolution and mechanical properties of these composites have been considered versus different WARM ARB cycles by tensile test, average Vickers micro hardness test, wear test and scanning electron microscopy (SEM). The SEM results revealed that during the higher warm- ARB cycles, big alumina clusters are broken and make a uniform distribution of alumina particles. It was shown that cumulating the forming cycles improved the mechanical properties of composites. In general, combined compo-casting and ARB process would consent making Al/Al2O3 composites with high consistency, good microstructural and mechanical properties.

A Study on the Engineering and Environmental Characteristics of Phosphogypsum-Cement-Soil Mixtures (인산석고 시멘트 혼합토의 공학적.환경적 특성 연구)

  • Chang, Dong-Su;Yeon, Kyu-Seok;Kim, Ki-Sung;Ha, Seon-Hyo;Kim, Yong-Seong
    • Journal of The Korean Society of Agricultural Engineers
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    • v.53 no.3
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    • pp.83-91
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    • 2011
  • This study aimed to investigate the engineering and environmental characteristics of phosphogypsum-cement-soil mixtures composed of phosphogypsum, soil, and a small amount of cement was analysed on the basis of the unconfined compression test, the tensile strength test, the freezing and thawing test, the wetting and drying test, SEM and EDS analysis, XRD analysis and Leaching test. The specimens were manufactured with soil, cement and phosphogypsum. The cement contents was 10 %, and the phosphogypsum contents was 10, 20, 30, and 40 % by the weight of total dry soil. Each specimen was manufactured after curing at constant temperature and humidity room for 3, 7 and 28 days, after which the engineering characteristics of phosphogypsum-cement-soil mixtures were investigated using the unconfined compression test, the tensile strength test, the freezing and thawing test, the wetting and drying test. The basic data were presented for the application of phosphogypsum-cement-soil mixtures as construction materials. To investigate the environmental characteristics, leaching test was performed and the leaching test results were far below than of regulatory requirement of Waste Management Act in Korea. Therefore the results show that phosphogypsum is environmentally safe and can be used as construction materials in environmental aspect.

Environmental Impact Review and Improvement of Durability of Silicasol-cement Grout Material (실리카졸 약액의 환경영향성 검토 및 내구증진방안)

  • Lee, Byungho;Kim, Younghun;Chun, Byungsik
    • Journal of the Korean GEO-environmental Society
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    • v.11 no.12
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    • pp.13-18
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    • 2010
  • This study was made on the fact that the environmental impact and durability of the recently developed alkali silicasol chemical grout material. The grout material used for this study was designed to understand its environmental impact and durability through the SEM, chemical resistance test, leaching test, permeability test. In order to compare with the engineering characteristics regarding alkali silicasol grout material and sodium silicate grout material. As a result of SEM, the surface and internal tissues of alkali silicasol grout material could be identified to be denser than those of sodium silicate. As a result of leaching test the adaptability was identified as grout material as it had proved to be an ecological material owing to the total amount of the element to be leached being extremely little. As a result of permeability test it is judged that it is possible to apply the silicasol to the site in the place requiring the water cut-off as the silicasol.

Engineering Geological Properties of Mudstone and Shale (이암과 셰일의 지질공학적 특성)

  • 박형동
    • Proceedings of the Korean Geotechical Society Conference
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    • 2002.11b
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    • pp.18-30
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    • 2002
  • 이암 및 셰일은 점토를 함유하고 있어 풍화작용을 받을 경우 공학적 성질이 급격히 변화하여 강도 저하, 내구성저하현상 및 토사와 유사한 거동을 보이는 등 토목공사에 위험한 요소가 되고 있다. 풍화된 시료엔 대한 실험용 시료 가공이 어렵고 적용 가능한 실험법이 적어 공학적 특성이나 거동을 정량적으로 파악하는 기법이 다른 암종에 비해 극히 제한된다. 현재까지 강도측정과 같은 일반적인 물성의 단순측정보다는 내구성을 분석하는 슬레이킹 내구성 시험 (Slake durability test), Modified Jar test, 팽창율 측정시험 (Swelling test) 등의 정량화 시험법이 주로 사용되고 있으며 국내 현장에서도 적용을 권장할 수 있다. 이러한 실험치의 해석에서 단일 실험치 (예: 팽창율)만으로 지질공학적 특성을 파악하는 경우 잘못된 판단을 할 수도 있으므로, X선 회절분석시험 (XRD: X-Ray Diffraction Test), TG-DTA분석, 주사전자현미경 (SEM: Scanning Electron Microscope) 이미지 분석, 투수계수 측정실험 등도 함께 수행하여 실험결과를 종합적으로 해석하는 것이 바람직하다.

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Analysis of RCD'S Material Degradation by Weathering Test (내후성시험에 의한 누전차단기 재질변화 분석)

  • Kim, Chong-Min;Bang, Sun-Bae;Shong, Kil-Mok;Yong, Shin-Jin;Kim, Chang-Hwan
    • The Transactions of the Korean Institute of Electrical Engineers P
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    • v.59 no.2
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    • pp.232-237
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    • 2010
  • Fault rate of RCD is increasing due to deterioration and long period usage in domestic. According to Korean standards, the RCDs are installed in panel boards. When RCDs are installed at outdoor, the RCDs must be protected from uv, water etc. by using the housing. However, many RCDs are exposed to the external environment. As a results, many RCDs have malfunctions so that cause the electrical accidents. The RCDs manufactured by four makes were used as the sample to weathering test. Futhermore, those were analyzed the ingredients of RCD'S using SEM, EDX and FT-IR/TAR before and after weathering test.

A Study on Material Characterization and Mechanical Properties of SMC Compression Molding Parts (SMC 압축성형재의 기계적 물성 및 특성에 관한 연구)

  • 김기택;임용택
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.18 no.9
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    • pp.2396-2403
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    • 1994
  • An experimental study on material characterization and mechanical properties of SMC(Sheet Molding Compounds) compression method parts was carried out. Simple compression test using grease oil as a lubricant was carried out to characterize flow stress of SMC at elevated temperatures. Two different mold temperatures, $130^{\circ}C{\;}and{\;}150^{\circ}C$ and two different mold speeds, 15, 45 mm/min were used for preparing the specimen of SMC compression molded parts. Surface roughness, tensile, and 3-point bending tests were used to determine the effects of molding temperatures and speeds on mechanical properties of compression molded SMC parts. Orientation and distribution of glass fiber in the compression molded SMC parts were also investigated by photographing the burnt flat specimen and taking SEM(Scanning Electron Microscope) of cross-sectional T-specimen.

Morphology and Impact Strength of High Density Polyethylene/Polyamide Alloy (HDPE/PA 알로이의 모포로지와 충격강도)

  • Lee, Yong-Moo;Kang, Doo-Whan
    • Elastomers and Composites
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    • v.28 no.4
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    • pp.283-292
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    • 1993
  • The morphology and impact strength of alloys of high density polyethylene(HDPE) and nylon-6(PA) with modified $ethylene-{\alpha}-olefin$ copolymer(OCP) as compatibilizer and impact modifier were measured by the scanning electron microscope(SEM) and the notched Izod impact test(and the high rate impact test), respectively. HDPE is incompatible with PA and specimens obtained from simple mechanical mixing show the inferior properties. However, it was indicated that OCP played roles of not only impact modifier but also compatibilizer. High rate impact test results were different from those of the notched Izod impact test, but in both tests OCP was effective for HDPE/PA blends. From SEM observation, the size of the dispersed phase in alloys prepared with OCP is much smaller than that of alloys without OCP and the interfacial adhesion of alloys prepared with OCP is also better. Toughening mechanism of polymer blends was discussed by combining the morphology analysis with mechanical and thermal properties.

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Examination of the Characteristics of Mortar Mixed with Boron Compounds Presenting Various Levels of Alkalinity (다양한 알칼리도를 가진 붕소화합물이 혼입된 모르타르의 특성 검토)

  • Lee, Binna;Lee, Jong-Suk;Min, Jiyoung;Lee, Jang Hwa
    • Journal of the Korea Concrete Institute
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    • v.29 no.1
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    • pp.85-92
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    • 2017
  • This study examines the characteristics of mortar mixed with various boron compounds. The adapted boron compounds, classified into acid, slightly alkaline and strongly alkaline with respect to the value of the pH are acid-based boron (AA), low-alkaline-based boron (AB), and high-alkaline-based boron (HB). The pH test, setting test and compressive strength test are performed to evaluate the physical and chemical properties of mortar, and SEM imaging is conducted to analyze the microstructure of mortar. The measured pH shows that the specimens mixed with boron compounds have lower pH than the basic mortar without boron and that loss of pH occurs according to time. The setting test reveals that the initial and final setting times of the specimens mixed with boron compounds occur later than the basic mortar, which disagrees slightly with the previous literature stating that the setting time can be shortened according to the alkalinity. From the compressive strength test and SEM imaging results, it is recommended to determine the optimal content of boron considering type and composition of the boron compounds.

Reproducibility of the Isokinetic Joint Torque as a Rotator Cuff Weakness Test Protocol in Patients With Rotator Cuff Tendinitis

  • Kim, Soo-yong;Oh, Jae-seop
    • Physical Therapy Korea
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    • v.24 no.3
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    • pp.21-29
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    • 2017
  • Background: The measurement of the strength of the shoulder muscles is an important element of the overall assessment of patients with various shoulder disorders. However, the clinical utilization of this measurement is dependent on its reproducibility. Objects: To explore the reproducibility of the measurements derived from testing of the isokinetic strength of shoulder muscles in patients with tendinitis of the rotator cuff. Methods: A total of 20 patients with tendinitis of the rotator cuff participated in this study and were assessed twice in 1 week. Isokinetic testing was performed concentrically for shoulder flexors, abductors, and external rotators and eccentrically for the shoulder extensors, adductors, and internal rotators. The relative and absolute reproducibility of the peak torque (PT) and ratios were assessed using intra-class correlation coefficients (ICC), standard error of measurement (SEM), and minimal clinically important difference (MCID), respectively. Results: Overall, high to excellent ICC, clinically acceptable SEM and MCID values were obtained for the PT (ICC: .83-.95, SEM: 1.2%-9%, MCID: 3.4%-25%) and ratios (ICC: .85-.93, SEM: 5.1%-10%, MCID: 14.2%-27.6%). Conclusion: These findings suggest that isokinetic tests may be effectively utilized for the determination of shoulder strength profiles and appropriate position are recommended to perform test without pain in patients with tendinitis of the rotator cuff.

In-Situ SEM Observation and DIC Strain Analysis for Deformation and Cracking of Hot-Dip ZnMgAl Alloy Coating

  • Naoki Takata;Hiroki Yokoi;Dasom Kim;Asuka Suzuki;Makoto Kobashi
    • Corrosion Science and Technology
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    • v.23 no.2
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    • pp.113-120
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    • 2024
  • An attempt was made to apply digital image correlation (DIC) strain analysis to in-situ scanning electron microscopy (SEM) observations of bending deformation to quantify local strain distribution inside a ZnMgAl-alloy coating in deformation. Interstitial-free steel sheets were hot-dipped in a Zn-3Mg-6Al (mass%) alloy melt at 400 ℃ for 2 s. The specimens were deformed using a miniature-sized 4-point bending test machine inside the SEM chamber. The observed in situ SEM images were used for DIC strain analysis. The hot-dip ZnMgAl-alloy coating exhibited a solidification microstructure composed of a three-phase eutectic of fine Al (fcc), Zn (hcp), and Zn2Mg phases surrounding the primary solidified Al phases. The relatively coarsened Zn2Mg phases were locally observed inside the ZnMgAl-alloy coating. The DIC strain analysis revealed that the strain was localized in the primary solidified Al phases and fine eutectic microstructure around the Zn2Mg phase. The results indicated high deformability of the multi-phase microstructure of the ZnMgAl-alloy coating.